CN102190801A - 一种以单一乳化剂制备非离子型氧化聚乙烯蜡乳液的方法 - Google Patents
一种以单一乳化剂制备非离子型氧化聚乙烯蜡乳液的方法 Download PDFInfo
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- CN102190801A CN102190801A CN 201110076883 CN201110076883A CN102190801A CN 102190801 A CN102190801 A CN 102190801A CN 201110076883 CN201110076883 CN 201110076883 CN 201110076883 A CN201110076883 A CN 201110076883A CN 102190801 A CN102190801 A CN 102190801A
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- polyoxyethylene
- emulsion
- wax
- pressure
- glycol
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000839 emulsion Substances 0.000 title claims abstract description 49
- 239000003995 emulsifying agent Substances 0.000 title claims abstract description 15
- 238000002360 preparation method Methods 0.000 title abstract description 9
- 235000013873 oxidized polyethylene wax Nutrition 0.000 title abstract 3
- 239000004209 oxidized polyethylene wax Substances 0.000 title abstract 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims abstract description 31
- -1 polyethylene Polymers 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 17
- 238000004945 emulsification Methods 0.000 claims abstract description 14
- 239000012875 nonionic emulsifier Substances 0.000 claims abstract description 14
- 239000008367 deionised water Substances 0.000 claims abstract description 9
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 9
- HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 claims abstract description 6
- 235000010262 sodium metabisulphite Nutrition 0.000 claims abstract description 6
- 239000001993 wax Substances 0.000 claims description 34
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 13
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 10
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 10
- 239000002671 adjuvant Substances 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 6
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 5
- 239000002826 coolant Substances 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 5
- 235000011187 glycerol Nutrition 0.000 claims description 5
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- ALSTYHKOOCGGFT-KTKRTIGZSA-N (9Z)-octadecen-1-ol Chemical compound CCCCCCCC\C=C/CCCCCCCCO ALSTYHKOOCGGFT-KTKRTIGZSA-N 0.000 claims description 4
- 229920002582 Polyethylene Glycol 600 Polymers 0.000 claims description 4
- KBPLFHHGFOOTCA-UHFFFAOYSA-N caprylic alcohol Natural products CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 claims description 4
- 229940055577 oleyl alcohol Drugs 0.000 claims description 4
- XMLQWXUVTXCDDL-UHFFFAOYSA-N oleyl alcohol Natural products CCCCCCC=CCCCCCCCCCCO XMLQWXUVTXCDDL-UHFFFAOYSA-N 0.000 claims description 4
- 229940057847 polyethylene glycol 600 Drugs 0.000 claims description 4
- 235000010486 polyoxyethylene sorbitan monolaurate Nutrition 0.000 claims description 4
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 4
- 229920000053 polysorbate 80 Polymers 0.000 claims description 4
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 3
- ONJQDTZCDSESIW-UHFFFAOYSA-N polidocanol Chemical compound CCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO ONJQDTZCDSESIW-UHFFFAOYSA-N 0.000 claims description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 2
- MOKBFXZQXUZAMV-UHFFFAOYSA-N 2-[2-[2-[2-[2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethyl octadecanoate Chemical group CCCCCCCCCCCCCCCCCC(=O)OCCOCCOCCOCCOCCOCCOCCOCCO MOKBFXZQXUZAMV-UHFFFAOYSA-N 0.000 claims description 2
- NLMKTBGFQGKQEV-UHFFFAOYSA-N 2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-(2-hexadecoxyethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethanol Chemical group CCCCCCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO NLMKTBGFQGKQEV-UHFFFAOYSA-N 0.000 claims description 2
- QYOVMAREBTZLBT-KTKRTIGZSA-N CCCCCCCC\C=C/CCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO Chemical group CCCCCCCC\C=C/CCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO QYOVMAREBTZLBT-KTKRTIGZSA-N 0.000 claims description 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 2
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 claims description 2
- 229920001213 Polysorbate 20 Polymers 0.000 claims description 2
- DTPCFIHYWYONMD-UHFFFAOYSA-N decaethylene glycol Polymers OCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO DTPCFIHYWYONMD-UHFFFAOYSA-N 0.000 claims description 2
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 2
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical compound CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 claims description 2
- 229940070765 laurate Drugs 0.000 claims description 2
- 229960003511 macrogol Drugs 0.000 claims description 2
- TVMXDCGIABBOFY-UHFFFAOYSA-N n-Octanol Natural products CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 claims description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 2
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 claims description 2
- 239000000600 sorbitol Substances 0.000 claims description 2
- 239000012177 spermaceti Substances 0.000 claims description 2
- 229940084106 spermaceti Drugs 0.000 claims description 2
- 239000007787 solid Substances 0.000 abstract description 11
- 238000004519 manufacturing process Methods 0.000 abstract description 10
- 238000006243 chemical reaction Methods 0.000 abstract description 7
- 239000004698 Polyethylene Substances 0.000 abstract description 5
- 230000001804 emulsifying effect Effects 0.000 abstract description 5
- 229920000573 polyethylene Polymers 0.000 abstract description 5
- 239000002245 particle Substances 0.000 abstract description 4
- 238000007789 sealing Methods 0.000 abstract description 4
- 239000004530 micro-emulsion Substances 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 229940001584 sodium metabisulfite Drugs 0.000 abstract 1
- 239000000047 product Substances 0.000 description 13
- 238000005516 engineering process Methods 0.000 description 9
- 239000004567 concrete Substances 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 239000010985 leather Substances 0.000 description 4
- 238000012986 modification Methods 0.000 description 4
- 230000004048 modification Effects 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 238000009941 weaving Methods 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 238000001556 precipitation Methods 0.000 description 3
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000008267 milk Substances 0.000 description 2
- 210000004080 milk Anatomy 0.000 description 2
- 235000013336 milk Nutrition 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 description 1
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 description 1
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 description 1
- 241000153282 Theope Species 0.000 description 1
- 239000012164 animal wax Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000008387 emulsifying waxe Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 235000012055 fruits and vegetables Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 1
- UGTZMIPZNRIWHX-UHFFFAOYSA-K sodium trimetaphosphate Chemical compound [Na+].[Na+].[Na+].[O-]P1(=O)OP([O-])(=O)OP([O-])(=O)O1 UGTZMIPZNRIWHX-UHFFFAOYSA-K 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Landscapes
- Medicinal Preparation (AREA)
- Paints Or Removers (AREA)
- Colloid Chemistry (AREA)
Abstract
Description
去离子水 | 69% |
AC-629 | 25% |
Brij-721 | 4.5% |
乙二醇 | 1.2% |
KOH | 0.25% |
Na2S2O5 | 0.05% |
去离子水 | 61.4% |
AC-629 | 31.0% |
AEO-9 | 6.0% |
丙三醇 | 1.0% |
KOH | 0.5% |
Na2S2O5 | 0.1% |
去离子水 | 55% |
AC-629 | 37% |
Tween-60 | 5.5% |
二甘醇 | 1.5% |
KOH | 0.8% |
Na2S2O5 | 0.2% |
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2011100768830A CN102190801B (zh) | 2011-03-29 | 2011-03-29 | 一种以单一乳化剂制备非离子型氧化聚乙烯蜡乳液的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN2011100768830A CN102190801B (zh) | 2011-03-29 | 2011-03-29 | 一种以单一乳化剂制备非离子型氧化聚乙烯蜡乳液的方法 |
Publications (2)
Publication Number | Publication Date |
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CN102190801A true CN102190801A (zh) | 2011-09-21 |
CN102190801B CN102190801B (zh) | 2012-11-21 |
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CN2011100768830A Expired - Fee Related CN102190801B (zh) | 2011-03-29 | 2011-03-29 | 一种以单一乳化剂制备非离子型氧化聚乙烯蜡乳液的方法 |
Country Status (1)
Country | Link |
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CN (1) | CN102190801B (zh) |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102532919A (zh) * | 2011-12-27 | 2012-07-04 | 深圳市乐普泰科技股份有限公司 | 纳米蜡乳液及其制备方法 |
CN103965657B (zh) * | 2014-05-05 | 2016-01-13 | 潍坊大耀新材料有限公司 | 一种ZnS粉的表面改性方法 |
US9238777B2 (en) | 2012-08-29 | 2016-01-19 | Metadynea Austria Gmbh | Method for producing phosphorus-containing flame retardants |
CN107892754A (zh) * | 2017-12-04 | 2018-04-10 | 上海雅运纺织助剂有限公司 | 一种多功能氧化聚乙烯蜡乳液及其制备方法 |
CN108586875A (zh) * | 2018-05-10 | 2018-09-28 | 浙江农林大学 | 一种天然纤维改性增强剂、增强剂制备方法、制备的复合材料及其复合材料制备方法 |
CN109169078A (zh) * | 2018-09-12 | 2019-01-11 | 蚌埠市瑞丰现代农业种植专业合作社 | 一种改良稻田土壤的种植方法 |
CN111234261A (zh) * | 2020-03-26 | 2020-06-05 | 湖南科技大学 | 两步乳化法制备高密度氧化聚乙烯微乳液 |
CN111253589A (zh) * | 2020-03-27 | 2020-06-09 | 东莞市汉维科技股份有限公司 | 一种超疏水高密度氧化聚乙烯微乳液的两步乳化法制备工艺 |
CN111647174A (zh) * | 2020-06-16 | 2020-09-11 | 天津洁清馨科技有限公司 | 一种除醛净味纳米蜡 |
CN113121844A (zh) * | 2019-12-31 | 2021-07-16 | 广州麦吉高分子新材料科技有限公司 | 一种纳米级乳化蜡制备方法 |
EP4145999A1 (en) * | 2020-05-05 | 2023-03-15 | Macquarie University | Fruit fly control |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20050107511A1 (en) * | 2002-02-14 | 2005-05-19 | Gerd Hohner | Utilization of oxidized polyolefin waxes for textile finishing |
CN101289540A (zh) * | 2008-06-12 | 2008-10-22 | 广东纺织职业技术学院 | 氧化聚乙烯蜡微乳液的制备方法 |
-
2011
- 2011-03-29 CN CN2011100768830A patent/CN102190801B/zh not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20050107511A1 (en) * | 2002-02-14 | 2005-05-19 | Gerd Hohner | Utilization of oxidized polyolefin waxes for textile finishing |
CN101289540A (zh) * | 2008-06-12 | 2008-10-22 | 广东纺织职业技术学院 | 氧化聚乙烯蜡微乳液的制备方法 |
Non-Patent Citations (1)
Title |
---|
《皮革科学与工程》 20100430 强西怀等 "氧化聚乙烯蜡乳液的制备及在皮革涂饰中的应用" 第20卷, 第2期 * |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102532919A (zh) * | 2011-12-27 | 2012-07-04 | 深圳市乐普泰科技股份有限公司 | 纳米蜡乳液及其制备方法 |
US9238777B2 (en) | 2012-08-29 | 2016-01-19 | Metadynea Austria Gmbh | Method for producing phosphorus-containing flame retardants |
CN103965657B (zh) * | 2014-05-05 | 2016-01-13 | 潍坊大耀新材料有限公司 | 一种ZnS粉的表面改性方法 |
CN107892754B (zh) * | 2017-12-04 | 2020-05-19 | 上海雅运新材料有限公司 | 一种多功能氧化聚乙烯蜡乳液及其制备方法 |
CN107892754A (zh) * | 2017-12-04 | 2018-04-10 | 上海雅运纺织助剂有限公司 | 一种多功能氧化聚乙烯蜡乳液及其制备方法 |
CN108586875A (zh) * | 2018-05-10 | 2018-09-28 | 浙江农林大学 | 一种天然纤维改性增强剂、增强剂制备方法、制备的复合材料及其复合材料制备方法 |
CN109169078A (zh) * | 2018-09-12 | 2019-01-11 | 蚌埠市瑞丰现代农业种植专业合作社 | 一种改良稻田土壤的种植方法 |
CN113121844A (zh) * | 2019-12-31 | 2021-07-16 | 广州麦吉高分子新材料科技有限公司 | 一种纳米级乳化蜡制备方法 |
CN111234261A (zh) * | 2020-03-26 | 2020-06-05 | 湖南科技大学 | 两步乳化法制备高密度氧化聚乙烯微乳液 |
CN111253589A (zh) * | 2020-03-27 | 2020-06-09 | 东莞市汉维科技股份有限公司 | 一种超疏水高密度氧化聚乙烯微乳液的两步乳化法制备工艺 |
EP4145999A1 (en) * | 2020-05-05 | 2023-03-15 | Macquarie University | Fruit fly control |
EP4145999A4 (en) * | 2020-05-05 | 2024-05-22 | Macquarie University | FRUIT FLY CONTROL |
CN111647174A (zh) * | 2020-06-16 | 2020-09-11 | 天津洁清馨科技有限公司 | 一种除醛净味纳米蜡 |
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CN102190801B (zh) | 2012-11-21 |
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