CN102176970B - 基于izm-2沸石的催化剂和含烃进料的加氢转化/加氢裂化的方法 - Google Patents

基于izm-2沸石的催化剂和含烃进料的加氢转化/加氢裂化的方法 Download PDF

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CN102176970B
CN102176970B CN2009801397576A CN200980139757A CN102176970B CN 102176970 B CN102176970 B CN 102176970B CN 2009801397576 A CN2009801397576 A CN 2009801397576A CN 200980139757 A CN200980139757 A CN 200980139757A CN 102176970 B CN102176970 B CN 102176970B
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catalyst
izm
weight
hydrocracking
zeolite
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CN102176970A (zh
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E·吉永
L·西蒙
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IFP Energies Nouvelles IFPEN
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/72—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing iron group metals, noble metals or copper
    • B01J29/76—Iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/78—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/20—Sulfiding
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/04—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used
    • C10G45/12—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C10G47/16—Crystalline alumino-silicate carriers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C10G47/16—Crystalline alumino-silicate carriers
    • C10G47/20—Crystalline alumino-silicate carriers the catalyst containing other metals or compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B01J21/04—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/12—Silica and alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/20—After treatment, characterised by the effect to be obtained to introduce other elements in the catalyst composition comprising the molecular sieve, but not specially in or on the molecular sieve itself
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/107—Atmospheric residues having a boiling point of at least about 538 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1074—Vacuum distillates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1077—Vacuum residues
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4018—Spatial velocity, e.g. LHSV, WHSV

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
CN2009801397576A 2008-08-08 2009-07-29 基于izm-2沸石的催化剂和含烃进料的加氢转化/加氢裂化的方法 Active CN102176970B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0804562A FR2934796B1 (fr) 2008-08-08 2008-08-08 Catalyseur a base de zeolithe izm-2 et procede d'hydroconversion/hydrocraquage de charges hydrocarbonees
FR08/04562 2008-08-08
PCT/FR2009/000942 WO2010015736A1 (fr) 2008-08-08 2009-07-29 Catalyseur à base de zéolithe izm-2 et procédé d'hydroconversion / hydrocraquage de charges hydrocarbonées

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CN102176970A CN102176970A (zh) 2011-09-07
CN102176970B true CN102176970B (zh) 2013-06-19

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US (1) US8936717B2 (enExample)
EP (1) EP2313195B1 (enExample)
JP (1) JP5577339B2 (enExample)
KR (1) KR101581983B1 (enExample)
CN (1) CN102176970B (enExample)
AT (1) ATE556771T1 (enExample)
DK (1) DK2313195T3 (enExample)
ES (1) ES2387864T3 (enExample)
FR (1) FR2934796B1 (enExample)
RU (1) RU2487755C2 (enExample)
WO (1) WO2010015736A1 (enExample)

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FR2934793B1 (fr) * 2008-08-08 2010-11-19 Inst Francais Du Petrole Catalyseur comprenant une zeolithe izm-2 et au moins un metal et son utilisation en transformation d'hydrocarbures
CN103842294B (zh) * 2011-08-04 2016-08-17 埃克森美孚化学专利公司 Emm-23分子筛材料、其合成和用途
KR101996105B1 (ko) 2011-10-12 2019-07-03 엑손모빌 리서치 앤드 엔지니어링 컴퍼니 Ｍｓｅ-골격 타입 분자체의 합성
CA2851798C (en) 2011-10-12 2018-01-02 Exxonmobil Research And Engineering Company Synthesis of mse-framework type molecular sieves
FR2984911B1 (fr) * 2011-12-22 2014-08-29 IFP Energies Nouvelles Procede de conversion de charges paraffiniques issues de la biomasse en bases distillats moyens mettant en oeuvre au moins un catalyseur a base de zeolithe izm-2
JP5862807B2 (ja) * 2012-02-21 2016-02-16 エクソンモービル ケミカル パテンツ インコーポレイテッド 分子篩材料、その合成および使用
FR2989382B1 (fr) * 2012-04-11 2016-01-01 IFP Energies Nouvelles Procede de deparaffinage de charges hydrocarbonees utilisant un catalyseur a base de zeolithe izm-2
FR2989383B1 (fr) * 2012-04-11 2015-10-30 IFP Energies Nouvelles Procede d'hydrotraitement et de deparaffinage d'une charge distillat moyen utilisant un catalyseur a base de zeolithe izm-2
RU2612134C1 (ru) * 2015-12-25 2017-03-02 Акционерное общество "Всероссийский научно-исследовательский институт по переработке нефти" (АО "ВНИИ НП") Катализатор гидроизодепарафинизации среднедистиллятных углеводородных фракций
FR3064262B1 (fr) * 2017-03-24 2019-03-22 IFP Energies Nouvelles Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane
FR3064261B1 (fr) * 2017-03-24 2019-03-22 IFP Energies Nouvelles Procede de synthese de la zeolithe izm-2 en presence d'un structurant dihydroxyde de 1,6-bis(methylpiperidinium)hexane
CN110248894B (zh) 2017-04-28 2022-08-19 雪佛龙美国公司 分子筛ssz-109、其合成和用途
WO2018229582A1 (en) * 2017-06-12 2018-12-20 Chevron U.S.A. Inc. Molecular sieve ssz-111, its synthesis and use
CN107140657B (zh) * 2017-06-29 2019-04-23 中国科学院上海高等研究院 一种izm-2分子筛的制备方法
FR3074428B1 (fr) * 2017-12-06 2022-01-21 Ifp Energies Now Procede de preparation d'un catalyseur a base d'izm-2 a partir d'une solution comprenant des precurseurs specifiques et utilisation pour l'isomerisation de charges paraffiniques
RU184350U1 (ru) * 2018-03-29 2018-10-23 Федеральное государственное бюджетное учреждение науки Институт физической химии и электрохимии им. А.Н. Фрумкина Российской академии наук (ИФХЭ РАН) Комбинированный фильтр для очистки радиоактивной парогазовой смеси
FR3101342B1 (fr) * 2019-09-26 2021-10-15 Ifp Energies Now Procede de preparation d’une zeolithe izm-2 en presence d’un melange de structurants organiques azotes sous forme hydroxyde et bromure et d’un chlorure de metal alcalin
FR3112790B1 (fr) * 2020-07-23 2023-02-24 Ifp Energies Now Procede de deparaffinage d’une charge distillat moyen utilisant un catalyseur a base de zeolithe izm-2 et d’une zeolithe de type mfi
US11542442B1 (en) 2022-04-05 2023-01-03 Saudi Arabian Oil Company Hydrocracking process and system including separation of heavy poly nuclear aromatics from recycle with heteropoly acids
FR3148602A1 (fr) * 2023-05-12 2024-11-15 IFP Energies Nouvelles Procédé d'hydrotraitement et d'hydroisomérisation d'huile végétale en une étape utilisant au moins un catalyseur sulfure avec une zéolithe isomérisante

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FR2931833B1 (fr) * 2008-05-28 2011-06-10 Inst Francais Du Petrole Procede de production de distillats moyens par hydrocraquage de charges issues du procede fischer-tropsch avec un catalyseur a base d'un materiau amorphe
FR2931834B1 (fr) 2008-05-28 2010-07-30 Inst Francais Du Petrole Procede de production de distillats moyens par hydrocraquage de charges issues du procede fischer-tropsch avec un catalyseur a base d'un materiau cristallise
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Publication number Priority date Publication date Assignee Title
US5207893A (en) * 1989-02-07 1993-05-04 Research Association For Residual Oil Processing Hydrocracking process employing a novel iron-containing aluminosilicate
EP1702888A1 (fr) * 2005-03-07 2006-09-20 Institut Francais Du Petrole Solide cristallise COK-7, procécé de préparation et utilisation pour la transformation d'hydrocarbures
EP1953118A1 (fr) * 2007-01-30 2008-08-06 Ifp Solide cristallisé IZM-1 et son procédé de préparation

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US20110192765A1 (en) 2011-08-11
DK2313195T3 (da) 2012-08-27
ATE556771T1 (de) 2012-05-15
CN102176970A (zh) 2011-09-07
EP2313195A1 (fr) 2011-04-27
KR20110042347A (ko) 2011-04-26
JP5577339B2 (ja) 2014-08-20
RU2487755C2 (ru) 2013-07-20
ES2387864T3 (es) 2012-10-03
EP2313195B1 (fr) 2012-05-09
US8936717B2 (en) 2015-01-20
FR2934796B1 (fr) 2010-09-03
JP2011530397A (ja) 2011-12-22
FR2934796A1 (fr) 2010-02-12
KR101581983B1 (ko) 2015-12-31
WO2010015736A1 (fr) 2010-02-11
RU2011108384A (ru) 2012-09-20

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