CN102107857B - 四氟化硫的提纯精馏工艺 - Google Patents
四氟化硫的提纯精馏工艺 Download PDFInfo
- Publication number
- CN102107857B CN102107857B CN2011100603274A CN201110060327A CN102107857B CN 102107857 B CN102107857 B CN 102107857B CN 2011100603274 A CN2011100603274 A CN 2011100603274A CN 201110060327 A CN201110060327 A CN 201110060327A CN 102107857 B CN102107857 B CN 102107857B
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- CN
- China
- Prior art keywords
- sulfur tetrafluoride
- gas
- sulfur
- purity
- iodine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- QHMQWEPBXSHHLH-UHFFFAOYSA-N sulfur tetrafluoride Chemical compound FS(F)(F)F QHMQWEPBXSHHLH-UHFFFAOYSA-N 0.000 title claims abstract description 105
- 238000000034 method Methods 0.000 title claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 24
- 238000009833 condensation Methods 0.000 claims abstract description 22
- 230000005494 condensation Effects 0.000 claims abstract description 22
- CEBDXRXVGUQZJK-UHFFFAOYSA-N 2-methyl-1-benzofuran-7-carboxylic acid Chemical compound C1=CC(C(O)=O)=C2OC(C)=CC2=C1 CEBDXRXVGUQZJK-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910000831 Steel Inorganic materials 0.000 claims abstract description 15
- 239000010959 steel Substances 0.000 claims abstract description 15
- 238000001816 cooling Methods 0.000 claims abstract description 8
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000000926 separation method Methods 0.000 claims abstract description 4
- 239000007789 gas Substances 0.000 claims description 75
- 238000000746 purification Methods 0.000 claims description 22
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 13
- 229910052731 fluorine Inorganic materials 0.000 claims description 13
- 239000011737 fluorine Substances 0.000 claims description 13
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 12
- 238000000465 moulding Methods 0.000 claims description 12
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 9
- 229910052740 iodine Inorganic materials 0.000 claims description 9
- 239000011630 iodine Substances 0.000 claims description 9
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 6
- 239000005864 Sulphur Substances 0.000 claims description 6
- 238000004458 analytical method Methods 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 6
- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims description 6
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims description 6
- 230000000717 retained effect Effects 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000004064 recycling Methods 0.000 claims description 3
- 230000014759 maintenance of location Effects 0.000 claims 1
- 238000005516 engineering process Methods 0.000 abstract description 12
- 229910052717 sulfur Inorganic materials 0.000 abstract 1
- 239000011593 sulfur Substances 0.000 abstract 1
- 239000012535 impurity Substances 0.000 description 5
- 230000002950 deficient Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 206010000372 Accident at work Diseases 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910018503 SF6 Inorganic materials 0.000 description 1
- UOBPHQJGWSVXFS-UHFFFAOYSA-N [O].[F] Chemical compound [O].[F] UOBPHQJGWSVXFS-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910001512 metal fluoride Inorganic materials 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- SFZCNBIFKDRMGX-UHFFFAOYSA-N sulfur hexafluoride Chemical compound FS(F)(F)(F)(F)F SFZCNBIFKDRMGX-UHFFFAOYSA-N 0.000 description 1
- 229960000909 sulfur hexafluoride Drugs 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
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Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2011100603274A CN102107857B (zh) | 2011-03-14 | 2011-03-14 | 四氟化硫的提纯精馏工艺 |
Applications Claiming Priority (1)
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CN2011100603274A CN102107857B (zh) | 2011-03-14 | 2011-03-14 | 四氟化硫的提纯精馏工艺 |
Publications (2)
Publication Number | Publication Date |
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CN102107857A CN102107857A (zh) | 2011-06-29 |
CN102107857B true CN102107857B (zh) | 2012-05-09 |
Family
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Family Applications (1)
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CN2011100603274A Active CN102107857B (zh) | 2011-03-14 | 2011-03-14 | 四氟化硫的提纯精馏工艺 |
Country Status (1)
Country | Link |
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CN (1) | CN102107857B (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP7057489B2 (ja) | 2016-12-26 | 2022-04-20 | ダイキン工業株式会社 | ジフルオロメチレン化合物の製造方法 |
CN109704291A (zh) * | 2019-03-01 | 2019-05-03 | 绵阳华鑫瑞建筑劳务有限公司 | 一种四氟化硫的提纯精馏工艺 |
CN113307232A (zh) * | 2021-05-20 | 2021-08-27 | 洛阳森蓝化工材料科技有限公司 | 一种六氟化硫和四氟化硫混合气的制备及分离方法 |
CN114348971B (zh) * | 2022-02-17 | 2023-05-12 | 中船(邯郸)派瑞特种气体股份有限公司 | 一种四氟化硫的制备方法及装置 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2217971A1 (de) * | 1972-04-14 | 1973-10-25 | Kali Chemie Ag | Verfahren zur kontinuierlichen herstellung von schwefeltetrafluorid |
US6764670B2 (en) * | 2001-11-01 | 2004-07-20 | Air Products And Chemicals, Inc. | Removal of thiothionylfluoride from sulfur tetrafluoride |
CN1644490A (zh) * | 2004-12-22 | 2005-07-27 | 马本辉 | 一种连续生产四氟化硫的方法 |
-
2011
- 2011-03-14 CN CN2011100603274A patent/CN102107857B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2217971A1 (de) * | 1972-04-14 | 1973-10-25 | Kali Chemie Ag | Verfahren zur kontinuierlichen herstellung von schwefeltetrafluorid |
US6764670B2 (en) * | 2001-11-01 | 2004-07-20 | Air Products And Chemicals, Inc. | Removal of thiothionylfluoride from sulfur tetrafluoride |
CN1644490A (zh) * | 2004-12-22 | 2005-07-27 | 马本辉 | 一种连续生产四氟化硫的方法 |
Non-Patent Citations (1)
Title |
---|
周伟杰等.四氟化硫的制备和提纯方法.《浙江化工》.2009,第40卷(第6期),1-4. * |
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Publication number | Publication date |
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CN102107857A (zh) | 2011-06-29 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20110629 Assignee: Shandong Ruihua Fluoride Industry Co., Ltd. Assignor: Li Xueqing Contract record no.: 2015370000051 Denomination of invention: Process for purifying and rectifying sulfur tetrafluoride Granted publication date: 20120509 License type: Exclusive License Record date: 20150408 |
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LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
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Effective date of registration: 20170816 Address after: 274700 Yuncheng Industrial Park, Heze, Shandong Patentee after: Shandong Ruihua Fluoride Industry Co., Ltd. Address before: 610015 No. three, unit 16, 13, lane, Qingyang District, Sichuan, Chengdu Patentee before: Li Xueqing |