CN102091754A - 纳米稀土水溶胶的制备方法 - Google Patents
纳米稀土水溶胶的制备方法 Download PDFInfo
- Publication number
- CN102091754A CN102091754A CN 201010564497 CN201010564497A CN102091754A CN 102091754 A CN102091754 A CN 102091754A CN 201010564497 CN201010564497 CN 201010564497 CN 201010564497 A CN201010564497 A CN 201010564497A CN 102091754 A CN102091754 A CN 102091754A
- Authority
- CN
- China
- Prior art keywords
- solution
- water
- hydrosol
- nano rare
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052761 rare earth metal Inorganic materials 0.000 title claims abstract description 27
- 150000002910 rare earth metals Chemical class 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000000243 solution Substances 0.000 claims abstract description 22
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 235000011114 ammonium hydroxide Nutrition 0.000 claims abstract description 8
- 239000012065 filter cake Substances 0.000 claims abstract description 6
- 239000011259 mixed solution Substances 0.000 claims abstract description 6
- 238000005406 washing Methods 0.000 claims abstract description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims abstract description 3
- 238000000034 method Methods 0.000 claims abstract description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 14
- 238000000605 extraction Methods 0.000 claims description 5
- 238000000967 suction filtration Methods 0.000 claims description 5
- 239000003153 chemical reaction reagent Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 230000001376 precipitating effect Effects 0.000 claims description 4
- 239000006185 dispersion Substances 0.000 abstract description 9
- 238000005266 casting Methods 0.000 abstract description 6
- 238000005054 agglomeration Methods 0.000 abstract description 2
- 230000002776 aggregation Effects 0.000 abstract description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Inorganic materials [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 abstract 1
- 235000010333 potassium nitrate Nutrition 0.000 abstract 1
- 229910001404 rare earth metal oxide Inorganic materials 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 239000011164 primary particle Substances 0.000 description 4
- 230000005540 biological transmission Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 239000007767 bonding agent Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000002105 nanoparticle Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- OBOSXEWFRARQPU-UHFFFAOYSA-N 2-n,2-n-dimethylpyridine-2,5-diamine Chemical compound CN(C)C1=CC=C(N)C=N1 OBOSXEWFRARQPU-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
- 229910018095 Ni-MH Inorganic materials 0.000 description 1
- 229910018477 Ni—MH Inorganic materials 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- VYLVYHXQOHJDJL-UHFFFAOYSA-K cerium trichloride Chemical compound Cl[Ce](Cl)Cl VYLVYHXQOHJDJL-UHFFFAOYSA-K 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000010041 electrostatic spinning Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229940074869 marquis Drugs 0.000 description 1
- LGZXYFMMLRYXLK-UHFFFAOYSA-N mercury(2+);sulfide Chemical compound [S-2].[Hg+2] LGZXYFMMLRYXLK-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- LHBNLZDGIPPZLL-UHFFFAOYSA-K praseodymium(iii) chloride Chemical compound Cl[Pr](Cl)Cl LHBNLZDGIPPZLL-UHFFFAOYSA-K 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- -1 rare earth compound Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Colloid Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201010564497 CN102091754B (zh) | 2010-11-30 | 2010-11-30 | 纳米稀土水溶胶的制备方法 |
Applications Claiming Priority (1)
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---|---|---|---|
CN 201010564497 CN102091754B (zh) | 2010-11-30 | 2010-11-30 | 纳米稀土水溶胶的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102091754A true CN102091754A (zh) | 2011-06-15 |
CN102091754B CN102091754B (zh) | 2013-01-23 |
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CN 201010564497 Active CN102091754B (zh) | 2010-11-30 | 2010-11-30 | 纳米稀土水溶胶的制备方法 |
Country Status (1)
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CN (1) | CN102091754B (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105597726A (zh) * | 2014-11-18 | 2016-05-25 | 天津发洋环保科技有限公司 | 一种复合光触媒水溶胶 |
CN108311156A (zh) * | 2018-02-01 | 2018-07-24 | 广州市新稀冶金化工有限公司 | 基于纳米稀土水溶胶的无矾脱硝催化剂及其制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1361750A (zh) * | 1999-06-16 | 2002-07-31 | 罗狄亚化学公司 | 铈和/或镧的磷酸盐凝胶,其制备方法及其在抛光中的应用 |
CN1568288A (zh) * | 2001-09-12 | 2005-01-19 | 罗狄亚电子与催化公司 | 稀土金属钒酸盐或磷钒酸盐颗粒的胶态分散体 |
EP1878698A2 (de) * | 2006-07-13 | 2008-01-16 | H.C. Starck GmbH | Hydrothermales Verfahren zur Herstellung von nano- bis mikroskaligen Partikeln |
US7407604B2 (en) * | 2004-01-08 | 2008-08-05 | Rutgers The State University Of New Jersey | Nanostructured re-doped SiO2-base fluorescent materials and methods for production of same |
-
2010
- 2010-11-30 CN CN 201010564497 patent/CN102091754B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1361750A (zh) * | 1999-06-16 | 2002-07-31 | 罗狄亚化学公司 | 铈和/或镧的磷酸盐凝胶,其制备方法及其在抛光中的应用 |
CN1568288A (zh) * | 2001-09-12 | 2005-01-19 | 罗狄亚电子与催化公司 | 稀土金属钒酸盐或磷钒酸盐颗粒的胶态分散体 |
US7407604B2 (en) * | 2004-01-08 | 2008-08-05 | Rutgers The State University Of New Jersey | Nanostructured re-doped SiO2-base fluorescent materials and methods for production of same |
EP1878698A2 (de) * | 2006-07-13 | 2008-01-16 | H.C. Starck GmbH | Hydrothermales Verfahren zur Herstellung von nano- bis mikroskaligen Partikeln |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105597726A (zh) * | 2014-11-18 | 2016-05-25 | 天津发洋环保科技有限公司 | 一种复合光触媒水溶胶 |
CN108311156A (zh) * | 2018-02-01 | 2018-07-24 | 广州市新稀冶金化工有限公司 | 基于纳米稀土水溶胶的无矾脱硝催化剂及其制备方法 |
Also Published As
Publication number | Publication date |
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CN102091754B (zh) | 2013-01-23 |
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EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Changzhou Geoquin Nano New Materials Co., Ltd. Assignor: Shi Liping Contract record no.: 2011320000973 Denomination of invention: Preparation method of nano rare-earth hydrosol License type: Exclusive License Open date: 20110615 Record date: 20110713 |
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C14 | Grant of patent or utility model | ||
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C41 | Transfer of patent application or patent right or utility model | ||
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Effective date of registration: 20170204 Address after: Zou Quzhen Zhonglou District Longtan Village 213000 Jiangsu city of Changzhou Province Patentee after: Changzhou Geoquin Nano New Materials Co., Ltd. Address before: 213144 Jiangsu Province, Changzhou City Longtan Village Wujin District Zou Changzhou Zhuoqun Nanometer Materials Co Ltd Patentee before: Shi Liping |