CN102077992A - Sheep embryo gelatin health food and preparation method thereof - Google Patents
Sheep embryo gelatin health food and preparation method thereof Download PDFInfo
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- CN102077992A CN102077992A CN2009103106952A CN200910310695A CN102077992A CN 102077992 A CN102077992 A CN 102077992A CN 2009103106952 A CN2009103106952 A CN 2009103106952A CN 200910310695 A CN200910310695 A CN 200910310695A CN 102077992 A CN102077992 A CN 102077992A
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- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention provides a sheep embryo gelatin health food comprising the following constituents of: animal skin gelatin, gelatin, a sheep embryo enzyme hydrolysate, edible sugar, yellow wine and edible vegetable oil, wherein the weight ratio of the animal skin gelatin to the gelatin to the sheep embryo enzyme hydrolysate is (8-12):(2-6):1, the content of amino acid nitrogen in the sheep embryo enzyme hydrolysate is (2-20)g/100ml, and the intrinsic viscosity Eta of the animal skin gelatin is (10-6)dL/g. The obtained health food contains abundant amino acids and some elements which facilitate the absorption by the body and are good for human health, can be used for regulating the body balance better, improving the circulation and preventing the arteriosclerosis, has a high effect of beauty and curative effects on a coronary heart disease and an ischemic brain disease, and also is suitable for critically ill patients such as a diabetic patient, a kidney patient and the like to take a high-quality high-protein health food.
Description
Technical field
The present invention relates to a kind of health-care nutritional food, particularly, relate to a kind of sheep embryo glue and preparation method thereof.
Background technology
Along with people's living standard and the improving constantly of health perception, wish that daily diet can be cooked adjusting to body, improve health, play simultaneously the effect of preventing/treating disease.Wherein sheep placenta class health products enjoy people's welcome, and sheep embryo and placenta are referred to as sheep placenta.Placenta has enriching yin and supports the effect that kidney, production of sperm are enriched blood, and is usually used in women's puerperal asthenia, excessive blood loss.Also often be used for tonic by people.Containing rich in amino acid, polypeptide and other bioactive ingredients in existing embryo of studies show that and the placental protein enzyme hydrolyzate, can strengthen human body immune function significantly, is one of main component in current such health care tonic.
The sheep placenta class health products that provide in prior art, main employing technology is tissue homogenate, vacuum drying and lixiviate etc., though can effectively keep its biologically active, but molecular weight is all bigger, and active peptide and amino acid content are very little, are unfavorable for absorption by human body, simultaneously because composition is single, regulating effect to body is limited, Given this, and special proposition the present invention.
Summary of the invention
A goal of the invention of the present invention is, a kind of sheep embryo glue food is provided, this food can better be regulated organism balance, have and improve circulation, prevention of arterial sclerosis, effective in cure, also be fit to patients with severe symptoms such as diabetes, kidney sufferer and absorb high-quality high-protein health food coronary heart disease, ischemic cerebral disease.
Another object of the present invention provides a kind of preparation method of sheep embryo glue food.
For realizing first purpose of the present invention, a kind of sheep embryo glue food is provided, comprise following component: animal skin glue, gelatin, sheep embryo enzyme hydrolyzate, table sugar, yellow rice wine and edible vegetable oil, wherein the weight ratio of animal skin glue, gelatin and sheep embryo enzyme hydrolyzate is 8-12: 2-6: 1, it is 220g/100ml that sheep embryo hydrolyzate contains amino-acid nitrogen, and the intrinsic viscosity η of animal skin glue is 10-6dL/g.
Animal skin glue of the present invention comprises one or more mixtures in sheepskin glue, pig skin gelatin, the animal glue, its preferred sheepskin glue.
Table sugar of the present invention comprises white granulated sugar, rock sugar etc., its preferred rock sugar.
Edible vegetable oil of the present invention comprises one or more mixture of peanut oil, soybean oil, Semen Benincasae oil, corn oil, its preferred soybean oil.
Sheep embryo of the present invention comprises sheep placenta dish or tire sheep.
Also comprise the sheep muscle in the sheep embryo glue glue food of the present invention.
The weight ratio of animal skin glue of the present invention, gelatin and sheep embryo enzyme hydrolyzate is 9.5-11: 3-4.5: 1
Described sheep embryo glue food is by following method preparation: animal skin glue, gelatin, sheep embryo enzyme hydrolyzate are mixed obtain glue A, under normal pressure, heat glue A with slow fire, it is concentrated, till not oozing paper, promptly obtain glue liquid B, and then adding table sugar, yellow rice wine and edible vegetable oil carry out seasoning.
Described seasoning is for adding table sugar, yellow rice wine and edible vegetable oil in glue liquid B, heating is stirred to oil bloom and disappears, and glue is old lip shape.
Old lip shape of the present invention is meant when provoking glue and then adheres to the state of glue when falling in the form of sheets and not on the rod.
The consumption of described yellow rice wine is the 0.01-5% of glue liquid B weight, and the consumption of its preferred yellow rice wine is 0.1～1.0% of a glue liquid B weight.
The consumption of described edible vegetable oil is the 0.1-5.0% of glue liquid B weight, and the consumption of its preferred edible vegetable oil is 0.5～3.0% of a glue liquid B weight.
Consumption 5～the 10g of used table sugar.
Described sheep embryo enzyme hydrolyzate is prepared by following method:
(1) fresh sheep embryo is cleaned after, with its homogenate;
(2) add entry among the sheep embryo after homogenate, wherein the weight ratio of sheep blastodisc and water is 1: 0.5-2.0 is under the condition of 0.13-0.16Mpa at pressure afterwards, boiling 0.5-1.5 hour;
(3) after the cooling of the homogenate mixed liquor after the boiling, regulate PH to 4.0～9.0 of mixed liquor, add hydrolysising protease, the weight ratio of described hydrolase protein and sheep placenta dish is 0.01～0.2: 1, after stirring evenly, be that hydrolysis was carried out 2～8 hours under 20～45 ℃ the condition in temperature;
(4) above-mentioned enzymolysis liquid is heated 10-15min at 90-100 ℃;
(5) centrifugal in centrifuge through step (4) enzymolysis liquor, get supernatant, promptly obtain sheep embryo hydrolyzate.
It is 2-20g/100ml that the sheep embryo hydrolyzate of gained contains amino-acid nitrogen.
The rotating speed of described centrifugation is 4000-6000r/min.
Adopt zymolysis technique to extract the sheep placental hormone, enzyme is produced by the organism living cells, with the special biocatalyst of a class that protein form exists, can participate in and promote various chemistry, biochemical reaction in the active somatic cell.Enzyme has high activity and height selectivity, can carry out catalytic reaction efficiently, thereby come into one's own and be used widely under the acid-base condition of normal temperature, normal pressure and gentleness.Sheep embryo raw material of the present invention is through cleaning, pull an oar, add the heating of water high pressure, enzyme-added enzymolysis, the enzyme that goes out, its hydrolyzate of centrifuging and taking.The sheep embryo generates polypeptide and amino acid whose mixed liquor through the incomplete hydrolysis of protease, and its digestibility improves greatly, and value improves.Special efficacy is arranged.
The preparation method of described animal skin glue is as follows:
(1) animal skin is cleaned after, put into temperature and be 70-100 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth;
(2) the little fourth of animal skin is handled 10～60min in the micro-wave vacuum device, and its temperature is controlled at 30～70 ℃;
(3) boiling under normal pressure after the little fourth of animal skin that step (2) is handled adds water was received a glue every 3-4 hour, till glue is exhausted;
(4) glue that obtains of step (3) promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 10-6dL/g.
When in step (2) the little fourth of animal skin being carried out micro-wave vacuum, pressure is under the normal pressure, and microwave power is 90-120W/kg.
Preferred 5cm * the 5cm of the size of described little fourth.
Preferably whole intact animal skin of animal skin described in the described step (1).
The preferred sheepskin of described animal skin.
In step (3) after getting glue, remaining residue obtains animal skin glue through the enzyme hydrolysis process, its enzyme hydrolysis process comprises: adding water to sludge concentration is 10-20%, and regulating PH is 4.0～9.0, under 20～45 ℃ of conditions of temperature, add trypsase 1000～6000U/g, behind reaction 0.5～3h, add flavor protease 100～1000U/g again, reaction 1～8h, the enzyme that goes out is got its clear liquid
In the animal skin glue of the present invention, collagen is rich in 18 seed amino acids except that tryptophan and cysteine, and wherein keeping the necessary amino acid of people's bulk-growth has 7 kinds.Glycine in the collagen accounts for 30%, proline and hydroxyproline account for about 25% altogether, be that content is the highest in the range protein, the content of alanine, glutamic acid is also than higher, also contains hydroxyproline rare in general albumen and pyroglutamic acid simultaneously and at the almost non-existent oxylysine of other protein.Animal skin infusion again after vacuum microwave is handled, the glue juice that infusion goes out belongs to the hydrolysate of collagen, is easier to absorption of human body.
Because collagen has multiple action to body, collagen can reduce blood triglyceride and cholesterol; Can increase the essential trace element of some shortage in the body, thereby it is maintained within the normal relatively scope; Be a kind of desirable reducing weight and blood fat food; Collagen can also assist body to discharge aluminium matter, and reducing aluminium matter gathering aspect in vivo also has effect unique; Collagen has and quickens hemoglobin and erythropoietic effect, and it has the circulation of improvement, prevention of arterial sclerosis, effective in cure to coronary heart disease, ischemic cerebral disease; And cancer cell is a kind of foreign matter for life entity, and collagen can encase cancer cell, prevents its increment or transfer.Be fit to patients with severe symptoms such as diabetes, kidney sufferer and absorb high-quality high-protein health food.
Be real another object of the present invention, a kind of preparation method of sheep placenta dish glue health food is provided, comprise the steps:
(1) with animal skin glue, gelatin and sheep embryo enzyme hydrolyzate by weight for 8-12: 2-6: 1 mixes and obtains glue A;
(2) under normal pressure, heat glue A, it is concentrated, till not oozing paper, promptly obtain glue liquid B with slow fire;
(3) adding table sugar, yellow rice wine and edible vegetable oil in glue liquid B, is that 70～90 ℃ of heating are stirred to the oil bloom disappearance in temperature, and glue is old lip shape;
(4) glue after step (3) is handled is poured in the groove of smearing with soybean oil, condenses into piece under 0-10 ℃ of temperature;
(5) step (4) obtain condensing into the glue of piece in temperature be under 20-45 ℃ the condition cold air drying to moisture less than 15%, promptly get sheep embryo glue.
The sheep placental hormone sheep embryo glue that the present invention adopts that the low-temperature cold wind machine is air-dry after condensing, air-dry with the low-temperature cold wind machine, can prevent that colloid from melting, and accelerates air-dry speed, and be not subjected to Effect of Environmental such as weather, humidity.With air-dry comparing under the normal temperature, production efficiency is arranged more.
Wherein said sheep embryo enzyme hydrolyzate is prepared by following method:
(1) fresh sheep embryo is cleaned after, with its homogenate;
(2) add entry among the sheep embryo after homogenate, wherein the weight ratio of sheep embryo and water is 1: 0.5-2.0 is under the condition of 0.13-0.16mPa at pressure afterwards, boiling 0.5-1.5 hour;
(3) after the cooling of the homogenate mixed liquor after the boiling, regulate PH to 4.0～9.0 of mixed liquor, add hydrolysising protease, described hydrolase protein and sheep embryo's weight ratio is 0.01～0.2: 1, after stirring evenly, be that hydrolysis was carried out 2～8 hours under 20～45 ℃ the condition in temperature;
(4) above-mentioned enzymolysis liquid is heated 10-15min at 90-100 ℃;
(5) centrifugal in centrifuge through step (4) enzymolysis liquor, get supernatant, promptly obtain sheep embryo enzyme hydrolyzate.
Described animal skin glue is prepared by following method:
(1) animal skin is cleaned after, put into temperature and be 70-100 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth;
(2) the little fourth of animal skin is handled 10～60min in the micro-wave vacuum device, and its temperature is controlled at 30～70 ℃;
(3) boiling under normal pressure after the little fourth of animal skin that step (2) is handled adds water was received a glue every 3-4 hour, till glue is exhausted;
(4) glue that obtains of step (3) promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 10-6dL/g.
When wherein in step (2) the little fourth of animal skin being carried out micro-wave vacuum, its microwave power is 90-120W/kg, and pressure is normal pressure.
Preferred 5cm * the 5cm of the size of described little fourth.
In the preparation process of sheep embryo glue health products of the present invention, animal skin glue be earlier through vacuum microwave drying, and then glue is got in boiling, in the vacuum microwave processing procedure, the macromolecular substances that the human body that contains in the animal skin is difficult for absorbing is decomposed into each seed amino acid of being convenient to absorption of human body at short notice, its content is very high, and human body is had special efficacy.
Described animal skin glue is preferably by following method preparation:
(1) animal skin is cleaned after, put into temperature and be 70-100 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth;
(2) the little fourth of animal skin is handled 10～60min in the micro-wave vacuum device, and its temperature is controlled at 30～70 ℃;
(3) boiling under normal pressure after the little fourth of animal skin that step (2) is handled adds water was received a glue every 3-4 hour, till glue is exhausted;
(4) in step (3) after getting glue, remaining residue obtains animal skin glue through the enzyme hydrolysis process, and its enzyme hydrolysis process comprises: adding water to sludge concentration is 10-20%, and regulating PH is 4.0～9.0, under 20～45 ℃ of conditions of temperature, add trypsase 1000～6000U/g, behind reaction 0.5～3h, add flavor protease 100～1000U/g again, reaction 1～8h, the enzyme that goes out is got its clear liquid, promptly gets glue;
(5) glue that combining step (3), (4) are obtained promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 10-6dL/g.
In the preparation process of above-mentioned animal skin glue, can fully the beneficiating ingredient in the animal skin be extracted, improved its value.
In the preparation process of sheep embryo glue health food, sheep placenta generates polypeptide and amino acid whose mixed liquor through the incomplete hydrolysis of protease, and its digestibility improves greatly, and value improves.After handling through vacuum microwave, again it is carried out infusion in the preparation process of animal skin glue, microwave has certain decomposition for collagen in the microwave drying process, makes the easy stripping of collagen, decomposes, and has shortened the time of enduring glue greatly.
Compared with prior art, sheep embryo glue health food of the present invention's preparation and preparation method thereof advantage is as follows:
In the sheep embryo glue health food provided by the invention owing to contain rich in amino acid kind and content thereof, and some are convenient to absorption of human body and the composition favourable to health, this food can better be regulated organism balance, has very high cosmetic result, have and improve circulation, prevention of arterial sclerosis, effective in cure, also be fit to patients with severe symptoms such as diabetes, kidney sufferer and absorb high-quality high-protein health food coronary heart disease, ischemic cerebral disease.
" big fire heating, moderate heat accelerates the ripening, the slow fire infusion " is that high temperature makes the structural deterioration in the raw material with the traditional handicraft principle of nearly one thousand years, and material such as nutritional labeling is discharged, and is dissolved in the water." Baoshang " that it has often been said also is the principle of utilization infusion.The present invention prepares that the used time ratio of sheep embryo glue is shorter, and the time of its whole process need high temperature is shorter, can not destroy nutrient composition in raw materials, is convenient to control, and is fit to technology production.
In preparation process, technologies such as desmoenzyme hydrolysis and microwave drying make as much as possible the extracting of various compositions that is beneficial to absorption of human body and health is helped in raw material sheep embryo or the animal skin, and have promptly improved utilization ratio of raw materials.
In addition, the production efficiency of whole process of preparation compared with prior art improves greatly.
The specific embodiment
Embodiment 1
The preparation of sheep placenta dish enzyme hydrolyzate
With fresh weight is after 1kg sheep placenta dish is cleaned, and with its homogenate, adds the water of 1.0kg in the sheep placenta dish after homogenate, is under the condition of 0.15mPa at pressure afterwards, boiling 1 hour; After the homogenate mixed liquor cooling, regulating the PH to 6.0 of mixed liquor, add the 0.1kg hydrolysising protease, after stirring evenly, is that hydrolysis was carried out 5 hours under 30 ℃ the condition in temperature; Above-mentioned enzymolysis liquid is heated 10min at 90 ℃; Centrifugal in centrifuge then, get clear liquid, promptly obtain containing the sheep placenta dish hydrolyzate that amino-acid nitrogen is 10g/100ml;
The preparation of sheepskin glue:
After sheepskin cleaned, put into temperature and be 80 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth; The little fourth of animal skin under the condition of microwave power 100W/kg, is handled 30min in the micro-wave vacuum device under normal pressure, its temperature is controlled at 50 ℃; Add boiling under normal pressure behind the water afterwards, received a glue every 3-4 hour, till glue is exhausted; The glue that obtains promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 7.5dL/g;
The preparation of sheep placenta dish glue health food:
Getting 10kg sheepskin glue, 4kg gelatin and 1kg sheep placenta dish enzyme hydrolyzate mixes and obtains glue A; Under normal pressure,, it is concentrated, till not oozing paper, promptly obtain glue liquid B with slow fire heating glue A; Adding the yellow rice wine of white granulated sugar, 2.0% glue liquid B weight and the soybean oil of 2% glue liquid B weight in glue liquid B, is that 80 ℃ of heating are stirred to the oil bloom disappearance in temperature, and glue is old lip shape; Be poured into afterwards in the groove of smearing with soybean oil, under 5 ℃ of temperature, condense into piece; Be that cold air drying promptly gets sheep placenta dish glue health food to moisture 10% under 30 ℃ the condition in temperature.
Embodiment 2
The preparation of sheep placenta dish enzyme hydrolyzate
With fresh weight is after 1kg sheep placenta dish is cleaned, and with its homogenate, adds the water of 2.0kg in the sheep placenta dish after homogenate, is under the condition of 0.13mPa at pressure afterwards, boiling 1.5 hours; After the homogenate mixed liquor cooling, regulating the PH to 4.0 of mixed liquor, add the 0.01kg hydrolysising protease, after stirring evenly, is that hydrolysis was carried out 8 hours under 45 ℃ the condition in temperature; Above-mentioned enzymolysis liquid is heated 10min at 100 ℃; Centrifugal in centrifuge then, get clear liquid, promptly obtain containing the sheep placenta dish hydrolyzate that amino-acid nitrogen is 5g/100ml;
The preparation of sheepskin glue:
After sheepskin cleaned, put into temperature and be 70 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth; The little fourth of animal skin under the condition of microwave power 110W/kg, is handled 60min in the micro-wave vacuum device under normal pressure, its temperature is controlled at 30 ℃; Add boiling under normal pressure behind the water afterwards, received a glue every 4 hours, till glue is exhausted; The glue that obtains promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 8dL/g;
The preparation of sheep placenta dish glue health food:
Getting 12kg sheepskin glue, 3kg gelatin and 1kg sheep placenta dish enzyme hydrolyzate mixes and obtains glue A; Under normal pressure,, it is concentrated, till not oozing paper, promptly obtain glue liquid B with slow fire heating glue A; Adding the yellow rice wine of white granulated sugar, 5.0% glue liquid B weight and the corn oil of 0.01% glue liquid B weight in glue liquid B, is that 90 ℃ of heating are stirred to the oil bloom disappearance in temperature, and glue is old lip shape; Be poured into afterwards in the groove of smearing with soybean oil, under 0 ℃ of temperature, condense into piece; Be that cold air drying promptly gets sheep placenta dish glue health food to moisture 13% under 20 ℃ the condition in temperature.
Embodiment 3
The preparation of sheep placenta dish enzyme hydrolyzate
With fresh weight is after 1kg sheep placenta dish is cleaned, and with its homogenate, adds the water of 0.5kg in the sheep placenta dish after homogenate, is under the condition of 0.16mPa at pressure afterwards, boiling 0.5 hour; After the homogenate mixed liquor cooling, regulating the PH to 9.0 of mixed liquor, add the 0.2kg hydrolysising protease, after stirring evenly, is that hydrolysis was carried out 2 hours under 20 ℃ the condition in temperature; Above-mentioned enzymolysis liquid is heated 15min at 90 ℃; Centrifugal in centrifuge then, get clear liquid, promptly obtain containing the sheep placenta dish hydrolyzate that amino-acid nitrogen is 18g/100ml;
The preparation of sheepskin glue:
After sheepskin cleaned, put into temperature and be 100 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth; The little fourth of animal skin under the condition of microwave power 90W/kg, is handled 10min in the micro-wave vacuum device under normal pressure, its temperature is controlled at 30 ℃; Add boiling under normal pressure behind the water afterwards, received a glue every 3-4 hour, till glue is exhausted; The glue that obtains promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 9dL/g;
The preparation of sheep placenta dish glue health food:
Getting 8kg animal skin glue, 6kg gelatin and 1kg sheep placenta dish enzyme hydrolyzate mixes and obtains glue A; Under normal pressure,, it is concentrated, till not oozing paper, promptly obtain glue liquid B with slow fire heating glue A; Adding the yellow rice wine of rock sugar, 0.1% glue liquid B weight and the Semen Benincasae oil of 5% glue liquid B weight in glue liquid B, is that 70 ℃ of heating are stirred to the oil bloom disappearance in temperature, and glue is old lip shape; Be poured into afterwards in the groove of smearing with soybean oil, under 0 ℃ of temperature, condense into piece; Be that cold air drying promptly gets sheep placenta dish glue health food to moisture 9% under 45 ℃ the condition in temperature.
Embodiment 4
The preparation of tire sheep enzyme hydrolyzate
With fresh weight is after 1kg tire sheep is cleaned, and with its homogenate, adds the water of 1.5kg in the tire sheep after homogenate, is under the condition of 0.15mPa at pressure afterwards, boiling 1 hour; After the homogenate mixed liquor cooling, regulating the PH to 7.0 of mixed liquor, add the 0.05kg hydrolysising protease, after stirring evenly, is that hydrolysis was carried out 6 hours under 40 ℃ the condition in temperature; Above-mentioned enzymolysis liquid is heated 10min at 90 ℃; Centrifugal in centrifuge then, get clear liquid, promptly obtain containing the tire sheep hydrolyzate that amino-acid nitrogen is 8g/100ml;
The preparation of animal skin glue:
After ox-hide and sheepskin cleaned, put into temperature and be 80 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth; The little fourth of animal skin under the condition of microwave power 120W/kg, is handled 40min in the micro-wave vacuum device under normal pressure, its temperature is controlled at 40 ℃; Add boiling under normal pressure behind the water afterwards, received a glue every 3-4 hour, till glue is exhausted; The glue that obtains promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 6dL/g;
The preparation of sheep placenta dish glue health food:
Getting 8kg animal skin glue, 5kg gelatin and 1kg sheep placenta dish enzyme hydrolyzate mixes and obtains glue A; Under normal pressure,, it is concentrated, till not oozing paper, promptly obtain glue liquid B with slow fire heating glue A; The yellow rice wine and the peanut oil of 0.03% glue liquid B weight and the mixing of soybean oil that add white granulated sugar, 1.0% glue liquid B weight in glue liquid B are that 90 ℃ of heating are stirred to the oil bloom disappearance in temperature, and glue is old lip shape; Be poured into afterwards in the groove of smearing with soybean oil, under 0 ℃ of temperature, condense into piece; In temperature be under 20 ℃ the condition cold air drying to moisture less than 12%, promptly get sheep placenta dish glue health food.
Embodiment 5
The preparation of sheep placenta dish enzyme hydrolyzate
With fresh weight is after 1kg sheep placenta dish is cleaned, and with its homogenate, adds the water of 0.8kg in the sheep placenta dish after homogenate, is under the condition of 0.15mPa at pressure afterwards, boiling 1.5 hours; After the homogenate mixed liquor cooling, regulating the PH to 6.0 of mixed liquor, add the 0.15kg hydrolysising protease, after stirring evenly, is that hydrolysis was carried out 7 hours under 45 ℃ the condition in temperature; Above-mentioned enzymolysis liquid is heated 10min at 90 ℃; Centrifugal in centrifuge then, get clear liquid, promptly obtain containing the sheep placenta dish hydrolyzate that amino-acid nitrogen is 6g/100ml;
The preparation of animal skin glue:
After pigskin and sheepskin cleaned, put into temperature and be 90 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth; The little fourth of animal skin under the condition of microwave power 105W/kg, is handled 10min in the micro-wave vacuum device under normal pressure, its temperature is controlled at 70 ℃; Add boiling under normal pressure behind the water afterwards, received a glue every 3-4 hour, till glue is exhausted; It is 12% that residue after getting glue adds water to concentration of substrate, transferring PH is 6.0, under 30 ℃ of temperature, add trypsase 5000U/g, reaction 2.5 backs add flavor protease 500U/g, react 4h again, enzyme goes out, get its clear liquid, mix the glue that obtains and promptly get animal skin liquid after filtration, the intrinsic viscosity η of gained animal skin glue is 7dL/g;
The preparation of sheep placenta dish glue health food:
Getting 10kg animal skin glue, 4kg gelatin and 1kg sheep placenta dish enzyme hydrolyzate mixes and obtains glue A; Under normal pressure,, it is concentrated, till not oozing paper, promptly obtain glue liquid B with slow fire heating glue A; Adding the yellow rice wine of white granulated sugar, 2.0% glue liquid B weight and the soybean oil of 0.5% glue liquid B weight in glue liquid B, is that 80 ℃ of heating are stirred to the oil bloom disappearance in temperature, and glue is old lip shape; Be poured into afterwards in the groove of smearing with soybean oil, under 10 ℃ of temperature, condense into piece; Be that cold air drying promptly gets sheep placenta dish glue health food to moisture 8.6% under 40 ℃ the condition in temperature.
Experimental example 1
This experimental example is the effect of sheep embryo glue health food of the present invention aspect beauty treatment, is specially the chloasma-dispelling function test:
One, adopts two kinds of control design between self and group.Chloasma color, area situation by the experimenter are divided into test-meal group and control group at random.Every group of experimenter's 60 examples.
Two, the dosage of given the test agent and using method
Test-meal group edible 10 sheep embryo glue every day, control group adopts blank.Given the test agent gives 30 days time.The experimenter stops using other articles for use oral and the relevant face-beautifying and spot-removing of external application at duration of test.Duration of test does not change original eating habit, normal diet.
Three, effect index
1, facial area chloasma area size detection: the area (mm that is tried the whole facial area chloasma in front and back with tape measure
2).
2, facial area chloasma shade detects: " standard color card " judges I degree, II degree, III degree.
Four, data are handled and result's judgement
Chloasma color integration before and after the test-meal and area change are added up, calculated efficient simultaneously.Colour atla I degree, II degree, III degree were counted respectively 1 minute, 2 minutes and 3 minutes.
Effect criterion
Effectively: chloasma color decline I degree, area reduces greater than 10%, and does not produce new chloasma.
Invalid: chloasma color and area do not have significant change
Five experimental results
60 routine chloasma persons behind test-meal sheep embryo glue, according to effect criterion, 35 routine produce effects (58%), 17 examples are (28%) effectively, total effective rate 86%.
Chloasma shade, area size variation before and after edible
| Project | The example number | Before being tried | After being tried | Difference |
| Colourity | 60 | 2.3±0.32 | 1.4±0.64 | 0.9±0.53 |
| Chloasma area (mm 2) | 60 | 73.3±49.6 | 39.5±29.1 | 33.8±26.4 |
This test-meal description of test, sheep embryo glue has positive effect for improving eliminating chloasma.
Claims (10)
1. sheep embryo glue health food, comprise following component: animal skin glue, gelatin, sheep embryo enzyme hydrolyzate, table sugar, yellow rice wine and edible vegetable oil, wherein the weight ratio of animal skin glue, gelatin and sheep embryo enzyme hydrolyzate is 8-12: 2-6: 1, it is 2g-20g/100ml that sheep embryo enzyme hydrolyzate contains amino-acid nitrogen, and the intrinsic viscosity η of animal skin glue is 10-6dL/g.
2. sheep embryo glue health food according to claim 1 is characterized in that the weight ratio of described animal skin glue, gelatin and sheep embryo enzyme hydrolyzate is 9.5-11: 3-4.5: 1.
3. sheep embryo glue health food according to claim 1, it is characterized in that, described sheep placenta dish glue food is by following method preparation: animal skin glue, gelatin, sheep embryo enzyme hydrolyzate are mixed obtain glue A, under normal pressure, heat glue A with slow fire, it is concentrated, till not oozing paper, promptly obtain glue liquid B, and then adding table sugar, yellow rice wine and edible vegetable oil carry out seasoning.
4. sheep embryo glue health food according to claim 1 is characterized in that, described sheep embryo enzyme hydrolyzate is prepared by following method:
(1) fresh sheep embryo is cleaned after, with its homogenate;
(2) add entry among the sheep embryo after homogenate, wherein the weight ratio of sheep blastodisc and water is 1: 0.5-2.0 is under the condition of 0.13-0.16Mpa at pressure afterwards, boiling 0.5-1.5 hour;
(3) after the cooling of the homogenate mixed liquor after the boiling, regulate PH to 4.0～9.0 of mixed liquor, add hydrolysising protease, the weight ratio of described hydrolase protein and sheep placenta dish is 0.01～0.2: 1, after stirring evenly, be that hydrolysis was carried out 2～8 hours under 20～45 ℃ the condition in temperature;
(4) above-mentioned enzymolysis liquid is heated 10-15min at 90-100 ℃;
(5) centrifugal in centrifuge through step (4) enzymolysis liquor, get supernatant, promptly obtain sheep embryo hydrolyzate.
5. sheep embryo glue health food according to claim 1 is characterized in that the preparation method of described animal skin glue is as follows:
(1) animal skin is cleaned after, put into temperature and be 70-100 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth
(2) the little fourth of animal skin is handled 10～60min in the micro-wave vacuum device, and its temperature is controlled at 30～70 ℃;
(3) boiling under normal pressure after the little fourth of animal skin that step (2) is handled adds water was received a glue every 3-4 hour, till glue is exhausted;
(4) glue that obtains of step (3) promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 10-6dL/g.
6. sheep embryo glue health food according to claim 1 is characterized in that when the micro-wave vacuum device was handled, pressure was under the normal pressure, and microwave power is 90-120W/kg.
7. according to each described sheep placenta dish glue food of claim 1-5, it is characterized in that described animal skin glue comprises one or more mixtures in sheepskin glue, pig skin gelatin, the animal glue, its preferred sheepskin glue; Described table sugar comprises white granulated sugar, rock sugar etc., its preferred rock sugar; Described edible vegetable oil comprises one or more mixture of peanut oil, soybean oil, Semen Benincasae oil, corn oil, its preferred soybean oil; The consumption of wherein said yellow rice wine is the 0.01-5% of glue liquid B weight, and the consumption of its preferred yellow rice wine is 0.1～1.0% of a glue liquid B weight; The consumption of described edible vegetable oil is the 0.1-5.0% of glue liquid B weight, and the consumption of its preferred edible vegetable oil is 0.5～3.0% of a glue liquid B weight.
8. the preparation method of a sheep placenta dish glue food comprises the steps:
(1) with animal skin glue, gelatin and sheep embryo enzyme hydrolyzate by weight for 8-12: 2-6: 1 mixes and obtains glue A;
(2) under normal pressure, heat glue A, it is concentrated, till not oozing paper, promptly obtain glue liquid B with slow fire;
(3) adding table sugar, yellow rice wine and edible vegetable oil in glue liquid B, is that 70～90 ℃ of heating are stirred to the oil bloom disappearance in temperature, and glue is old lip shape;
(4) glue after step (3) is handled is poured in the groove of smearing with soybean oil, condenses into piece under 0-10 ℃ of temperature;
(5) step (4) obtain condensing into the glue of piece in temperature be under 20-45 ℃ the condition cold air drying to moisture less than 15% animal skin glue.
9. preparation method according to claim 8 is characterized in that,
Described sheep embryo enzyme hydrolyzate is prepared by following method:
(1) fresh sheep placenta dish is cleaned after, with its homogenate;
(2) add entry in the sheep placenta dish after homogenate, wherein the weight ratio of sheep placenta dish and water is 1: 0.5-2.0, and afterwards under the condition of pressure 0-0.15mPa, boiling 0.5-1.5 hour;
(3) after the cooling of the homogenate mixed liquor after the boiling, regulate PH to 4.0～9.0 of mixed liquor, add hydrolysising protease, the weight ratio of described hydrolase protein and sheep placenta dish is 0.01～0.2: 1, after stirring evenly, be that hydrolysis was carried out 2～8 hours under 20～45 ℃ the condition in temperature;
(4) above-mentioned enzymolysis liquid is heated 10-15min at 90-100 ℃;
(5) centrifugal in centrifuge through step (4) enzymolysis liquor, get clear liquid, promptly obtain sheep placenta dish hydrolyzate;
Described animal skin glue is prepared by following method:
(1) animal skin is cleaned after, put into temperature and be 70-100 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth;
(2) the little fourth of animal skin is handled 10～60min in the micro-wave vacuum device, and its temperature is controlled at 30～70 ℃;
(3) boiling under normal pressure after the little fourth of animal skin that step (2) is handled adds water was received a glue every 3-4 hour, till glue is exhausted;
(4) glue that obtains of step (3) promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 10-6dL/g.
10. according to Claim 8 or 9 described preparation methods, it is characterized in that described animal skin glue is prepared by following method:
(1) animal skin is cleaned after, put into temperature and be 70-100 ℃ water, treat to pull out after the skin thermal denaturation, be cut into little fourth;
(2) the little fourth of animal skin is handled 10～60min in the micro-wave vacuum device, and its temperature is controlled at 30～70 ℃;
(3) boiling under normal pressure after the little fourth of animal skin that step (2) is handled adds water was received a glue every 3-4 hour, till glue is exhausted;
(4) in step (3) after getting glue, remaining residue obtains animal skin glue through the enzyme hydrolysis process, and its enzyme hydrolysis process comprises: adding water to sludge concentration is 10-20%, and regulating PH is 4.0～9.0, under 20～45 ℃ of conditions of temperature, add trypsase 1000～6000U/g, behind reaction 0.5～3h, add flavor protease 100～1000U/g again, reaction 1～8h, the enzyme that goes out is got its clear liquid, promptly gets glue;
(5) glue that combining step (3), (4) are obtained promptly gets animal skin liquid after filtration, and the intrinsic viscosity η of gained animal skin glue is 10-6dL/g.
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| CN105343128A (en) * | 2015-11-19 | 2016-02-24 | 界首市菁华科技信息咨询服务有限公司 | Processing method of sheep placenta instant powder |
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| CN1099274A (en) * | 1993-08-27 | 1995-03-01 | 龙惠民 | Ginseng placenta product |
| CN1110128A (en) * | 1994-04-14 | 1995-10-18 | 浙江康恩贝集团研究开发中心 | Method for preparation of active placenta powder |
| CN1283506A (en) * | 2000-06-20 | 2001-02-14 | 苏州朗力福保健品有限公司 | Health-care composition and its preparing process |
| CN1465368A (en) * | 2002-07-01 | 2004-01-07 | 邓先明 | Black boned chicken active capsule and preparation process thereof |
| CN101023993A (en) * | 2007-03-08 | 2007-08-29 | 吉林省东丰药业股份有限公司 | Chloasma diminishing medicine containing deer foetus and functional food and preparing method |
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2009
- 2009-12-01 CN CN2009103106952A patent/CN102077992B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099274A (en) * | 1993-08-27 | 1995-03-01 | 龙惠民 | Ginseng placenta product |
| CN1110128A (en) * | 1994-04-14 | 1995-10-18 | 浙江康恩贝集团研究开发中心 | Method for preparation of active placenta powder |
| CN1283506A (en) * | 2000-06-20 | 2001-02-14 | 苏州朗力福保健品有限公司 | Health-care composition and its preparing process |
| CN1465368A (en) * | 2002-07-01 | 2004-01-07 | 邓先明 | Black boned chicken active capsule and preparation process thereof |
| CN101023993A (en) * | 2007-03-08 | 2007-08-29 | 吉林省东丰药业股份有限公司 | Chloasma diminishing medicine containing deer foetus and functional food and preparing method |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105343128A (en) * | 2015-11-19 | 2016-02-24 | 界首市菁华科技信息咨询服务有限公司 | Processing method of sheep placenta instant powder |
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