CN106072668A - Health product of eliminating toxin and beautifying the skin and preparation method thereof - Google Patents
Health product of eliminating toxin and beautifying the skin and preparation method thereof Download PDFInfo
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- 235000019710 soybean protein Nutrition 0.000 claims abstract description 66
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- 235000001206 Amorphophallus rivieri Nutrition 0.000 claims abstract description 16
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- 235000010485 konjac Nutrition 0.000 claims abstract description 16
- 239000000252 konjac Substances 0.000 claims abstract description 16
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to health product of a kind of eliminating toxin and beautifying the skin and preparation method thereof, be made up through techniques such as enzymolysis, ultrafiltration, boiling and mixing of raw materials such as Caulis et Folium Tritici aestivi extract, konjac oligosaccharides, Herba Apii graveolentis, nattokinase, micromolecular collagen peptide and soybean protein powders.The health product that the invention have the benefit that the eliminating toxin and beautifying the skin of the present invention are that by enzymatic isolation method, soybean protein powder is converted it into low molecule soybean protein peptide, in addition the health product of the eliminating toxin and beautifying the skin that other raw materials such as nattokinase, chitin oligosaccharide, micromolecular collagen peptide are made have raising body immunity, regulate body metabolism, improve blood circulation, improve effect of skin problem, eliminating toxin and beautifying the skin.
Description
Technical field
The invention belongs to field of pharmaceutical technology, be specifically related to health product of a kind of eliminating toxin and beautifying the skin and preparation method thereof.
Background technology
Along with environmental pollution is day by day serious, rhythm of life accelerates, and pressure is excessive, and present people's quantity of motion is but constantly subtracting
Few, overfatigue so that body metabolism function gradually fails, the reasons such as intestinal peristalsis promoting reduces, contraction of abdominal muscle power minimizing, easily go out
The raw skin ulcer of existing mouth heat, facial colour spot, sallow, the symptoms such as defecation is the most smooth, it is exactly cannot normal toxin expelling that its reason is appointed.People are more and more heavier
Depending on self eliminating toxin and beautifying the skin and healthy.
Soybean protein is referred to as the king of albumen, and the protein of a kind of high nutritive value being well recognized as, it belongs to adequate proteins
Matter, its aminoacid reasonable mixture ratio is close to the demand percentage of human body.But soybean protein has sensitivity, under hot, sour effect
Easily degeneration, dissolubility is decreased obviously so that it is range of application is significantly restrained.Low molecule soybean protein peptide then digestion resistant, resistance to
Hot acid and alkali-resistance, storage endurance stability and the most supplementary protein and raising immunity, its distinctive soybean protein anti-oxidation peptide
The generation of free radical and active oxygen, slow down aging can be removed；Antibacterial peptide then has natural antibacterial and beautification function, than chemistry
Preservative has unique advantage for medicine or cosmetics.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides health product and the system thereof of a kind of eliminating toxin and beautifying the skin
Preparation Method.Its preparation method is simple to operation, and the health product of the eliminating toxin and beautifying the skin prepared have eliminating toxin and beautifying the skin, improve immunity of organisms
Effect.
The technical solution adopted in the present invention is: the health product of a kind of eliminating toxin and beautifying the skin, including the raw material of following weight portion: little
Wheat straw extract 12-18 part, konjac oligosaccharides 13-19 part, yeast rich in selenium 3-5 part, Herba Apii graveolentis 5-15 part, Fructus Perillae 25-35 part, thin
Lotus 20-40 part, Bulbus Lilii 10-15 part, nattokinase 8-13 part, chitin oligosaccharide 5-9 part, soybean protein powder 250-350 part and
Micromolecular collagen peptide 50-100 part.
Further, including the raw material of following weight portion: Caulis et Folium Tritici aestivi extract 15 parts, konjac oligosaccharides 16 parts, selenium-rich ferment
Mother 4 parts, Herba Apii graveolentis 10 parts, Fructus Perillae 30 parts, Herba Menthae 30 parts, Bulbus Lilii 13 parts, nattokinase 10 parts, chitin oligosaccharide 7 parts, Semen sojae atricolor
Egg albumen powder 300 parts and micromolecular collagen peptide 75 parts.
The preparation method of the health product of a kind of described eliminating toxin and beautifying the skin, comprises the following steps:
(1) enzymatic hydrolysis of soybean egg albumen powder: after the water dissolution of soybean protein powder is added its weight 10-15 times, pre-through 85 DEG C
Hot 10min, is then cooled to 55-60 DEG C, and pH is adjusted to 9.0-9.5, adds alkaline protease and carry out enzyme for the first time after insulation 10min
Solving, keep pH and temperature-resistant in described first time enzymolysis process, the time of described first time enzymolysis is 2.5-3.5 hour, so
Rear boiling water bath enzyme denaturing 10-15min；Then, being cooled to 45-50 DEG C, pH is adjusted to 6.5-7.0, adds local flavor after insulation 10-15min
Protease carries out second time enzymolysis, keeps pH and temperature-resistant in described second time enzymolysis process, described second time enzymolysis time
Between be 1.5-2.5 hour, then boiling water bath enzyme denaturing 10-15min；Obtain soybean protein hydrolysate；
(2) ultrafiltration: described soybean protein hydrolysate is cooled to room temperature, regulates the pH of described soybean protein hydrolysate extremely
7.0, centrifuging and taking supernatant, carry out ultrafiltration with ultrafilter membrane, filtrate lyophilization obtains low molecule soybean protein Gly-His-Lys；
(3) boiling: Herba Apii graveolentis, Fructus Perillae, Herba Menthae and Bulbus Lilii being mixed, mix homogeneously makes compound, with described mixed
Described compound is first soaked by the water of close the weight expected 8-10 times, then carries out boiling 2-3 hour, filters, abandon after standing
Going to expect that slag obtains feed liquid, will add konjac oligosaccharides in described feed liquid, mix homogeneously postlyophilization obtains expecting powder；
(4) mixing: carry out mixing for the first time by described low molecule soybean protein Gly-His-Lys and material powder, add little after mix homogeneously
Wheat straw extract, yeast rich in selenium, nattokinase, chitin oligosaccharide and micromolecular collagen peptide carry out second time again and mix,
Mix homogeneously makes the health product of eliminating toxin and beautifying the skin.
Further, described in step (1), for the first time the pH of enzymolysis is 9.3, and the time of described first time enzymolysis is 3 little
Time；The pH of described second time enzymolysis is 6.8, and the time of described second time enzymolysis is 2 hours.
Further, the addition of alkaline protease described in step (1) is the 0.5-of described soybean protein powder weight
0.7wt%；The addition of described flavor protease is the 0.3-0.4wt% of described soybean protein powder weight.
Further, being centrifuged as under conditions of 4 DEG C described in step (2), 8000r/min is centrifuged 10min.
Further, the lyophilization described in step (2) and step (3) is vacuum lyophilization, and described freezing is done
Dry cryogenic temperature is subzero 50 DEG C of subzero 45-；The described cryodesiccated time is 6-8 hour.
Further, the minimum molecular weight that described in step (2), ultrafilter membrane can retain is 0.5 × 104Da。
Further, boiling described in step (3) be first decoct with big fire after use the slow fire infusion, the temperature of described big fire to be
85-93 DEG C, the time of described decoction is 1-1.5 hour；The temperature of described slow fire is 60-70 DEG C, and the time of described infusion is 1-
1.5 hour.
Further, the temperature of described big fire is 90 DEG C, and the time of described decoction is 80 minutes；The temperature of described slow fire
Being 65 DEG C, the time of described infusion is 70 minutes.
Hereinafter, the character etc. of primary raw material used in the present invention is slightly explained:
Caulis et Folium Tritici aestivi is the Semen Tritici aestivi of a kind of uniqueness, is the seedling that grows through the fermentation of earth of the seed of Semen Tritici aestivi, after maturation is
Red Semen Tritici aestivi berry.Containing abundant chlorophyll, vitamin A, vitamin C, vitamin E and vitamin in Caulis et Folium Tritici aestivi extract
B race, and mineral calcium, magnesium, phosphorus, ferrum, selenium, and super antioxidant SOD, fiber and useful ferment.Chlorophyll therein has
Liver heat removing, the effect purified the blood；Mineral can improve constipation and dyspepsia, prevention decayed tooth, allaying tiredness；Super antioxidant SOD
Can be with defying age, anti-oxidation with useful ferment.
Konjac oligosaccharides, is Rhizoma amorphophalli polysaccharide product after enzymolysis.Rhizoma amorphophalli polysaccharide is mainly composed of mannan and Fructus Vitis viniferae
Sugar, it has blood fat reducing, blood sugar lowering, blood pressure lowering, loses weight, improves looks, keeps healthy and the multiple curative effect such as relieving constipation；Konjac oligosaccharides not only has
The above characteristic having Rhizoma amorphophalli polysaccharide can also promote bacillus bifidus to breed and suppress pernicious bacteria to grow, and improves human body intestinal canal function
Effect.
Yeast rich in selenium be during culture yeasts addition selenium element, absorbed selenium during yeast growth, make selenium with
Protein and polysaccharide organic in yeast body combine and are converted into biological selenium, thus eliminate chemistry selenium (such as sodium selenite) to human body
Toxicity and the intestines and stomach stimulate, enable that selenium is more efficient, be more safely absorbed by the body utilization.Yeast rich in selenium is also
Only the most domestic the most efficiently, the selenium-replenishing preparation that equalizes most of the safest, nutrition.Selenium can remove the accumulation of machine heavy metal of body, has releasing
The ability of heavy metal poisoning, is the natural antidote of part heavy metal element；Liver heme catabolism can be affected, and can substantially suppress
By the mitochondrial swelling phenomenon caused by sulfide or sulfur-based compound；Also there is the effect of defying age.
Nattokinase (being called for short NK) is a kind of Proteinkinase, is by natto hay bar in soybean isoflavone by natto strain
A kind of serine protease that bacterium produces.Having thrombolytic effect, nattokinase is the most thrombosed in directly dissolving
Simultaneously, moreover it is possible to activate the thrombolytic ability strengthening human body self；Also there is obvious blood pressure lowering, reduce blood viscosity, suppress platelet
Coagulation, improves blood circulation, softens and increase the effect of blood vessel elasticity.
Micromolecular collagen peptide is the Gly-His-Lys of low-molecular-weight, is easily fully absorbed by human body.The stability of peptide is far superior to
Common collagen molecules, they have more resistant to heat, acid and alkali-resistance, are not easy the advantage of degeneration, and need not move through gastrointestinal tract
Digest and decompose and can be directly absorption of human body, alleviate renal metabolism burden, for you provide more high-quality, be more easy to absorb high-quality egg
In vain.The oligomeric Gly-His-Lys of marine fish can effectively solve the problem that skin and muscle moisture reduce problem, supplements collagen peptide in good time, skin can be made to protect
Hold youth；Make calcareous to combine closely with osteocyte, will not run off or degenerate；Cornea can be made to keep moistening transparent, increase eyes
Transparency；Promote muscle cell tight union so that it is there is elasticity and gloss；Endocrine regulation, protect and strengthen viscera function；
Binding domain-immunoglobulin, increases immunity.
The low molecule soybean protein peptide that soybean protein powder is made after enzymolysis, it is not only digested and assimilated and is better than single ammonia
Base acid, Heat stability is good, and there is multiple body metabolism and the physiological regulation such as the strongest antioxidation, defying age, blood pressure lowering, fat-reducing
Function.
Fructus Perillae: pungent, temperature；Return lung meridian；Sending down the abnormal ascending QI expectorant, relievings asthma, intestine moistening.Stopping up QI rising in reverse order for expectorant, cough and asthma, dryness of the intestine is just
Secret.
Nattokinase and oligopeptide have preferable synergism；Nattokinase, chitin oligosaccharide, micromolecular collagen
Peptide and low molecule soybean protein peptide are used in conjunction with being possible not only to regulate body metabolism, improve blood circulation, improve skin problem and reach
To improving immunity, the effect of looks improving and the skin nourishing；Fructus Perillae, Bulbus Lilii, Herba Menthae and Herba Apii graveolentis etc. play auxiliary toxin expelling and supplementary human body institute
The function of multiple nutrients, all raw materials is needed to share the effect having preferable eliminating toxin and beautifying the skin, improving body immunity.
The present invention uses enzymatic hydrolysis soybean protein powder, successively uses flavor protease and alkaline protease that it is carried out enzyme
Solve, obtain the hydrolyzate of soybean protein with optimal physiologically active, then rely on hyperfiltration technique, obtained that there is eliminating toxin and beautifying the skin effect
Low molecule soybean protein peptide.Enzymatic Hydrolysis Process is easy to control, mild condition, and the response time is short, and efficiency is high, and the product obtained
Product purity is high, with low cost.The aperture of ultrafilter membrane is 0.001-0.02 μm, and the ultrafilter membrane used in the present invention can retain
Small-molecular-weight is 0.5 × 104Da, can be 0.5 × 10 by molecular weight4The small-molecular peptides of below Da and other things in enzymolysis solution
Matter is separated.
The present invention uses in preparation method vacuum lyophilization, also referred to as sublimation drying.Its principle is that material is freezing, makes
Its moisture content contained becomes ice cube, makes ice distillation reach drying purpose the most under vacuo.Vacuum Freezing & Drying Technology be by
Wet stock or solution are frozen into solid-state at a lower temperature, make moisture therein directly distil without liquid the most under vacuo
Become gaseous state, finally make the dry technology of material dewatering.During vacuum lyophilization, there is not Surface hardened layer problem in material,
And it is internally formed the spongy of porous, thus there is the rehydration of excellence, the state before being dried can be recovered at short notice.By
It is to carry out at quite low temperatures in dry run, and has substantially completely cut off air, therefore restrained effectively heat-sensitive substance
There is biology, chemically or physically change, and preferably save the active substance in raw material, and maintain the color and luster of raw material.
The invention have the benefit that the health product of the eliminating toxin and beautifying the skin of the present invention are will by enzymatic isolation method by soybean protein powder
It changes into low molecule soybean protein peptide, in addition other raw materials such as nattokinase, chitin oligosaccharide, micromolecular collagen peptide
The health product of the eliminating toxin and beautifying the skin made have raising body immunity, regulate body metabolism, improve blood circulation, improve skin and ask
Topic, effect of eliminating toxin and beautifying the skin.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further details.
The flavor protease and the alkaline protease that use in the present invention are all purchased from NOVO company.
Embodiment 1
The health product of a kind of eliminating toxin and beautifying the skin, are made up of following raw material:
Caulis et Folium Tritici aestivi extract 12kg, konjac oligosaccharides 19kg, yeast rich in selenium 5kg, Herba Apii graveolentis 5kg, Fructus Perillae 35kg, Herba Menthae
20kg, Bulbus Lilii 15kg, nattokinase 13kg, chitin oligosaccharide 5kg, soybean protein powder 250kg and micromolecular collagen peptide
100kg。
Its preparation method, comprises the following steps:
(1) enzymatic hydrolysis of soybean egg albumen powder: after the water dissolution of 12 times that soybean protein powder adds its weight, through 85 DEG C of preheatings
10min, is then cooled to 58 DEG C, and pH is adjusted to 9.3, the basic protein of the 0.5% of addition soybean protein powder weight after insulation 10min
Enzyme carries out enzymolysis for the first time, and keeping temperature for the first time in enzymolysis process is 58 DEG C, and the pH of enzymolysis is 9.3 for the first time, enzyme for the first time
The time solved is 2.5 hours, then boiling water bath enzyme denaturing 12min；Being cooled to 48 DEG C, pH is adjusted to 6.8, adds big after insulation 12min
The flavor protease of the 0.3% of soybean protein grain weight amount carries out second time enzymolysis, and keeping temperature for the second time in enzymolysis process is 48 DEG C,
The pH of enzymolysis is 8.5 for the second time, and the time of enzymolysis is 2 hours for the second time, and then boiling water bath enzyme denaturing 12min, obtains soybean protein
Zymolyte；
(2) ultrafiltration: soybean protein hydrolysate is cooled to room temperature, adjusts pH to 7.0, under conditions of 4 DEG C, 8000r/min
Centrifugal 10min, takes supernatant, is 1 × 10 with the minimum molecular weight that can retain4The ultrafilter membrane of Da carries out ultrafiltration, lyophilization
Obtaining low molecule soybean protein Gly-His-Lys, cryogenic temperature-48 DEG C, the cryodesiccated time is 7 hours；
(3) boiling: Herba Apii graveolentis, Fructus Perillae, Herba Menthae and Bulbus Lilii are mixed, mix homogeneously makes compound, mix homogeneously
Make compound, with the water of 9 times of the weight of compound, compound is first soaked, then carry out boiling 2.5 hours, after standing
Filtering, discard material slag and obtain feed liquid, will add konjac oligosaccharides in feed liquid, mix homogeneously postlyophilization obtains expecting powder, freezing
Temperature-48 DEG C, the cryodesiccated time is 7 hours；
(4) mixing: carry out mixing for the first time by described low molecule soybean protein Gly-His-Lys and material powder, add little after mix homogeneously
Wheat straw extract, yeast rich in selenium, nattokinase, chitin oligosaccharide and micromolecular collagen peptide carry out second time again and mix,
Mix homogeneously makes the health product of eliminating toxin and beautifying the skin.
Embodiment 2
The health product of a kind of eliminating toxin and beautifying the skin, are made up of following raw material: Caulis et Folium Tritici aestivi extract 18kg, konjac oligosaccharides 13kg,
Yeast rich in selenium 3kg, Herba Apii graveolentis 15kg, Fructus Perillae 25kg, Herba Menthae 40kg, Bulbus Lilii 10kg, nattokinase 8kg, chitin oligosaccharide
9kg, soybean protein powder 350kg and micromolecular collagen peptide 50kg.
Its preparation method, comprises the following steps:
(1) enzymatic hydrolysis of soybean egg albumen powder: after the water dissolution of 10 times that soybean protein powder adds its weight, through 85 DEG C of preheatings
10min, is then cooled to 55 DEG C, and pH is adjusted to 9.5, the basic protein of the 0.7% of addition soybean protein powder weight after insulation 10min
Enzyme carries out enzymolysis for the first time, and the pH of enzymolysis remains 9.5 for the first time, and temperature is 55 DEG C, and the time of enzymolysis is 3.0 for the first time
Hour, then boiling water bath enzyme denaturing 15min；Being cooled to 50 DEG C, pH is adjusted to 7.0, adds soybean protein powder weight after insulation 15min
The flavor protease of 0.4% carries out second time enzymolysis, and the pH of enzymolysis remains 7.0 for the second time, and temperature is 50 DEG C, for the second time
The time of enzymolysis is 2.5 hours, and then boiling water bath enzyme denaturing 15min, obtains soybean protein hydrolysate；
(2) ultrafiltration: soybean protein hydrolysate is cooled to room temperature, adjusts pH to 7.0, under conditions of 4 DEG C, 8000r/min
Centrifugal 10min, takes supernatant, is 0.5 × 10 with the minimum molecular weight that can retain4The ultrafilter membrane of Da carries out ultrafiltration, freezing dry
The dry low molecule soybean protein Gly-His-Lys that obtains, cryogenic temperature-45 DEG C, the cryodesiccated time is 8 hours；
(3) boiling: Herba Apii graveolentis, Fructus Perillae, Herba Menthae and Bulbus Lilii being mixed, mix homogeneously makes compound, uses compound
The water of 8 times of weight compound is first soaked, then carry out boiling 2 hours, boiling is for using slow fire after first decocting with big fire
Infusion, the temperature of big fire is 93 DEG C, and the time of decoction is 1 hour；The temperature of slow fire is 70 DEG C, and the time of infusion is 1 hour；Quiet
Postponing filtration, discard material slag and obtain feed liquid, will add konjac oligosaccharides in feed liquid, mix homogeneously postlyophilization obtains expecting powder,
Cryogenic temperature-45 DEG C, the cryodesiccated time is 8 hours；
(4) mixing: carry out mixing for the first time by described low molecule soybean protein Gly-His-Lys and material powder, add little after mix homogeneously
Wheat straw extract, yeast rich in selenium, nattokinase, chitin oligosaccharide and micromolecular collagen peptide carry out second time again and mix,
Mix homogeneously makes the health product of eliminating toxin and beautifying the skin.
Embodiment 3
The health product of a kind of eliminating toxin and beautifying the skin, are made up of following raw material: Caulis et Folium Tritici aestivi extract 15kg, konjac oligosaccharides 16kg,
Yeast rich in selenium 4kg, Herba Apii graveolentis 10kg, Fructus Perillae 30kg, Herba Menthae 30kg, Bulbus Lilii 13kg, nattokinase 10kg, chitin oligosaccharide
7kg, soybean protein powder 300kg and micromolecular collagen peptide 75kg.
Its preparation method, comprises the following steps:
(1) enzymatic hydrolysis of soybean egg albumen powder: after the water dissolution of 15 times that soybean protein powder adds its weight, through 85 DEG C of preheatings
10min, is then cooled to 60 DEG C, and pH is adjusted to 9.0, the basic protein of the 0.6% of addition soybean protein powder weight after insulation 10min
Enzyme carries out enzymolysis for the first time, and the pH of enzymolysis is 9.0 for the first time, and the time of enzymolysis is 3.5 hours for the first time, then boiling water bath enzyme denaturing
10min；Being cooled to 45 DEG C, pH is adjusted to 6.5, the flavor protease of the 0.35% of addition soybean protein powder weight after insulation 10min
Carrying out second time enzymolysis, the pH of enzymolysis is 6.5 for the second time, and the time of enzymolysis is 1.5 hours for the second time, then boiling water bath enzyme denaturing
10min, obtains soybean protein hydrolysate；
(2) ultrafiltration: soybean protein hydrolysate is cooled to room temperature, adjusts pH to 7.0, under conditions of 4 DEG C, 8000r/min
Centrifugal 10min, takes supernatant, is 0.8 × 10 with the minimum molecular weight that can retain4The ultrafilter membrane of Da carries out ultrafiltration, freezing dry
The dry low molecule soybean protein Gly-His-Lys that obtains, cryogenic temperature-50 DEG C, the cryodesiccated time is 8 hours；
(3) boiling: Herba Apii graveolentis, Fructus Perillae, Herba Menthae and Bulbus Lilii being mixed, mix homogeneously makes compound, uses compound
The water of 10 times of weight compound is first soaked, then carry out boiling 3 hours, boiling is for using slow fire after first decocting with big fire
Infusion, the temperature of big fire is 85 DEG C, and the time of decoction is 1.5 hours；The temperature of slow fire is 60 DEG C, and the time of infusion is 1.5 little
Time；Filtering after standing, discard material slag and obtain feed liquid, will add konjac oligosaccharides in feed liquid, mix homogeneously postlyophilization obtains
Material powder, cryogenic temperature-50 DEG C, the cryodesiccated time is 6 hours；
(4) mixing: carry out mixing for the first time by described low molecule soybean protein Gly-His-Lys and material powder, add little after mix homogeneously
Wheat straw extract, yeast rich in selenium, nattokinase, chitin oligosaccharide and micromolecular collagen peptide carry out second time again and mix,
Mix homogeneously makes the health product of eliminating toxin and beautifying the skin.
Embodiment 4
The health product of a kind of eliminating toxin and beautifying the skin, are made up of following raw material: Poria 30kg, Fructus Perillae 25kg, Rhizoma Chuanxiong 19kg, Bulbus Lilii
10kg, Herba Menthae 40kg, Radix Bupleuri 5kg, Rhizoma Alpiniae Officinarum 0.5kg, Fructus Aurantii 10kg, Rhizoma Atractylodis Macrocephalae 30kg, Radix Scutellariae 10kg, Radix Ginseng 40kg, natto swash
Enzyme 8kg, marine fish oligomeric Gly-His-Lys 5kg, soybean protein powder 200kg.
Its preparation method, comprises the following steps:
(1) enzymatic hydrolysis of soybean egg albumen powder: after the water dissolution of 15 times that soybean protein powder adds its weight, through 85 DEG C of preheatings
10min, is then cooled to 60 DEG C, and pH is adjusted to 9.0, the basic protein of the 0.6% of addition soybean protein powder weight after insulation 10min
Enzyme carries out enzymolysis for the first time, and the pH of enzymolysis is 9.0 for the first time, and the time of enzymolysis is 3.5 hours for the first time, then boiling water bath enzyme denaturing
10min；Being cooled to 45 DEG C, pH is adjusted to 6.5, and 0.38% flavor protease adding soybean protein powder weight after insulation 10min enters
Row second time enzymolysis, the pH of enzymolysis is 6.5 for the second time, and the time of enzymolysis is 1.0 hours for the second time, then boiling water bath enzyme denaturing
10min, obtains soybean protein hydrolysate；
(2) ultrafiltration: soybean protein hydrolysate is cooled to room temperature, adjusts pH to 7.0, under conditions of 4 DEG C, 8000r/min
Centrifugal 10min, takes supernatant, is 0.8 × 10 with the minimum molecular weight that can retain4The ultrafilter membrane of Da carries out ultrafiltration, freezing dry
The dry low molecule soybean protein Gly-His-Lys that obtains, cryogenic temperature-50 DEG C, the cryodesiccated time is 8 hours；
(3) boiling: Herba Apii graveolentis, Fructus Perillae, Herba Menthae and Bulbus Lilii being mixed, mix homogeneously makes compound, uses compound
The water of 10 times of weight compound is first soaked, then carry out boiling 3 hours, boiling is for using slow fire after first decocting with big fire
Infusion, the temperature of big fire is 90 DEG C, and the time of decoction is 80 minutes；The temperature of slow fire is 65 DEG C, and the time of infusion is 70 minutes；
Filter after standing, discard material slag and obtain feed liquid, feed liquid will add konjac oligosaccharides, after mix homogeneously, cryogenic temperature-50 DEG C,
The cryodesiccated time is 6 hours；
(4) mixing: carry out mixing for the first time by described low molecule soybean protein Gly-His-Lys and material powder, add little after mix homogeneously
Wheat straw extract, yeast rich in selenium, nattokinase, chitin oligosaccharide and micromolecular collagen peptide carry out second time again and mix,
Mix homogeneously makes the health product of eliminating toxin and beautifying the skin.
The present invention is not limited to above-mentioned preferred forms, and anyone can show that under the enlightenment of the present invention other are various
The product of form, no matter but in its shape or structure, make any change, every have same as the present application or akin skill
Art scheme, within all falling within protection scope of the present invention.
Claims (10)
1. the health product of an eliminating toxin and beautifying the skin, it is characterised in that: include the raw material of following weight portion: Caulis et Folium Tritici aestivi extract 12-18
Part, konjac oligosaccharides 13-19 part, yeast rich in selenium 3-5 part, Herba Apii graveolentis 5-15 part, Fructus Perillae 25-35 part, Herba Menthae 20-40 part, Bulbus Lilii
10-15 part, nattokinase 8-13 part, chitin oligosaccharide 5-9 part, soybean protein powder 250-350 part and micromolecular collagen
Peptide 50-100 part.
The health product of eliminating toxin and beautifying the skin the most according to claim 1, it is characterised in that: include the raw material of following weight portion: little
Wheat straw extract 15 parts, konjac oligosaccharides 16 parts, yeast rich in selenium 4 parts, Herba Apii graveolentis 10 parts, Fructus Perillae 30 parts, Herba Menthae 30 parts, Bulbus Lilii 13
Part, nattokinase 10 parts, chitin oligosaccharide 7 parts, soybean protein powder 300 parts and micromolecular collagen peptide 75 parts.
3. the preparation method of the health product of an eliminating toxin and beautifying the skin as claimed in claim 1 or 2, it is characterised in that: include following
Step:
(1) enzymatic hydrolysis of soybean egg albumen powder: after the water dissolution of 10-15 times that soybean protein powder adds its weight, through 85 DEG C of preheatings
10min, is then cooled to 55-60 DEG C, and pH is adjusted to 9.0-9.5, adds alkaline protease and carry out enzyme for the first time after insulation 10min
Solving, keep pH and temperature-resistant in described first time enzymolysis process, the time of described first time enzymolysis is 2.5-3.5 hour, so
Rear boiling water bath enzyme denaturing 10-15min；Then, being cooled to 45-50 DEG C, pH is adjusted to 6.5-7.0, adds local flavor after insulation 10-15min
Protease carries out second time enzymolysis, keeps pH and temperature-resistant in described second time enzymolysis process, described second time enzymolysis time
Between be 1.5-2.5 hour, then boiling water bath enzyme denaturing 10-15min；Obtain soybean protein hydrolysate；
(2) ultrafiltration: described soybean protein hydrolysate is cooled to room temperature, regulates the pH to 7.0 of described soybean protein hydrolysate, from
The heart takes supernatant, carries out ultrafiltration with ultrafilter membrane, and filtrate lyophilization obtains low molecule soybean protein Gly-His-Lys；
(3) boiling: Herba Apii graveolentis, Fructus Perillae, Herba Menthae and Bulbus Lilii being mixed, mix homogeneously makes compound, uses described compound
The water of 8-10 times of weight described compound is first soaked, then carry out boiling 2-3 hour, filter after standing, discard material
Slag obtains feed liquid, will add konjac oligosaccharides in described feed liquid, and mix homogeneously postlyophilization obtains expecting powder；
(4) mixing: carry out mixing for the first time by described low molecule soybean protein Gly-His-Lys and material powder, add Caulis et Folium Tritici aestivi after mix homogeneously
Extract, yeast rich in selenium, nattokinase, chitin oligosaccharide and micromolecular collagen peptide carry out second time again and mix, mixing
Uniformly make the health product of eliminating toxin and beautifying the skin.
The preparation method of the health product of eliminating toxin and beautifying the skin the most according to claim 3, it is characterised in that: described in step (1)
The pH of enzymolysis is 9.3 for the first time, and the time of described first time enzymolysis is 3 hours；The pH of described second time enzymolysis is 6.8, described
The time of enzymolysis is 2 hours for the second time.
The preparation method of the health product of eliminating toxin and beautifying the skin the most according to claim 3, it is characterised in that: described in step (1)
The addition of alkaline protease is the 0.5-0.7wt% of described soybean protein powder weight；The addition of described flavor protease is
The 0.3-0.4wt% of described soybean protein powder weight.
The preparation method of the health product of eliminating toxin and beautifying the skin the most according to claim 3, it is characterised in that: described in step (2)
Being centrifuged as under conditions of 4 DEG C, 8000r/min is centrifuged 10min.
The preparation method of the health product of eliminating toxin and beautifying the skin the most according to claim 3, it is characterised in that: step (2) and step
(3) lyophilization described in is vacuum lyophilization, and described cryodesiccated cryogenic temperature is subzero 45-subzero 50
℃；The described cryodesiccated time is 6-8 hour.
The preparation method of the health product of eliminating toxin and beautifying the skin the most according to claim 3, it is characterised in that: described in step (2)
The minimum molecular weight that ultrafilter membrane can retain is 0.5 × 104Da。
The preparation method of the health product of eliminating toxin and beautifying the skin the most according to claim 3, it is characterised in that: described in step (3)
Boiling is first to use slow fire infusion, the temperature of described big fire to be 85-93 DEG C after big fire decoction, and the time of described decoction is 1-1.5
Hour；The temperature of described slow fire is 60-70 DEG C, and the time of described infusion is 1-1.5 hour.
The preparation method of the health product of eliminating toxin and beautifying the skin the most according to claim 9, it is characterised in that: the temperature of described big fire
Degree is 90 DEG C, and the time of described decoction is 80 minutes；The temperature of described slow fire is 65 DEG C, and the time of described infusion is 70 minutes.
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Application publication date: 20161109 |