CN102050847A - Extraction and separation method of tannic acid used for curing spontaneous perspiration and night sweat, tannic acid preparation and preparation method of tannic acid preparation - Google Patents
Extraction and separation method of tannic acid used for curing spontaneous perspiration and night sweat, tannic acid preparation and preparation method of tannic acid preparation Download PDFInfo
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Abstract
The invention relates to an extraction and separation method of tannic acid in the effective-part of gallnut, a tannic acid preparation and a preparation method of the tannic acid preparation. The extraction and separation method comprises the following steps: 1) cleaning and selecting medicinal material gallnut, breaking open, removing impurities; 2) grinding medicinal material gallnut, sieving with a 80 mesh sieve; 3) taking a defined amount of the grinded gallnut, adding five times of 45-55 DEG C warm water by volume to soak for 2 hours, stirring at 1000-1200rpm for 1 hour, then adding three times of water by volume to stir and extract for 1 hour, cooling the extract to 3-8 DEG C, sieving with a 200 mesh sieve; and 4) adding the filtrate in an activated carbon dry thin-film column, wherein the amount of the loaded sample is determined according to the result of thin layer chromatography; then determining the position of tannic acid in the column according to the result of thin layer chromatography, cutting the positioned tannic acid section, eluting with water, concentrating under reduced pressure and drying. The invention provides the extraction and separation method of tannic acid which has definite treatment effect and no toxic and side effect, is used for treating spontaneous perspiration and night sweat and takes effect fast and the preparation method of the tannic acid preparation.
Description
Technical field
The invention belongs to the Chemistry for Chinese Traditional Medicine field, relate to a kind of extracting method of tannic acid, relate in particular to a kind of extraction and separation method, tannic acid preparation of the Turkey-galls efficient part tannic acid that is used for the treatment of spontaneous perspiration, night sweat and insomnia thereof and the preparation method who contains the tannic acid preparation.
Background technology
Spontaneous perspiration, night sweat belong to difficult and complicated illness.Huangdi's Internal Classics is said: " sweat is bloodization, and spontaneous perspiration, night sweat leak not normal, exhausts Tianjin blood, and is serious to physical effects.The general therapeutic effect is relatively poor.Control and to seek its root, the unrooted difficult treatment.Sweat gland inhibitor for treating spontaneous perspiration, night sweat such as modern medicine coromegine commonly used are with the stable insomnia that waits tranquilizer treatment spontaneous perspiration, night sweat to follow.
With atropine treatment spontaneous perspiration, night sweat, just where itch which scratched, and following shortcoming is arranged:
1, with behind the coromegine, blurred vision, palpitaition, uroschesis, dysphoria, dry, xerosis cutis flush, heating etc., improper vain hope, the convulsions etc. of also can occurring of consumption; Patients such as pyloric obstruction, prostatomegaly, bladder neck obstruction or uroschesis, glaucoma, paralytic ileus, hematencephalon are forbidden atropine treatment.
2, with after stable, can produce tolerance and dependency.Suddenly drug withdrawal, otherwise it is uneasy irritated insomnia to occur, even cause convulsions, Withrawal symptom; Glaucoma patient's forbidding, the careful usefulness of the hepatic and renal function person of going down.
At present, the medicine that the spontaneous perspiration of shortage treatment still, night sweat one important efficient part are made on the market.The drug market of Western medicine (pharmaceutical chemicals) treatment spontaneous perspiration, night sweat more lacks.
Summary of the invention
In order to solve the above-mentioned technical problem that exists in the background technology, the invention provides that a kind of result of treatment is definite, rapid-action, the extraction and separation method of the tannic acid that is used for the treatment of spontaneous perspiration, night sweat and insomnia thereof that has no side effect and contain the preparation method of tannic acid preparation.
Technical solution of the present invention is: the invention provides a kind of extraction and separation method that is used for the treatment of the tannic acid of spontaneous perspiration, night sweat and insomnia thereof, its special character is: this method may further comprise the steps:
1) the medicinal material Turkey-galls is cleaned, break, remove impurity, standby;
2) Turkey-galls pulverizing medicinal materials is crossed 80 mesh sieves, and is standby;
3) get the Turkey-galls medicinal material that crushes, 45-55 ℃ the warm water temperature that adds 5 times of volumes was soaked 1.5-2.5 hour, stirred 0.5-1.5 hour in 1000～1200r/ minute, and the water that adds 3 times of volumes once more stirs and extracted 1 hour, extracting solution is cooled to 3～8 ℃, and 200 mesh sieves filter;
4) resulting filtrate in the step 3) is passed through the dried post of gac film, determine the sample upper column quantity, determine the location of tannic acid in post with the thin-layer chromatography result again, cut oriented tannic acid paragraph, water wash-out, concentrating under reduced pressure drying with the thin-layer chromatography result.
Above-mentioned steps 3) temperature of warm water is 48～52 ℃ in, and temperature was soaked 2 hours, stirs 1 hour in 1000～1200r/ minute, and extracting solution is cooled to 4-6 ℃.
A kind of tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat, its special character is: the described tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat and insomnia thereof mainly is prepared from for 25-35% tannic acid, 25-40% ethanol and 30-40% edible vinegar by weight percent hundred.
The above-mentioned tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat also comprises 1-3% cutaneous permeable agent and 0.03-0.08% sanitas.
The above-mentioned tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat also comprises the gel vehicle of 2-4%.
The above-mentioned tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat is a gelifying agent.
Above-mentioned ethanol is 60% ethanol.
Above-mentioned gel vehicle is a polyoxyethylene glycol, especially Macrogol 4000.
Above-mentioned cutaneous permeable agent and sanitas are respectively laurocapram and chlorhexidine.
A kind of preparation method who contains the tannic acid preparation who is used for the treatment of spontaneous perspiration, night sweat, its special character is: this method may further comprise the steps:
1) gets 60% ethanol and the 30-40% edible vinegar that the 25-35% tannic acid adds 25-40%;
2) add 1-3% cutaneous permeable agent and 0.03-0.08% sanitas;
3) add 2-4% Macrogol 4000 gel vehicle;
4) 1000-1200 rev/min emulsification 6-8 minute;
5) by this product standard test;
6) divide packing after the assay was approved.
Advantage of the present invention is:
The present invention is about spontaneous perspiration according to the traditional Chinese medical science, night sweat is not urge because of lung qi, disharmony between ying and wei, fire excess from yin deficiency, sweat leaked not normal due to heat symptoms caused by an exopathgen were hot and suffocating cause of disease theory and application experience, from the Turkey-galls (gas of astringing the lung, the fire of deficiency type is fallen, the convergence hidroschesis), shizandra berry (the nourshing kidney of astringing the lung, the arrest sweating hidroschesis), skunk bush (is the invigorating the liver and kidney key medicine, and the merit of the heart-yin of holding back hidroschesis arranged), dark plum (sour-puckery flavor, go into lung channel, can astringe the lung, be used for insufficiency of lung-QI, spontaneous perspiration, night sweat), (fall fire astringes the lung chebule, be used for insufficiency of lung-QI, breathe hard, spontaneous perspiration, night sweat) Turkey-galls of screening in the plurality of Chinese such as, by extraction separation, again by gallotannic acid being prepared into the treatment spontaneous perspiration to Turkey-galls efficient part tannic acid, the preparation of night sweat (abnormal sweating sport gel), it has the following advantages:
1, Turkey-galls has the gas of astringing the lung, and falls the fire of deficiency type, and harmonizing yingfen and weifen is separated the hot and suffocating effect of heat symptoms caused by an exopathgen.The basic cause of disease at spontaneous perspiration, night sweat is treated, and medication just produced curative effect the same day, and 5～10 curative ratios of medication can reach more than 60%; And spontaneous perspiration, night sweat patient's insomnia there is definite curative effect; Have no side effect.
2, dosage is few, saves medicinal material, saves manufactured energy, has no side effect after the medication.Abnormal sweating health medication every day 1 time is calculated by the Turkey-galls medicinal material, 1 usefulness 1～2 gram.The traditional Chinese medical science is prescribed and is treated spontaneous perspiration, night sweat, (1 dose) medication in a day 80～140 grams.Once opening 6～10 doses is a course of treatment, determines the course of treatment according to the treatment situation.Select its efficient part gallotannic acid of Turkey-galls extraction separation, make the abnormal sweating health, bigger value is arranged.
3, the advantage of SHENQUE acupoint medication, this product are used for SHENQUE acupoint (navel) outward, have both brought into play the therapeutic action of medicine itself, play a role by SHENQUE acupoint again.SHENQUE acupoint is the life crisis of human body, the door that manner is current, the root of passages through which vital energy circulates.It links to each other with the human body twelve regular channels, and the vital organs of the human body communicate, and the critical role of " navel is a congenital foundation, the origin of life " is arranged, and is human qi and blood running's passage, is in the communication table, the system of a uniqueness up and down.Learn medication at Shenque, performance medicine and acupuncture point dual function, drug dose few (can medication in to two day once, ampoule is equivalent to crude drug in whole 1 gram), effective.The SHENQUE acupoint medication belongs to externally applied medicine, need not have an injection, need not be oral, medication in 1～2 day once, medication is convenient.
Embodiment
The present invention is the efficient part gallotannic acid that extraction separation is used for the treatment of spontaneous perspiration, night sweat and insomnia thereof from Turkey-galls, gallotannic acid is prepared into the preparation (abnormal sweating sport gel) of treatment spontaneous perspiration, night sweat and insomnia thereof again, its Turkey-galls screening foundation:
Is short, disharmony between ying and wei, fire excess from yin deficiency because of lung qi according to the traditional Chinese medical science about spontaneous perspiration, night sweat, and the Chinese medicine of spontaneous perspiration, night sweat is treated in the theoretical screening of the cause of disease that sweat leaked not normal due to heat symptoms caused by an exopathgen were hot and suffocating.Though many Chinese medicines have the effect of treatment spontaneous perspiration, night sweat, single firmly thin, need be used, for example:
1. glutinous rice root: it is sweet to distinguish the flavor of, and suffering is nontoxic, and reinforcing stomach reg fluid is arranged, the hidroschesis antipyretic effect.Be used for the treatment of abnormal sweating, reducing the asthenic fever, single firmly book, normal and Radix Asparagi, Radix Ophiopogonis, Tree Peony Bark, Root-bark of Chinese Wolfberry etc. are used.
2. shriveled wheat: it is sweet, nontoxic to distinguish the flavor of.Useful gas heat extraction anti-hidropoiesis.So all spontaneous perspiration due to yang insufficiencies, night sweat due to yin deficiency all can be selected for use.As " formulary of peaceful benevolent dispensary. volume eight " Muli San, form by 6 flavor Chinese medicines such as oysters.
3. the Radix Astragali: it is sweet, nontoxic to distinguish the flavor of.Usefully defend solid table effect, be used for the abnormal sweating card, as " formulary of peaceful benevolent dispensary. volume eight " Muli San: this product and oyster, Radix Ephedrae, shriveled wheat, the bighead atractylodes rhizome, windproof being used.
4. oyster: it is salty to distinguish the flavor of, and is slightly cold, nontoxic.The astringent or styptic treatment for spontaneous sweating effect of convergence is arranged, be used for abnormal sweating etc., as " formulary of peaceful benevolent dispensary. volume eight " Muli San.
5. the bighead atractylodes rhizome: bitter, sweet, nontoxic, anti-hidropoiesis is arranged, be used for spontaneous sweating due to deficiency of QI etc.As " Essential Recipes for Emergent Use Worth A Thousand Gold. volume ten ": this product normal and the Radix Astragali, oyster, Radix Ephedrae, shriveled wheat are equal to usefulness.
6. Radix Ephedrae: it is sweet to distinguish the flavor of, and little hardship is nontoxic.Anti-hidropoiesis is arranged, be used for spontaneous perspiration, abnormal sweating etc., this product convergence hidroschesis is the product that take stopgap measures, allocates compound into and uses, as " Standards of Diagnosis and Treatment. volume five " Radix Ephedrae looses, is used with this product and the Radix Astragali, Radix Angelicae Sinensis, shriveled wheat, oyster, the dried rhizome of rehmannia, Turkey-galls, skunk bush etc.
7. date: it is sweet, nontoxic to distinguish the flavor of, and the effect of bowl spares gas is arranged.When inducing sweat sweating, prevent that with date ginger sweating sweat hinders battalion, harmonizing nutrient QI and difensive QI more with ginger.
8. Radix Codonopsis: invigorating the spleen and replenishing QI is used for lung qi and loses void etc.
9. shizandra berry flavor acid, temperature, nontoxic.Have the sweat restrain action of promoting the production of body fluid, it is thirsty to be used for Tianjin wound, spontaneous sweating.As " general Ji ability side. volume five ": " shizandra berry is joined Turkey-galls, Radix Ephedrae, and oyster, Folium Mori treatment spontaneous sweating is effective.”
10. skunk bush flavor acid, tepor, nontoxic.Have the astringent or styptic treatment for spontaneous sweating effect of convergence, be used for diseases such as abnormal sweating.As " square dragon's pool man secret ": " skunk bush is joined Turkey-galls, oyster, shizandra berry, root of herbaceous peony treatment spontaneous sweating etc. ".
11. Fruit of Cherokee Rose acid is puckery, and is nontoxic.The merit that arrest sweating is arranged.As " book on Chinese herbal medicine is just ": " Fruit of Cherokee Rose is received abnormal sweating, the treatment abnormal sweating, and joining Turkey-galls has good effect.”
12. Turkey-galls: flavor acid, puckery, nontoxic, go into lung, liver, kidney etc.Have the gas of astringing the lung, fall the fire of deficiency type, effects such as convergence hidroschesis cure mainly spontaneous sweating.Say as " interior warp ": " sweat be blood biochemistry, disharmony between ying and wei because of insufficiency of lung-QI, fire excess from yin deficiency, due to heat symptoms caused by an exopathgen were hot and suffocating, it is not normal that sweat leaks, liquid consumption liver void, the convergence hidroschesis falls the fire of deficiency type, in the available Turkey-galls gas of astringing the lung." and for example " Compendium of Materia Medica. roll up 39. Turkey-galls " draw " Ji Lingfang ": list is used this product levigation, controls abnormal sweating with the Fagopyrum esculentum Moench equal portions; An amount of with gallnut extract, water is in harmonious proportion and applies on the navel, controls the night sweat spontaneous perspiration and imitates good.Ran Xuefeng." Datong District's pharmacology ": " Turkey-galls, its tart flavour is very dense, and on real super each this oxalic acid medicine of its function, Turkey-galls is large effective constituent with tart flavour.
Have abnormal sweating to stop particle (treatment spontaneous perspiration, night sweat), multiple stilbene hidroschesis particle (treatment spontaneous perspiration) and Radix Astragali essenc oral liquid (treatment spontaneous perspiration), its shortcoming at present on the market: 1. diabetics's spontaneous perspiration, night sweat and insomniac thereof can not use; 2. to spontaneous perspiration, the insomniac of night sweat is invalid; 3. multiple stilbene hidroschesis particle, the Radix Astragali essenc oral liquid is invalid to the night sweat patient.Turkey-galls is single, and night sweat is imitated good with the treatment spontaneous perspiration, and on real super each this oxalic acid medicine of its function, Turkey-galls is large effective constituent with its tart flavour.In sum, for selecting the Turkey-galls project verification that important evidence is provided.
The inventor engages in the research of Chinese materia medica aspect for a long time, through constantly practice, creates out a kind of extraction and separation method that is used for the treatment of the Turkey-galls efficient part tannic acid of spontaneous perspiration, night sweat and insomnia thereof, and this method may further comprise the steps:
1) the medicinal material Turkey-galls is cleaned, break, remove impurity, standby;
2) Turkey-galls pulverizing medicinal materials is crossed 80 mesh sieves, and is standby;
3) get the Turkey-galls medicinal material that crushes, 45-55 ℃ the warm water temperature that adds 5 times of volumes was soaked 1.5-2.5 hour, stirred 0.5-1.5 hour in 1000～1200r/ minute, and the water that adds 3 times of volumes once more stirs and extracted 1 hour, extracting solution is cooled to 3～8 ℃, and 200 mesh sieves filter;
4) resulting filtrate in the step 3) is passed through the dried post of gac film, determine the sample upper column quantity, determine the location of tannic acid in post with the thin-layer chromatography result again, cut oriented tannic acid paragraph, water wash-out, concentrating under reduced pressure drying with the thin-layer chromatography result.
A kind of tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat mainly is prepared from by the gel vehicle and the 0.03-0.08% sanitas of weight percent hundred for 25-35% tannic acid, 25-40%60% ethanol, 30-40% edible vinegar, 1-3% cutaneous permeable agent, 2-4%.Gel vehicle is a polyoxyethylene glycol, especially Macrogol 4000.Cutaneous permeable agent and sanitas are respectively laurocapram and chlorhexidine.This tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat is a gelifying agent.
Below be concrete proportioning example of the present invention (is unit with the weight percent):
The present invention also provides a kind of preparation method who uses with the Turkey-galls efficient part tannic acid preparation (abnormal sweating sport gel) for the treatment of spontaneous perspiration, night sweat, and this method may further comprise the steps:
1) gets 60% ethanol and the 30-40% edible vinegar that the 25-35% tannic acid adds 25-40%;
2) add 1-3% cutaneous permeable agent and 0.03-0.08% sanitas;
3) add 2-4% Macrogol 4000 gel vehicle;
4) 1000-1200 rev/min emulsification 6-8 minute;
5) by this product standard test;
6) divide packing after the assay was approved.
Choose Turkey-galls, according to aforesaid method gallic efficient part tannic acid is carried out extraction separation, and be made into preparation (abnormal sweating sport gel), to the clinical comparison experiment, experiment divides two groups, and every group 180 people observes the result of treatment to spontaneous perspiration, night sweat, and the result is as follows:
Experiment one: control group, with dark plum 1500 grams, Turkey-galls 1500 grams, the Radix Astragali 1500 grams, with 60% alcohol reflux, reclaim ethanol, concentrating under reduced pressure is prepared into gelifying agent according to the method for abnormal sweating health, each consumption is equivalent to Chinese medicinal materials 5 grams, once a day, continuous use 5 times, external application is affixed on SHENQUE acupoint treatment spontaneous perspiration, night sweat patient 180 examples.As a result, cure 53 examples (29.4%), effective 81 examples (45%), invalid 46 examples (25.6%), total effective rate 74.4%.
Experiment two: treatment group, be equivalent to Turkey-galls medicinal material 1 gram with abnormal sweating sport gel (gelifying agent that Turkey-galls efficient part tannic acid is made) at every turn, logotype 5 times, external application is affixed on SHENQUE acupoint, treats 180 routine spontaneous perspirations, night sweat patient, the result, cure 119 examples (66.1%), effective 52 examples (28.9%), invalid 9 examples (5%), total effective rate 95%.Spontaneous perspiration, night sweat person insomnia also there is good result.
Experiment three: treatment group, be equivalent to Turkey-galls medicinal material 1 gram with abnormal sweating sport gel (gelifying agent that Turkey-galls efficient part tannic acid is made) at every turn, logotype 5 times, external application is affixed on SHENQUE acupoint, treats 240 routine spontaneous perspirations, night sweat patient, the result, cure 163 examples (68.2%), effective 71 examples (29.6%), invalid 6 examples (2.2%), total effective rate 97.8%.Spontaneous perspiration, night sweat person insomnia also there is good result.
Experiment four: treatment group, be equivalent to Turkey-galls medicinal material 1 gram with abnormal sweating sport gel (gelifying agent that Turkey-galls efficient part tannic acid is made) at every turn, logotype 5 times, external application is affixed on SHENQUE acupoint, treats 200 routine spontaneous perspirations, night sweat patient, the result, cure 135 examples (67.4%), effective 54 examples (27.1%), invalid 11 examples (5.5%), total effective rate 94.5%.Spontaneous perspiration, night sweat person insomnia also there is good result.
Claims (10)
1. extraction and separation method that is used for the treatment of the tannic acid of spontaneous perspiration, night sweat, it is characterized in that: this method may further comprise the steps:
1) the medicinal material Turkey-galls is cleaned, break, remove impurity, standby;
2) Turkey-galls pulverizing medicinal materials is crossed 80 mesh sieves, and is standby;
3) get the Turkey-galls medicinal material that crushes, 45-55 ℃ the warm water temperature that adds 5 times of volumes was soaked 1.5-2.5 hour, stirred 0.5-1.5 hour in 1000～1200r/ minute, and the water that adds 3 times of volumes once more stirs and extracted 1 hour, extracting solution is cooled to 3～8 ℃, and 200 mesh sieves filter;
4) resulting filtrate in the step 3) is passed through the dried post of gac film, determine the sample upper column quantity, determine the location of tannic acid in post with the thin-layer chromatography result again, cut oriented tannic acid paragraph, water wash-out, concentrating under reduced pressure drying with the thin-layer chromatography result.
2. the extraction and separation method that is used for the treatment of the tannic acid of spontaneous perspiration, night sweat according to claim 1, it is characterized in that: the temperature of warm water is 48～52 ℃ in the described step 3), temperature was soaked 2 hours, stirred 1 hour in 1000～1200r/ minute, and extracting solution is cooled to 4-6 ℃.
3. tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat is characterized in that: the described tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat mainly is prepared from for 25-35% tannic acid, 25-40% ethanol and 30-40% edible vinegar by weight percent hundred.
4. the tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat according to claim 3 is characterized in that: the described tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat also comprises 1-3% cutaneous permeable agent and 0.03-0.08% sanitas.
5. the tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat according to claim 4 is characterized in that: the described tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat also comprises the gel vehicle of 2-4%.
6. according to claim 3 or the 4 or 5 described tannic acid preparations that are used for the treatment of spontaneous perspiration, night sweat, it is characterized in that: the described tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat is a gelifying agent.
7. the tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat according to claim 6 is characterized in that: described ethanol is 60% ethanol.
8. the tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat according to claim 7, it is characterized in that: described gel vehicle is a polyoxyethylene glycol, especially Macrogol 4000.
9. the tannic acid preparation that is used for the treatment of spontaneous perspiration, night sweat according to claim 8 is characterized in that: described cutaneous permeable agent and sanitas are respectively laurocapram and chlorhexidine.
10. preparation method who contains the tannic acid preparation who is used for the treatment of spontaneous perspiration, night sweat, it is characterized in that: this method may further comprise the steps:
1) gets 60% ethanol and the 30-40% edible vinegar that the 25-35% tannic acid adds 25-40%;
2) add 1-3% cutaneous permeable agent and 0.03-0.08% sanitas;
3) add 2-4% Macrogol 4000 gel vehicle;
4) 1000-1200 rev/min emulsification 6-8 minute;
5) by this product standard test;
6) divide packing after the assay was approved.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023208807A1 (en) * | 2022-04-28 | 2023-11-02 | L'oreal | Makeup composition comprising a polyphenol, a polyoxyalkylenated hydrocarbon-based compound and a monoalcohol, and processes using same |
| WO2023212371A3 (en) * | 2022-04-28 | 2023-12-07 | L'oreal | Cosmetic compositions comprising polyphenols, suitable as setters |
| FR3137566A1 (en) * | 2022-07-05 | 2024-01-12 | L'oreal | COMPOSITIONS SUITABLE AS FIXATORS |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023208807A1 (en) * | 2022-04-28 | 2023-11-02 | L'oreal | Makeup composition comprising a polyphenol, a polyoxyalkylenated hydrocarbon-based compound and a monoalcohol, and processes using same |
| WO2023212371A3 (en) * | 2022-04-28 | 2023-12-07 | L'oreal | Cosmetic compositions comprising polyphenols, suitable as setters |
| FR3137566A1 (en) * | 2022-07-05 | 2024-01-12 | L'oreal | COMPOSITIONS SUITABLE AS FIXATORS |
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Application publication date: 20110511 |