CN101983133A - 可喷墨印刷的制品及其制造方法 - Google Patents

可喷墨印刷的制品及其制造方法 Download PDF

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CN101983133A
CN101983133A CN2008801284658A CN200880128465A CN101983133A CN 101983133 A CN101983133 A CN 101983133A CN 2008801284658 A CN2008801284658 A CN 2008801284658A CN 200880128465 A CN200880128465 A CN 200880128465A CN 101983133 A CN101983133 A CN 101983133A
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B-J·牛
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Abstract

本发明涉及一种可喷墨印刷制品，其具有结合到芯基底上的油墨接受层，该油墨接受层包括下面各组分的混合物：i)至少一种可自交联的聚氨酯树脂；ii)至少一种可自交联的苯乙烯丁二烯共聚物；和iii)至少一种苯乙烯丙烯酸共聚物，其中该油墨接受层是阴离子性的或者中性的，和其中该芯基底包括选自织造材料和非织造材料的材料。

Description

可喷墨印刷的制品及其制造方法
发明背景
本发明通常涉及织造和非织造基底。已经发现当用专门开发用于印刷乙烯基和其它类似有机材料的油墨进行印刷时，这些基底具有差的印刷质量和耐久性。这种基底的一个主要问题是缺少这样的表面层，该表面层在油墨碰撞到基底时能够获得良好的润湿。结果通常是低的色域和不期望的渗色。此外，印刷的区域通常不具有良好的耐擦性。
发明内容
本文公开的制品、方法和系统的实施方案有利地表明当用包括颜料着色剂、胶乳粘合剂、非水溶剂和水的油墨印刷织造和非织造基底时，包括苯乙烯丙烯酸、可自交联的聚氨酯和可自交联的苯乙烯-丁二烯共聚物的优化的涂料配方明显地提高了色域(能够达到高到500000色域)和渗色。印刷样品的耐久性也得以提高。在一种实施方案中，该印刷在可喷墨印刷制品的油墨接受层上的油墨包括颜料着色剂、胶乳粘合剂、非水溶剂和水。
在结合到芯基底上的可喷墨印刷制品的一种实施方案中，油墨接受层包括下面组分的混合物：i)至少一种可自交联的聚氨酯树脂；ii)至少一种可自交联的苯乙烯丁二烯共聚物；和iii)至少一种苯乙烯丙烯酸共聚物。在另外一种实施方案中，该可喷墨印刷制品的油墨接受层包括20-60重量％的可自交联的聚氨酯树脂；10-40重量％的可自交联的苯乙烯丁二烯共聚物；和10-50重量％的苯乙烯丙烯酸共聚物。
在上述可喷墨印刷制品的另一种实施方案中，该可喷墨印刷制品的油墨接受层的硬度是大约5MPa-大约50MPa。
在本发明的一种实施方案中，使用下面成分的组合来获得用于织造或者非织造基底的油墨接受层的涂料配方。Sancure
Figure BPA00001233634500011
815和Turboset
Figure BPA00001233634500012
2025都是可自交联的聚氨酯，获自USA，OH，Cleveland的Lubrizol。它们都用于该实施方案中。这两种聚氨酯一起为使用Windex清洁器的擦拭试验中的涂料配方提供了良好的耐擦性。它们还有助于保持良好的图像质量。Rovene
Figure BPA00001233634500014
4151是一种可自交联的苯乙烯-丁二烯共聚物，获自USA，NC，Charlotte的Mallard Creek Polymer，Inc.。该共聚物提供了对于包括颜料着色剂、胶乳粘合剂、非水溶剂和水的油墨良好的亲合性。它还提供了良好的图像质量(IQ)。Hycar26448获自USA，OH，Cleveland的Lubrizol，它是一种苯乙烯丙烯酸共聚物，其能够将油墨接受层的表面能从30达因/cm的初始低水平提高到最高达45达因/cm。这进而有助于提高色域。
还在油墨接受层中测试了下面的其它已知的聚氨酯，并且发现除了加入特别的交联剂例如Xama
Figure BPA00001233634500022
外，它们不是有效的，该其它已知的聚氨酯例如是获自USA，CT，Middlebury的Chemtura Corp.的Witcobond213；获自USA，NC，Greensboro的AlberdingK Boley Inc.的AlberdingK
Figure BPA00001233634500024
 U2101和AlberdingK CUR21；获自USA，PA，Pittsburgh的Bayer Material Science LLC.的Bayhydrol
Figure BPA00001233634500026
140AQ和Bayhydrol
Figure BPA00001233634500027
XP2618；和获自USA，OH，Cleveland的Lubrizol的Sancure
Figure BPA00001233634500028
2715。
作为一种非限定性的例子，上述的油墨接受层可以施用到由织造或者非织造基底材料制成的基底上。不同的方法可以用于将该油墨接受层施用到基底上。这样的方法的一些非限定性的例子包括门-辊计量涂布，刮刀计量涂布，Meyer棒计量涂布，或者狭缝计量涂布。在由织造或者非织造材料制成的基底中所用的材料的非限定性的例子包括高密度聚乙烯(HDPE)。
在织造基底材料的一种非限定性的例子中，开始时将HDPE粉碎，并且挤出来生产HDPE纤维。将该纤维织入基底中。作为一个例子，由HDPE纤维织造的基底可购自加拿大安大略湖的PGI-Fabrene Inc.，产品名称PGI-Fabrene-V749-2W5W3。在另一种实施方案中，该可喷墨印刷制品的织造基底可以处于由天然和/或合成纤维制成的织造的或者编织的织物的形式。
在非织造基底材料的一种非限定性的例子中，将HDPE加压和固结成为一种平的、片状基底材料。这样的基底的一个例子是以商标名Tyvek销售自USA，DE，Wilmington的DuPont公司。
织造和非织造基底二者都具有许多空隙或者孔，其每个可以用直径大约为3μm-20μm的阴离子性或者中性颗粒填充。二氧化硅颗粒(其是阴离子的)特别适用于填充存在于这样的基底中的孔。还可以使用具有阴离子或者中性电荷的其它无机或者有机颗粒。它们包括具有中性电荷的有机球体。
这样的用于填充孔或者空隙的颗粒给基底本身赋予了电荷。因此基底(其具有施用到整个表面上来填充空隙的二氧化硅颗粒)将具有完全的负性表面电荷。相反，具有用有机球体来填充空隙的基底将具有完全的中性表面电荷。
在一种实施方案中，作为上述阴离子颗粒赋予的表面电荷的结果，该可喷墨印刷制品的油墨接受层的Zeta(ζ)电位范围是从-10到-80mV。ζ电位值是用来自USA，MA，Westborough的Malvern Instruments的Zetasizer Nano-ZS(型号：Zen 3600)来测量的。
同样在一种实施方案中，已经发现使用印刷到上述涂料配方上的油墨时，在该油墨之间发生的渗色在该油墨之间为小于10mil间隔。
为了进一步说明本发明的实施方案，在此给出了下面的实施例。应当明白这些实施例是作为示例性目的提供的，并且不解释为对所公开的实施方案范围的限制。
                        实施例
实施例1
测量了本发明所述的基底的油墨接受层中所用的不同的聚合物的ζ电位，包括聚氨酯和其它聚合物。该ζ电位值示于表1中。该ζ电位值代表了离子特性。正值代表了阳离子特性，负值代表阴离子特性。
表1
Figure BPA00001233634500031
实施例2
油墨接受层配方1和配方2是用表2所示的组分和所给出的重量浓度来制备的。
表2
Figure BPA00001233634500041
测量了配方1和2各自的ζ电位，如下表3所示。
表3
化学品        ζ电位(mV)
配方1         -59.8
配方2         -57.3
实施例3
对不同的聚氨酯进行了采用Windex
Figure BPA00001233634500042
溶剂的擦拭测试。将聚氨酯包覆的表面用Windex
Figure BPA00001233634500043
溶剂浸泡的布进行擦拭。基于用Windex
Figure BPA00001233634500044
溶剂擦拭的面上表面保持的完好程度来将所述配方分为通过/失败。“通过”情形给予任何这样的测试样品，即在用Windex
Figure BPA00001233634500045
清洁器擦拭所述的膜6次之后，该膜没有表现出任何的损坏。“失败”情形给予任何这样的测试样品，即在用Windex
Figure BPA00001233634500046
清洁器擦拭所述的膜6次之后，该膜出现损坏。不同的配方的测试结果在下表4中示出。
表4
成分                擦拭测试(通过/失败)
Witcobond
Figure BPA00001233634500051
W-213                   失败
Witcobond
Figure BPA00001233634500052
W-296                   失败
Sancure
Figure BPA00001233634500053
2715                    失败
Sancure815                     失败
Bayhydrol
Figure BPA00001233634500055
140AQ                   失败
Bayhydrol
Figure BPA00001233634500056
 XP 2618                失败
AlberdingK Cur 21                 失败
Turboset
Figure BPA00001233634500058
2025                    通过
实施例4
将聚氨酯和其它聚合物的四种配方作为油墨接受层分别施用到四个基底上。所述层中的配方指定为配方3-6。该非水溶剂油墨然后施用到配方3-6的每个上。胶乳含水油墨也分别施用到配方3-6的每个上。结果如下表5所示。仅有非水溶剂油墨配方6表现出良好的结果。
还通过将两种油墨颜色彼此相邻印刷来测试了配方3-6的色对色的渗色。当一种颜色的油墨进入到另一色油墨中时发生渗色。在本申请中所示的色对色的渗色结果是用一种油墨渗入到相邻油墨时经过的距离来度量的。表5中较高的色对色的渗色结果数值(单位毫英寸(mil))代表了渗色的增加。这样增加的渗色导致了更差的图像锐度，该锐度影响图像质量。当油墨间的色对色渗色仅仅发生在小的距离时(例如＜10mil)，这对于图像锐度和图像质量具有好的影响。
表5
Figure BPA00001233634500061
实施例5
获得了上述实施例所述的配方1-6的样品的印刷质量可见的分级。将样品用非水溶剂油墨和带有胶乳聚合物的含水油墨单独进行印刷。在分级中，1是最差，5是最好。该分级列表在下表6中。该表还包括了实施例3中所述的基于用Windex
Figure BPA00001233634500062
清洁器作为溶剂的擦拭测试的膜耐久性结果。测试是在非织造和织造基底二者上进行的。
表6：性能汇总
Figure BPA00001233634500063
实施例6
将配方2作为油墨接受层施用到Tyvek
Figure BPA00001233634500071
基底和HPDE织造膜二者上。测量了每个基底的油墨接受层的硬度，单位是MPa。硬度测量结果列于表7中。该实施例中的膜硬度数据是用带有Berkovich压头的MTS Nanoindenter XP来测量的。
表7：硬度测试结果
Figure BPA00001233634500072
虽然已经详细描述了几种实施方案，但是对本领域技术人员来说显然可以对所公开的实施方案进行改进。所以，前面的说明被认为示例性的，而非限制性的。

Claims (25)

1.一种可喷墨印刷制品，其包含结合到芯基底上的油墨接受层，该油墨接受层包括下面各组分的混合物：i)至少一种可自交联的聚氨酯树脂；ii)至少一种可自交联的苯乙烯丁二烯共聚物；和iii)至少一种苯乙烯丙烯酸共聚物，其中该油墨接受层是阴离子性的或者中性的，和其中该芯基底包括选自织造材料和非织造材料的材料。
2.权利要求1的制品，其中该油墨接受层基本上由下列组分组成：
大约20-60重量％的可自交联的聚氨酯树脂；
大约10-40重量％的可自交联的苯乙烯丁二烯共聚物；和
大约10-50重量％的苯乙烯丙烯酸共聚物。
3.权利要求1的制品，其中该芯基底表面包括无机或者有机颗粒，该颗粒的直径是大约3μm-大约20μm，并且带有阴离子电荷或者中性电荷；和其中该芯基底表面颗粒选自二氧化硅颗粒、有机塑料球形颗粒及其组合。
4.权利要求1的制品，其中该油墨接受层的ζ电位范围是从-10mV到-80mV。
5.权利要求1的制品，其中该油墨接受层的硬度是5MPa-50MPa。
6.权利要求1的制品，其中该织造材料或者非织造材料包括聚合物。
7.权利要求6的制品，其中该聚合物包括高密度聚乙烯。
8.权利要求1的制品，其中该织造材料包括HDPE纤维。
9.权利要求1的制品，其中该织造材料是织物。
10.权利要求1的制品，其中在印刷到该可喷墨印刷制品上的两个油墨之间的渗色为小于10mil的间隔。
11.权利要求1的制品，其中印刷到该油墨接受层上的油墨包括颜料着色剂、胶乳粘合剂、非水溶剂和水。
12.一种生产可喷墨印刷制品的方法，该制品包括芯基底和油墨接受层，该方法包含将涂料组合物施涂到芯基底上的步骤，该涂料组合物包括：
至少一种可自交联的聚氨酯树脂；
至少一种苯乙烯丁二烯共聚物；和
至少一种苯乙烯丙烯酸聚合物；
其中该芯基底包括选自织造材料和非织造材料的材料。
13.权利要求12的方法，其中该油墨接受层基本上由下列组分组成：
大约20-60重量％的可自交联的聚氨酯树脂；
大约10-40重量％的可自交联的苯乙烯丁二烯共聚物；和
大约10-50重量％的苯乙烯丙烯酸共聚物。
14.权利要求12的方法，其中该芯基底表面包括无机或者有机颗粒，该颗粒的直径是3-20μm，并且带有阴离子电荷或者中性电荷；和其中该芯基底表面颗粒选自二氧化硅颗粒和有机塑料球形颗粒及其组合。
15.权利要求12的方法，其中该油墨接受层的ζ电位范围是从-10mV到-80mV。
16.权利要求12的方法，其中该油墨接受层的硬度是5MPa-50MPa。
17.权利要求12的方法，其中印刷到该油墨接受层上的油墨包括颜料着色剂、胶乳粘合剂、非水溶剂和水。
18.权利要求12的方法，其中在印刷到该油墨接受层上的两个油墨之间的渗色为小于10mil的间隔。
19.一种喷墨印刷具有油墨接受层的芯基底的系统，其包含：
喷墨印刷机；
该油墨接受层包括i)至少一种可自交联的聚氨酯树脂；ii)至少一种苯乙烯丁二烯共聚物；和iii)至少一种苯乙烯丙烯酸聚合物；和
该芯基底包括选自织造材料和非织造材料的材料。
20.权利要求19的系统，其中该油墨接受层基本上由下列组分组成：20-60重量％的可自交联的聚氨酯树脂；10-40重量％的可自交联的苯乙烯丁二烯共聚物；和10-50重量％的苯乙烯丙烯酸共聚物。
21.权利要求19的系统，其中该芯基底表面包括无机或者有机颗粒，该颗粒的直径是3-20μm，并且带有阴离子电荷或者中性电荷；和其中该芯基底表面颗粒选自二氧化硅颗粒和有机塑料球形颗粒及其组合。
22.权利要求19的系统，其中该油墨接受层的ζ电位范围是从-10到-80mV。
23.权利要求19的系统，其中该油墨接受层的硬度是5MPa-50MPa。
24.权利要求19的系统，其中印刷到该油墨接受层上的油墨包括颜料着色剂、胶乳粘合剂、非水溶剂和水。
25.权利要求19的系统，其中在印刷到该油墨接受层上的两个油墨之间的渗色为小于10mil的间隔。
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