CN101966140B - Method for preparing fishy smell removed submicron pearl powder with regular geometric shape - Google Patents
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- 238000000034 method Methods 0.000 title claims abstract description 38
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- 244000293323 Cosmos caudatus Species 0.000 claims description 104
- 239000000796 flavoring agent Substances 0.000 claims description 20
- 238000010298 pulverizing process Methods 0.000 claims description 19
- 239000000725 suspension Substances 0.000 claims description 17
- 239000002245 particle Substances 0.000 claims description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 235000019634 flavors Nutrition 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 9
- 238000005516 engineering process Methods 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 238000009423 ventilation Methods 0.000 claims description 7
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
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- 235000015097 nutrients Nutrition 0.000 abstract description 3
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 230000036541 health Effects 0.000 description 5
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- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- RGHNJXZEOKUKBD-SQOUGZDYSA-N Gluconic acid Natural products OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 3
- 230000003851 biochemical process Effects 0.000 description 3
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- RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 230000003796 beauty Effects 0.000 description 2
- 239000000174 gluconic acid Substances 0.000 description 2
- 235000012208 gluconic acid Nutrition 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000005469 granulation Methods 0.000 description 2
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- 239000004310 lactic acid Substances 0.000 description 2
- 235000014655 lactic acid Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
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- 235000013619 trace mineral Nutrition 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 241000201295 Euphrasia Species 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 241000475481 Nebula Species 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000008033 biological extinction Effects 0.000 description 1
- 150000001669 calcium Chemical class 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
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- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
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- 230000035764 nutrition Effects 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000000643 oven drying Methods 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
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- 239000003440 toxic substance Substances 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
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- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention relates to a method for processing pearl powder for high-grade cosmetics, health-care products and medicaments, in particular to a method for preparing fishy smell removed submicron pearl powder with regular geometric shape. The method for preparing the fishy smell removed submicron pearl powder with regular geometric shape comprises the following steps of: (1) first crushing; (2) cracking treatment; (3) second submicron crushing; (4) smell removal; and 5) third crushing. The submicron pearl powder prepared by the method has unchangeable color and regular geometric shape, and the grain diameter of the submicron pearl powder is more than 100 nanometers and less than 1,000 nanometers; and the method avoids potential hazard of a nano product to the human body on the premise of effectively improving the skin osmotic absorption efficiency and gastrointestinal absorption efficiency of the pearl powder, ensures the use safety of the product, and is widely applied in the production fields of medicaments, nutrient health-care food, skin-care products and cosmetics.
Description
Technical field
The present invention relates to the processing method of a kind of cosmetics of super quality, health product, pharmaceutical Margarita powder, relate in particular to a kind of method for preparing with regular geometric shapes smelling removal submicron Margarita powder.
Background technology
Margarita is a kind of jewelry adornment of top grade, still a kind of famous and precious Chinese crude drug, cosmetics and nutrient and healthcare products, its medicinal health and beauty functions as far back as Ming Dynasty's Compendium of Material Medica that Li Shizhen (1518-1593 A.D.) is shown roll up four or six and other medical ancient books and records in just on the books.Cure the disease in the existing very long history of China with the Margarita powder aesthetic health care.Through the modern science analysis; Margarita not only contains aminoacid, the trace element more than 20 kinds that surpasses more than 17 kinds; But also containing a large amount of biologically actived calcium, it takes orally has: effects such as tranquillizing and allaying excitement, heat-clearing and toxic substances removing, relieving cough and resolving phlegm, hemostasia and promoting granulation, the nebula that makes eye bright; External then has: looks improving and the skin nourishing, whitening and speckle dispelling, dispel dead bark, restrain granulation promoting, separate pox and treat effects such as poison.
Improving constantly of Along with people's material and cultural life, more and more to the demand of cosmetics and nutrient and healthcare products, require also increasingly high to product quality; Margarita powder has limited the product scope of application because of receiving the influence of product fineness, though along with the application of nanotechnology in the field of Margarita processing; This problem is resolved; But new problem also occurs thereupon, mainly is: one, the nanometer Margarita powder on the present market causes darkening because of its grain shape is irregular; Two, owing to have the irregular of nanometer Margarita powder grain shape now, limited of the application of more new and high technologies such as liposomal in Margarita deep processing field; Three, the inherent off-flavors of Margarita powder is effectively solved; Four, possibly there is potential hazard in particle diameter to human body less than the nanoparticle of 100 nanometers.
Existing processing method to nanometer Margarita powder roughly has following several kinds: one, physics method; Through applying external force; Destroy the concentric laminated construction that Margarita has, use mechanical efficiently case of wet attrition method (nano-pulverization) then, make through carrying out the secondary depolymerization behind the oven drying; Two, biochemical process carries out acidolysis through adding lactic acid or dilute hydrochloric acid to the super-fine pearl powder powder, adopts sol-gel technology and spray drying technology to make.Biochemical process has not only changed the Main Ingredients and Appearance of Margarita, and has destroyed effective effect, though the physics method has been avoided the weak point of biochemical process; But because the nanometer Margarita powder grain shape that makes is irregular; Influence reflection of light, cause Margarita powder to darken, and do not remove the off-flavors of Margarita; Also can't guarantee the being perfectly safe property of product, therefore having limited it is applied to the scope of application of the cosmetics of super quality, health product and medicine.
Chinese invention patent (application number: 01132213.6; The applying date: the 2001-11-13) method for preparing of disclosed a kind of nanometer pearl powder, this method are to be that solvent dissolves Margarita with the lactic acid aqueous solution, and the pH value of adjustment solution is to neutral; Hydrolyzed pearl solution is processed colloid; Make Margarita powder on grain size, reach nanoscale, adopt spray drying will make the rapid draing of hydrolyzed pearl colloid, solidify pelletize, process the Margarita powder that sphere, mean diameter are of a size of the 90-100 nanometer.Prepared nanometer Margarita powder has kept effectively nutritional labeling such as the several amino acids in the Margarita, trace element, and makes the calcium carbonate in the Margarita be converted into the easy activated calcium for absorbing of human body.This method efficient is high, energy consumption is little, and production cost is lower, is applicable to the suitability for industrialized production of medicine, nutrition and health and beauty care product.
Chinese invention patent (application number: 03153808.8; The applying date: 2003-08-22) disclose the method for preparing of nanometer pearl powder; This method is broken into 300～500 purpose fine powders with Margarita powder earlier, adds the deionized water in 4～19 times of weight portions, processes suspension; Place high pressure homogenizer to pulverize pearl suspension again, obtain the Margarita powder of particle diameter in 50～100 nanometers.This method does not change composition and the structure of Margarita, helps absorption of human body, and technology is simple, is easy to suitability for industrialized production.
Chinese invention patent (application number: 03122900.X, the applying date: this method of method for preparing that 2003-04-30) discloses nanometer pearl powder is that to adopt high pressure homogenizer that crushing pearl is become particle diameter earlier be 2～5 microns granule; And then to use concentration be citric acid or the gluconic acid aqueous solution dissolved pearl granule of 30～50wt%, and obtaining concentration is the pearl powder solution of 20～30wt%; With sodium bicarbonate the pH value of step (2) hydrolyzed pearl powder solution is adjusted to neutrality, at room temperature leaves standstill, obtain the Margarita powder colloid, drying is solidified pelletize, particle diameter be 50～90 nanometer Margarita powders.This method is pulverized Margarita owing to first, and then adopts citric acid or gluconic acid aqueous solution to disperse, and has shortened the time that obtains nanometer Margarita powder, has improved specific duty.
Summary of the invention
Darken in order to solve the existing prepared Margarita powder of nanometer Margarita powder technology of preparing; Can't effectively dispel the technical problem of the weak point existence of Margarita off-flavors; The purpose of this invention is to provide method for preparing with regular geometric shapes smelling removal submicron Margarita powder; This method has effectively been avoided the potential hazard of nano material to human body, can make the Margarita powder range of application wider, and Product Safety is higher.
In order to realize above-mentioned purpose, the technical scheme below the present invention has adopted.
A kind of method for preparing with regular geometric shapes smelling removal submicron Margarita powder, this method comprises the steps:
(1) once pulverizes: high quality pearl is adopted the beater grinder coarse pulverization, be crushed to 1000～2000 orders through supersonic jet mill behind 200 mesh sieves excessively;
(2) crack processing: import deionized water in the Margarita powder after once pulverizing, put into pressurizer, reduce pressure at last, crack Margarita powder through continuing supercharging;
(3) the secondary submicron is pulverized: adopt the compound pulverizing of flexible multidimensional field of force technology that the Margarita powder that cracks after the processing is carried out the submicron pulverizing, make particle diameter at 0.1 micron to the 1 micron submicron Margarita powder suspension with regular geometric shapes;
(4) taste removal: in submicron Margarita powder suspension, add flavor guide, the submicron Margarita powder suspension that is added with flavor guide is inserted efficient ventilation drying device,, remove the off-flavors in the Margarita powder through the outer circulation ventilation;
Pulverize for (5) three times: go the submicron Margarita powder body after the raw meat to pulverize through supersonic airstream once more drying, form the smelling removal Margarita powder with regular geometric shapes, particle diameter is 20%～100% at 0.1 micron to 1 micron submicron Margarita powder content in the Margarita powder.
Be further improvement, the 2. described weight that cracks the deionized water that adds in the treatment process of above-mentioned step is 5%～15% of Margarita powder weight, and institute's plus-pressure scope is 0.1MPa to 1MPa.Preferred as again, described lasting pressurization time is 3～12 hours.
Be further improvement, the 3. described secondary submicron of above-mentioned step pulverizing process Central Asia micron pearl powder suspension concentration is 30%～45%.
Flavor guide of the present invention for dissolve each other with water and harmless and not with the organic solvent of Margarita powder reaction, preferably use in ethanol, ethyl acetate and their aqueous solution one or more.Preferred as again, described flavor guide is an edible ethanol, and addition is 1%～5% of a submicron Margarita powder suspension quality.
Be further improvement, particle diameter is 20%～80% at 0.1 micron to 0.5 micron accumulative perception in the smelling removal submicron Margarita powder with regular geometric shapes after 5. step is pulverized for three times.
An other purpose of the present invention provides the smelling removal submicron Margarita powder with regular geometric shapes that an above-mentioned arbitrary technical scheme obtains.
The present invention compared with prior art has following outstanding advantage and good effect.
1, Margarita is very tough and tensile, and it is very difficult to be ground into the submicron order Margarita powder.The present invention is directed to the inherent physical arrangement of Margarita, through importing deionized water, put into pressurizer, lasting supercharging is reduced pressure at last, cracks Margarita powder.Margarita powder after cracking is ground into the submicron order Margarita powder easily.
2, the technological shearing of nano-pulverization equipment, the friction that is adopted of existing nanometer Margarita powder prepared by physical method is too strong; Impel Margarita powder to be crushed to particle diameter less than the irregular nano-powder of 100 nanometer geometries; Because the optical effect of nano material changes (extinction effect); Powder body after not only causing processing darkens, and makes product have potential safety hazard.Adopt the special disintegrating apparatus of the compound pulverizing of the flexible multidimensional of utilization field of force principle; Under the prerequisite that does not influence crush efficiency, both avoided Margarita powder by overground phenomenon; Product cut size is controlled at 0.1 micron to 1 micron scope; Also make the submicron Margarita powder after the processing have spherical or approximate globular regular geometric shapes, make the color of Margarita powder present white or off-white color.
3, the off-flavors that has to Margarita; Is flavor guide in the drying process link through adding the 1-5% edible ethanol; Adopt efficient outer circulation ventilation drying device; Not only removed the off-flavors in the Margarita, but also made dried Margarita powder body be puffy, be easy to be again crushed into submicron Margarita powder with regular geometric shapes.
By the prepared submicron Margarita powder of the present invention, product powder body color is constant, has the geometry of rule; Product cut size is greater than 100 nanometers; Less than 1000 nanometers,, avoided the potential hazard of nanometer product to human body effectively improving under the prerequisite of Margarita powder dermal osmosis absorption efficiency and the intestines and stomach absorption efficiency; Guaranteed the product safety in utilization, adaptable across medicine, nutritional health food, skin care item, adopt the production field of making up product.
The specific embodiment
A kind of method for preparing with regular geometric shapes smelling removal submicron Margarita powder, this method comprises the steps.
(1) selects the former pearl of high-quality: select and culture in pollution-free waters and content of beary metal such as lead, arsenic, hydrargyrum meet the high quality pearl of the provisions of the relevant regulations issued by the State.
(2) once pulverize: high quality pearl is adopted the beater grinder coarse pulverization, be crushed to 1000～2000 orders through supersonic jet mill behind 200 mesh sieves excessively.
(3) crack processing: import deionized water in the Margarita powder after once pulverizing, the weight of deionized water is 10% of Margarita powder weight, puts into pressurizer; Reduce pressure at last through continuing supercharging; Lasting pressurization time is 6 hours, and institute's plus-pressure scope is 0.1MPa to 1MPa, cracks Margarita powder.
(4) the secondary submicron is pulverized: adopt the compound pulverizing of flexible multidimensional field of force technology that the Margarita powder that cracks after the processing is carried out the submicron pulverizing; Make particle diameter at 0.1 micron to 1 micron submicron Margarita powder suspension with regular geometric shapes; Submicron Margarita powder suspension concentration is 35%, and it is that 200820164740.9 or 200820164741.3 disclosed grinding discs are installed in the compound pulverizing of the flexible multidimensional of the realization field of force on the micropowder milling apparatus that the present invention can adopt the patent No..
(5) taste removal: in submicron Margarita powder suspension, add flavor guide; Flavor guide is an edible ethanol; Addition is 3.5% of a submicron Margarita powder suspension quality; The submicron Margarita powder suspension that is added with flavor guide is inserted efficient ventilation drying device,, remove the off-flavors in the Margarita powder through the outer circulation ventilation.
Pulverize for (6) three times: go the submicron Margarita powder body after the raw meat to pulverize through supersonic airstream once more drying, form smelling removal submicron Margarita powder with regular geometric shapes; Wherein, particle diameter is 75% at 0.1 micron to 1 micron accumulative perception.
Claims (7)
1. the method for preparing with regular geometric shapes smelling removal submicron Margarita powder is characterized in that this method comprises the steps:
1. once pulverize: high quality pearl is adopted the beater grinder coarse pulverization, be crushed to 1000～2000 orders through supersonic jet mill behind 200 mesh sieves excessively;
2. crack processing: import deionized water in the Margarita powder after once pulverizing, put into pressurizer, reduce pressure at last, crack Margarita powder through continuing supercharging;
3. the secondary submicron is pulverized: adopt the compound pulverizing of flexible multidimensional field of force technology that the Margarita powder that cracks after the processing is carried out the submicron pulverizing, adopting the patent No. is that 200820164741.3 disclosed grinding discs are installed in and realize the compound pulverizing of the flexible multidimensional field of force on the micropowder milling apparatus; Make particle diameter at 0.1 micron to 1 micron submicron Margarita powder suspension with regular geometric shapes;
4. taste removal: in submicron Margarita powder suspension, add flavor guide, flavor guide is selected in ethanol and ethyl acetate and their aqueous solution one or more for use; The submicron Margarita powder suspension that is added with flavor guide is inserted efficient ventilation drying device,, remove the off-flavors in the Margarita powder through the outer circulation ventilation;
5. pulverize for three times: go the submicron Margarita powder body after the raw meat to pulverize through supersonic airstream once more drying; Formation has the smelling removal Margarita powder of regular geometric shapes, and particle diameter is 20%～100% at 0.1 micron to 1 micron submicron Margarita powder content in the Margarita powder.
2. a kind of method for preparing according to claim 1 with regular geometric shapes smelling removal submicron Margarita powder; It is characterized in that: the 2. described weight that cracks the deionized water that adds in the treatment process of step is 5%～15% of Margarita powder weight, and institute's plus-pressure scope is 0.1MP to 1MP.
3. a kind of method for preparing with regular geometric shapes smelling removal submicron Margarita powder according to claim 2, it is characterized in that: lasting pressurization time is 3～12 hours.
4. a kind of method for preparing with regular geometric shapes smelling removal submicron Margarita powder according to claim 1 is characterized in that: the 3. described secondary submicron of step pulverizing process Central Asia micron pearl powder suspension concentration is 30%～45%.
5. a kind of method for preparing according to claim 1 with regular geometric shapes smelling removal submicron Margarita powder, it is characterized in that: flavor guide is an edible ethanol, addition is 1%～5% of a submicron Margarita powder suspension quality.
6. a kind of method for preparing with regular geometric shapes smelling removal submicron Margarita powder according to claim 1 is characterized in that: particle diameter is 20%～80% at 0.1 micron to 0.5 micron accumulative perception in the smelling removal submicron Margarita powder with regular geometric shapes after 5. step is pulverized for three times.
7. one kind has regular geometric shapes smelling removal submicron Margarita powder, it is characterized in that: this Margarita powder adopts any described method for preparing of claim of claim 1～6 to prepare.
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| CN106619727A (en) * | 2016-11-28 | 2017-05-10 | 湖州珍露生物制品有限公司 | Pearl powder and preparation method thereof |
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| CN105476946B (en) * | 2015-12-22 | 2018-05-08 | 浙江工业大学 | A kind of preparation method of deodorization pearl powder |
| CN113876682B (en) * | 2021-10-11 | 2023-11-03 | 欧诗漫生物股份有限公司 | Pearl powder self-foaming cleansing composition and preparation method and application thereof |
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| CN1165316C (en) * | 2001-11-13 | 2004-09-08 | 浙江大学 | Method for preparing nanometer level pearli powder |
| CN1251691C (en) * | 2003-04-30 | 2006-04-19 | 北京自然爱康生物技术发展有限公司 | Nano-scale pearl powder preparation method |
| CN101695504B (en) * | 2009-10-19 | 2011-08-31 | 海南京润珍珠生物技术股份有限公司 | Preparation method of nanometer pearl powder |
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| CN106619727A (en) * | 2016-11-28 | 2017-05-10 | 湖州珍露生物制品有限公司 | Pearl powder and preparation method thereof |
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