CN101961350B - Preparation method of fishy smell-removed pearl powder - Google Patents
Preparation method of fishy smell-removed pearl powder Download PDFInfo
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- 238000002360 preparation method Methods 0.000 title claims abstract description 4
- 238000000034 method Methods 0.000 claims abstract description 36
- 239000000725 suspension Substances 0.000 claims abstract description 26
- 238000001035 drying Methods 0.000 claims abstract description 12
- 235000005956 Cosmos caudatus Nutrition 0.000 claims description 101
- 244000293323 Cosmos caudatus Species 0.000 claims description 101
- 239000000796 flavoring agent Substances 0.000 claims description 25
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 235000019634 flavors Nutrition 0.000 claims description 14
- 238000010298 pulverizing process Methods 0.000 claims description 12
- 238000005516 engineering process Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000008367 deionised water Substances 0.000 claims description 7
- 229910021641 deionized water Inorganic materials 0.000 claims description 7
- 238000009423 ventilation Methods 0.000 claims description 7
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 4
- 230000008676 import Effects 0.000 claims description 3
- 230000002045 lasting effect Effects 0.000 claims description 3
- 235000020995 raw meat Nutrition 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- 239000002537 cosmetic Substances 0.000 abstract description 5
- 238000003672 processing method Methods 0.000 abstract description 3
- 239000011049 pearl Substances 0.000 abstract 12
- 239000003795 chemical substances by application Substances 0.000 abstract 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 239000002245 particle Substances 0.000 description 6
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 5
- 230000036541 health Effects 0.000 description 5
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- RGHNJXZEOKUKBD-SQOUGZDYSA-N Gluconic acid Natural products OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 3
- 230000003851 biochemical process Effects 0.000 description 3
- 239000000084 colloidal system Substances 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000001788 irregular Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 230000003796 beauty Effects 0.000 description 2
- 239000000174 gluconic acid Substances 0.000 description 2
- 235000012208 gluconic acid Nutrition 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000005469 granulation Methods 0.000 description 2
- 230000003179 granulation Effects 0.000 description 2
- 239000004310 lactic acid Substances 0.000 description 2
- 235000014655 lactic acid Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 241000201295 Euphrasia Species 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 241000475481 Nebula Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
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- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 150000001669 calcium Chemical class 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
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- 239000002075 main ingredient Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
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- 239000000203 mixture Substances 0.000 description 1
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- 230000035764 nutrition Effects 0.000 description 1
- 238000000643 oven drying Methods 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 238000009700 powder processing Methods 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
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Abstract
The invention relates to a processing method of high-grade cosmetics, health-care products and medicinal pearl powder, in particular to a preparation method of fishy smell-removed pearl powder. The method comprises the following steps of: crushing pearls, preparing a pearl powder suspension, adding a taste guiding agent into the pearl powder suspension, adding the pearl powder suspension with the taste guiding agent into a high-efficiency air exchange drying device, removing the fishy smell from the pearl powder through external circulation air exchange, and crushing the dried and smell-removed pearl powder again to form the smell-removed pearl powder. The taste guiding agent is added in the drying process and the high-efficiency air exchange drying device is adopted, so that the fishy smell is removed from the pearl powder and the dried pearl powder is fluffy and is easy to be crushed into submicron pearl powder with regular geometrical shapes again.
Description
Technical field
The present invention relates to the processing method of a kind of cosmetics of super quality, health product, pharmaceutical Margarita powder, relate in particular to a kind of method for preparing of smelling removal Margarita powder.
Background technology
Margarita is a kind of jewelry adornment of top grade, still a kind of famous and precious Chinese crude drug, cosmetics and nutrient and healthcare products, its medicinal health and beauty functions as far back as Ming Dynasty's Compendium of Material Medica that Li Shizhen (1518-1593 A.D.) is shown roll up four or six and other medical ancient books and records in just on the books.Cure the disease in the existing very long history of China with the Margarita powder aesthetic health care.Through the modern science analysis; Margarita not only contains aminoacid, the trace element more than 20 kinds that surpasses more than 17 kinds; But also containing a large amount of biologically actived calcium, it takes orally has: effects such as tranquillizing and allaying excitement, heat-clearing and toxic substances removing, relieving cough and resolving phlegm, hemostasia and promoting granulation, the nebula that makes eye bright; External then has: looks improving and the skin nourishing, whitening and speckle dispelling, dispel dead bark, restrain granulation promoting, separate pox and treat effects such as poison.
Improving constantly of Along with people's material and cultural life, more and more to the demand of cosmetics and nutrient and healthcare products, require also increasingly high to product quality; Margarita powder has limited the product scope of application because of receiving the influence of product fineness, though along with the application of nanotechnology in the field of Margarita processing; This problem is resolved; But new problem also occurs thereupon, mainly is: one, the nanometer Margarita powder on the present market causes darkening because of its grain shape is irregular; Two, owing to have the irregular of nanometer Margarita powder grain shape now, limited of the application of more new and high technologies such as liposomal in Margarita deep processing field; Three, the inherent off-flavors of Margarita powder is effectively solved; Four, possibly there is potential hazard in particle diameter to human body less than the nanoparticle of 100 nanometers.
Existing processing method to nanometer Margarita powder roughly has following several kinds: one, physics method; Through applying external force; Destroy the concentric laminated construction that Margarita has, use mechanical efficiently case of wet attrition method (nano-pulverization) then, make through carrying out the secondary depolymerization behind the oven drying; Two, biochemical process carries out acidolysis through adding lactic acid or dilute hydrochloric acid to the super-fine pearl powder powder, adopts sol-gel technology and spray drying technology to make.Biochemical process has not only changed the Main Ingredients and Appearance of Margarita, and has destroyed effective effect, though the physics method has been avoided the weak point of biochemical process; But because the nanometer Margarita powder grain shape that makes is irregular; Influence reflection of light, cause Margarita powder to darken, and do not remove the off-flavors of Margarita; Also can't guarantee the being perfectly safe property of product, therefore having limited it is applied to the scope of application of the cosmetics of super quality, health product and medicine.
Chinese invention patent (application number: 01132213.6; The applying date: the 2001-11-13) method for preparing of disclosed a kind of nanometer pearl powder, this method are to be that solvent dissolves Margarita with the lactic acid aqueous solution, and the pH value of adjustment solution is to neutral; Hydrolyzed pearl solution is processed colloid; Make Margarita powder on grain size, reach nanoscale, adopt spray drying will make the rapid draing of hydrolyzed pearl colloid, solidify pelletize, process the Margarita powder that sphere, mean diameter are of a size of the 90-100 nanometer.Prepared nanometer Margarita powder has kept effectively nutritional labeling such as the several amino acids in the Margarita, trace element, and makes the calcium carbonate in the Margarita be converted into the easy activated calcium for absorbing of human body.This method efficient is high, energy consumption is little, and production cost is lower, is applicable to the suitability for industrialized production of medicine, nutrition and health and beauty care product.
Chinese invention patent (application number: 03153808.8; The applying date: 2003-08-22) disclose the method for preparing of nanometer pearl powder; This method is broken into 300～500 purpose fine powders with Margarita powder earlier, adds the deionized water in 4～19 times of weight portions, processes suspension; Place high pressure homogenizer to pulverize pearl suspension again, obtain the Margarita powder of particle diameter in 50～100 nanometers.This method does not change composition and the structure of Margarita, helps absorption of human body, and technology is simple, is easy to suitability for industrialized production.
Chinese invention patent (application number: 03122900.X, the applying date: this method of method for preparing that 2003-04-30) discloses nanometer pearl powder is that to adopt high pressure homogenizer that crushing pearl is become particle diameter earlier be 2～5 microns granule; And then to use concentration be citric acid or the gluconic acid aqueous solution dissolved pearl granule of 30～50wt%, and obtaining concentration is the pearl powder solution of 20～3wt%; With sodium bicarbonate the pH value of step (2) hydrolyzed pearl powder solution is adjusted to neutrality, at room temperature leaves standstill, obtain the Margarita powder colloid, drying is solidified pelletize, particle diameter be 50～90 nanometer Margarita powders.This method is pulverized Margarita owing to first, and then adopts citric acid or gluconic acid aqueous solution to disperse, and has shortened the time that obtains nanometer Margarita powder, has improved specific duty.
Above-mentioned crushing pearl technology is not all considered the problem that the off-flavors of Margarita is removed, and it is a difficult problem of puzzlement Margarita powder processing industry that the off-flavors of Margarita is removed all the time.
Summary of the invention
Can't effectively dispel the weak point of Margarita off-flavors in order to solve existing Margarita powder technology of preparing; The method for preparing that the purpose of this invention is to provide a kind of smelling removal Margarita powder; This method has effectively been dispeled the Margarita off-flavors, can make the Margarita powder range of application wider, and Product Safety is higher.
In order to realize above-mentioned purpose, the technical scheme below the present invention has adopted.
A kind of method for preparing of smelling removal Margarita powder; This method comprises crushing pearl operation and Margarita powder suspension preparation section, with adding flavor guide in the Margarita powder suspension, the Margarita powder suspension that is added with flavor guide is inserted efficient ventilation drying device; Through the outer circulation ventilation; Remove the off-flavors in the Margarita powder, go the Margarita powder body after the raw meat to pulverize once more drying, form the Margarita powder of smelling removal.
Flavor guide of the present invention for dissolve each other with water and harmless and not with the organic solvent of Margarita powder reaction, as preferably, flavor guide is selected in ethanol, ethyl acetate and their aqueous solution one or more for use.Preferred as again, described flavor guide is selected edible ethanol for use.The addition of edible ethanol is 1%～5% of a Margarita powder suspension quality.
As preferably, 20%～50% of said Margarita powder suspension, Margarita powder are superfine powder.Preferred as again, 30%～45% of described Margarita powder suspension, Margarita powder are micron order or submicron order.
As preferably, the method for preparing of said Margarita powder suspension is following:
1. once pulverize: high quality pearl is adopted the beater grinder coarse pulverization, be crushed to 1000～2000 orders through supersonic jet mill behind 200 mesh sieves excessively;
2. crack processing: import deionized water in the Margarita powder after once pulverizing, put into pressurizer, reduce pressure at last, crack Margarita powder through continuing supercharging;
3. the secondary submicron is pulverized: adopt the compound pulverizing of flexible multidimensional field of force technology that the Margarita powder that cracks after the processing is pulverized, make the Margarita powder suspension.
Preferred as again, the 2. described weight that cracks the deionized water that adds in the treatment process of step is 5%～15% of Margarita powder weight, and institute's plus-pressure scope is 0.1MP to 1MP, and lasting pressurization time is 3～12 hours.
The present invention and the off-flavors that has to Margarita; Pass through to add flavor guide in the drying process link; Adopt efficient outer circulation ventilation drying device; Not only removed the off-flavors in the Margarita, but also made dried Margarita powder body be puffy, be easy to be again crushed into submicron Margarita powder with regular geometric shapes.
The specific embodiment
A kind of method for preparing of smelling removal Margarita powder, this method comprises the steps.
(1) selects the former pearl of high-quality: select and culture in pollution-free waters and content of beary metal such as lead, arsenic, hydrargyrum meet the high quality pearl of the provisions of the relevant regulations issued by the State.
(2) once pulverize: high quality pearl is adopted the beater grinder coarse pulverization, be crushed to 1000～2000 orders through supersonic jet mill behind 200 mesh sieves excessively.
(3) crack processing: import deionized water in the Margarita powder after once pulverizing, the weight of deionized water is 10% of Margarita powder weight, puts into pressurizer; Through moment supercharging decompression; Institute's plus-pressure scope is 0.1MP to 1MP, and lasting pressurization time is 6 hours, cracks Margarita powder.
(4) the secondary submicron is pulverized: adopt the compound pulverizing of flexible multidimensional field of force technology that the Margarita powder that cracks after the processing is carried out the submicron pulverizing; Make particle diameter at 0.1 micron to the 1 micron submicron Margarita powder suspension with regular geometric shapes, submicron Margarita powder suspension concentration is 35%; It is that 200820164740.9 or 200820164741.3 disclosed grinding discs are installed in the compound pulverizing of the flexible multidimensional of the realization field of force on the micropowder milling apparatus that the present invention can adopt the patent No..
(6) taste removal: in submicron Margarita powder suspension, add flavor guide; Flavor guide is an edible ethanol; Addition is 3.5% of a submicron Margarita powder suspension quality; The submicron Margarita powder suspension that is added with flavor guide is inserted efficient ventilation drying device,, remove the off-flavors in the Margarita powder through the outer circulation ventilation.
Pulverize for (6) three times: go the submicron Margarita powder body after the raw meat to pulverize through supersonic airstream once more drying, form smelling removal submicron Margarita powder with regular geometric shapes; Wherein, particle diameter is 75% at 0.1 micron to 1 micron Margarita powder accumulative perception.
Claims (8)
1. the method for preparing of a smelling removal Margarita powder; This method comprises crushing pearl operation and Margarita powder suspension preparation section; It is characterized in that: with adding flavor guide in the Margarita powder suspension, described flavor guide for dissolve each other with water and harmless and not with the organic solvent of Margarita powder reaction; The Margarita powder suspension that is added with flavor guide is inserted efficient ventilation drying device,, remove the off-flavors in the Margarita powder, go the Margarita powder body after the raw meat to pulverize once more drying, form the Margarita powder of smelling removal through outer circulation ventilation; Described flavor guide is selected in ethanol, ethyl acetate and their aqueous solution one or more for use.
2. the method for preparing of a kind of smelling removal Margarita powder according to claim 1 is characterized in that: flavor guide is selected edible ethanol for use.
3. the method for preparing of a kind of smelling removal Margarita powder according to claim 2 is characterized in that: the addition of edible ethanol is 1%～5% of a Margarita powder suspension quality.
4. according to the method for preparing of any described a kind of smelling removal Margarita powder of claim of claim 1～3, it is characterized in that: 20%～50% Margarita powder of Margarita powder suspension is a superfine powder.
5. the method for preparing of a kind of smelling removal Margarita powder according to claim 4 is characterized in that: 30%～45% Margarita powder of Margarita powder suspension is micron order or submicron order.
6. the method for preparing of a kind of smelling removal Margarita powder according to claim 4 is characterized in that the method for preparing of Margarita powder suspension is following:
1. once pulverize: high quality pearl is adopted the beater grinder coarse pulverization, be crushed to 1000～2000 orders through supersonic jet mill behind 200 mesh sieves excessively;
2. crack processing: import deionized water in the Margarita powder after once pulverizing, put into pressurizer, reduce pressure at last, crack Margarita powder through continuing supercharging;
3. the secondary submicron is pulverized: adopt the compound pulverizing of flexible multidimensional field of force technology that the Margarita powder that cracks after the processing is pulverized, make the Margarita powder suspension.
7. the method for preparing of a kind of smelling removal Margarita powder according to claim 6 is characterized in that: the 2. described weight that cracks the deionized water that adds in the treatment process of step is 5%～15% of Margarita powder weight, and institute's plus-pressure scope is 0.1MP to 1MP.
8. a kind of method for preparing with regular geometric shapes smelling removal submicron Margarita powder according to claim 6, it is characterized in that: lasting pressurization time is 3～12 hours.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106619727A (en) * | 2016-11-28 | 2017-05-10 | 湖州珍露生物制品有限公司 | Pearl powder and preparation method thereof |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105250192A (en) * | 2015-10-01 | 2016-01-20 | 常州市奥普泰科光电有限公司 | Preparing method for nanoscale pure white pearl powder fishy smell |
| CN105476946B (en) * | 2015-12-22 | 2018-05-08 | 浙江工业大学 | A kind of preparation method of deodorization pearl powder |
| CN110432488A (en) * | 2019-09-16 | 2019-11-12 | 海南京润珍珠科技有限公司 | A kind of preparation method of deodorization pearl powder |
| CN114403437A (en) * | 2022-01-27 | 2022-04-29 | 海南久常制药有限公司 | A method for preparing Margarita powder |
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|---|---|---|---|---|
| CN1182594A (en) * | 1997-12-10 | 1998-05-27 | 单佩南 | Method for producing extracted powder by pearl nucleus-removing and technology and device thereof |
| CN1582966A (en) * | 2003-08-22 | 2005-02-23 | 中科纳米技术工程中心有限公司 | Preparation of nano pearls powder |
| CN1813806A (en) * | 2005-12-12 | 2006-08-09 | 浙江东豪集团股份有限公司 | Nano-level chelate pearl product, and its production process and use |
| CN1875989A (en) * | 2006-01-17 | 2006-12-13 | 李伊为 | A method for preparing nano-grade pure pearl powder |
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2010
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1182594A (en) * | 1997-12-10 | 1998-05-27 | 单佩南 | Method for producing extracted powder by pearl nucleus-removing and technology and device thereof |
| CN1582966A (en) * | 2003-08-22 | 2005-02-23 | 中科纳米技术工程中心有限公司 | Preparation of nano pearls powder |
| CN1813806A (en) * | 2005-12-12 | 2006-08-09 | 浙江东豪集团股份有限公司 | Nano-level chelate pearl product, and its production process and use |
| CN1875989A (en) * | 2006-01-17 | 2006-12-13 | 李伊为 | A method for preparing nano-grade pure pearl powder |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106619727A (en) * | 2016-11-28 | 2017-05-10 | 湖州珍露生物制品有限公司 | Pearl powder and preparation method thereof |
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Denomination of invention: A preparation method of deodorized pearl powder Effective date of registration: 20210729 Granted publication date: 20120530 Pledgee: Agricultural Bank of China Limited Deqing County sub branch Pledgor: OSM Biology Co.,Ltd. Registration number: Y2021330001041 |
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