CN101952199B - 聚合物材料离散固体粒子的制备 - Google Patents
聚合物材料离散固体粒子的制备 Download PDFInfo
- Publication number
- CN101952199B CN101952199B CN200780037656.9A CN200780037656A CN101952199B CN 101952199 B CN101952199 B CN 101952199B CN 200780037656 A CN200780037656 A CN 200780037656A CN 101952199 B CN101952199 B CN 101952199B
- Authority
- CN
- China
- Prior art keywords
- stream
- droplet
- beads
- dispersion medium
- polymerization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/12—Polymerisation in non-solvents
- C08F2/16—Aqueous medium
- C08F2/18—Suspension polymerisation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/318—Preparation characterised by the starting materials
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/336—Preparation characterised by gaseous activating agents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/342—Preparation characterised by non-gaseous activating agents
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/44—Polymerisation in the presence of compounding ingredients, e.g. plasticisers, dyestuffs, fillers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/14—Treatment of polymer emulsions
- C08F6/16—Purification
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/14—Powdering or granulating by precipitation from solutions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0083—Nucleating agents promoting the crystallisation of the polymer matrix
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/13—Phenols; Phenolates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Materials Engineering (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Polymerisation Methods In General (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB0619974.9 | 2006-10-09 | ||
| GB0619974A GB0619974D0 (en) | 2006-10-09 | 2006-10-09 | Process |
| GB0710007.6 | 2007-05-24 | ||
| GBGB0710007.6A GB0710007D0 (en) | 2007-05-24 | 2007-05-24 | Process |
| PCT/GB2007/003759 WO2008043983A2 (en) | 2006-10-09 | 2007-10-04 | Making discrete solid particles of polymeric material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101952199A CN101952199A (zh) | 2011-01-19 |
| CN101952199B true CN101952199B (zh) | 2014-09-17 |
Family
ID=38969316
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200780037656.9A Expired - Fee Related CN101952199B (zh) | 2006-10-09 | 2007-10-04 | 聚合物材料离散固体粒子的制备 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8383703B2 (enExample) |
| EP (1) | EP2054342B1 (enExample) |
| JP (2) | JP5358443B2 (enExample) |
| KR (1) | KR101482283B1 (enExample) |
| CN (1) | CN101952199B (enExample) |
| AR (1) | AR063179A1 (enExample) |
| BR (1) | BRPI0719161A2 (enExample) |
| CA (1) | CA2665052C (enExample) |
| RU (1) | RU2466931C2 (enExample) |
| WO (1) | WO2008043983A2 (enExample) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8119555B2 (en) | 2008-11-20 | 2012-02-21 | R. J. Reynolds Tobacco Company | Carbonaceous material having modified pore structure |
| US8511319B2 (en) | 2008-11-20 | 2013-08-20 | R. J. Reynolds Tobacco Company | Adsorbent material impregnated with metal oxide component |
| EP2398959B1 (en) * | 2009-01-13 | 2013-01-23 | Biogasol ApS | Treatment, such as cutting, soaking and/or washing, of organic material |
| GB0921528D0 (en) | 2009-12-09 | 2010-01-27 | Mast Carbon Internat Ltd | Carbon and its use in blood cleansing applications |
| CN103221120B (zh) | 2010-08-19 | 2016-08-17 | 株式会社明治 | 微粒化装置 |
| CA2808572C (en) * | 2010-08-19 | 2018-04-03 | Meiji Co., Ltd. | Performance estimation method and scale-up method for particle size breakup apparatus |
| JP2012116832A (ja) * | 2010-11-11 | 2012-06-21 | Sumitomo Chemical Co Ltd | 有害生物防除成分を含有する分散液の製造方法及びマイクロカプセルの製造方法 |
| GB201204696D0 (en) | 2012-03-16 | 2012-05-02 | Ucl Business Plc | Therapy |
| GB201221227D0 (en) | 2012-11-26 | 2013-01-09 | Mast Carbon Internat Ltd | Carbon materials and their use |
| JP6505020B2 (ja) * | 2012-11-26 | 2019-04-24 | ジョージア − パシフィック ケミカルズ エルエルシー | ポリマ樹脂および炭素材料の調製 |
| GB201512468D0 (en) | 2015-07-16 | 2015-08-19 | C Tex Ltd And University Of Brighton | Shaped nanoporous bodies |
| EP3538563B1 (en) * | 2016-11-08 | 2021-07-07 | DDP Specialty Electronic Materials US, LLC | Controlled particle size distribution |
| US20210146333A1 (en) * | 2017-12-19 | 2021-05-20 | ImMutriX Therapeutics, Inc. | Tailored porosity materials and methods of making and using same |
| CN109179405A (zh) * | 2018-09-27 | 2019-01-11 | 凯瑞环保科技股份有限公司 | 一种利用废离子交换树脂制备炭化树脂的方法 |
| JP2020059765A (ja) * | 2018-10-05 | 2020-04-16 | 国立大学法人 熊本大学 | 蛍光性重合体および蛍光性重合体の製造方法、ならびに蛍光性ポリマー粒子、分散液、複合体、蛍光性重合体の被覆方法 |
| CN109850863B (zh) * | 2019-01-16 | 2020-10-13 | 浙江大学 | 一种类齿轮状介孔炭纳米球材料、制备方法及应用 |
| JP7462353B2 (ja) * | 2020-03-02 | 2024-04-05 | ミレニアル マテリアルズ アンド デバイセズ インコーポレイテッド | カーボンビーズの合成方法 |
| CN114685742B (zh) * | 2020-12-31 | 2024-03-29 | 上海昶法新材料有限公司 | 一种酚醛树脂的制备方法 |
| WO2024261472A1 (en) | 2023-06-20 | 2024-12-26 | Yaqrit Limited | Porous carbon particles for use in therapy |
| CN118788316B (zh) * | 2024-08-09 | 2025-12-02 | 中国科学院南京土壤研究所 | 一种可漂浮中空微球制备装置 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0042192A1 (en) * | 1980-06-13 | 1981-12-23 | Duolite International S.A. | Continuous production of polymer beads of controlled size |
| CN1159198A (zh) * | 1994-09-09 | 1997-09-10 | 帝国化学工业澳大利亚经营有限公司 | 聚合物珠粒及其制造方法 |
| CN1486790A (zh) * | 2002-09-05 | 2004-04-07 | 罗姆和哈斯公司 | 制备细小固体颗粒和分散体的方法 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1505517A (en) | 1919-05-05 | 1924-08-19 | John C Woodruff | Process of activating carbon |
| GB228954A (en) * | 1923-08-09 | 1925-02-09 | Johan Nicolaas Adolf Sauer | Improvements in and relating to processes for the production of active carbon |
| US3620988A (en) * | 1968-10-31 | 1971-11-16 | Goodrich Co B F | Method of preparing bead-type polymers |
| CH642564A5 (de) | 1979-10-26 | 1984-04-30 | Sulzer Ag | Statische mischvorrichtung. |
| US4344821A (en) | 1979-11-19 | 1982-08-17 | Angelo Ii James F | Apparatus for continuously carbonizing and activating carbonaceous materials |
| US4666673A (en) * | 1980-10-30 | 1987-05-19 | The Dow Chemical Company | Apparatus for preparing large quantities of uniform size drops |
| CA1166413A (en) | 1980-10-30 | 1984-05-01 | Edward E. Timm | Process and apparatus for preparing uniform size polymer beads |
| US4487898A (en) * | 1981-06-12 | 1984-12-11 | Kanegafuchi Chemical Industry Co., Ltd. | Process of continuous suspension polymerization |
| SU1610211A1 (ru) * | 1989-01-17 | 1990-11-30 | Предприятие П/Я Р-6956 | Вращающа с муфельна печь |
| KR0161286B1 (ko) * | 1989-08-08 | 1999-01-15 | 엠. 윌킨스 | 중합방법과 반응기 |
| IT1273678B (it) * | 1993-08-12 | 1997-07-09 | Bluecher Hasso Von | Processo per la produzione di carbone attivo |
| RU2085486C1 (ru) * | 1994-01-01 | 1997-07-27 | Вячеслав Евгеньевич Чиликин | Способ получения сферического углеродного адсорбента |
| DE59609690D1 (de) * | 1995-01-11 | 2002-10-24 | Mhb Filtration Gmbh & Co Kg | Verfahren zur herstellung von körniger aktivkohle |
| DE19912154C5 (de) | 1999-03-17 | 2007-02-01 | Carbotex Produktions-Und Veredelungsbetriebe Gmbh | Verfahren zur Herstellung von geformter Aktivkohle |
| DE19920794A1 (de) | 1999-05-06 | 2000-11-09 | Merck Patent Gmbh | Verfahren zur Herstellung von Perlpolymerisaten |
| EP1276694B1 (de) * | 2000-04-28 | 2004-11-24 | Blücher GmbH | Verfahren zur herstellung kugelförmiger aktivkohle |
| EP1289883B1 (de) * | 2000-05-24 | 2006-01-04 | Carbotex Produktions- und Veredelungsbetriebe GmbH | Verfahren zur herstellung von geformter aktivkohle |
| GB0019417D0 (en) | 2000-08-09 | 2000-09-27 | Mat & Separations Tech Int Ltd | Mesoporous carbons |
| JP2003171405A (ja) * | 2001-12-04 | 2003-06-20 | Sekisui Chem Co Ltd | 樹脂微粒子の製造装置、および、この製造装置を用いた樹脂微粒子の製造方法 |
| AU2003259124A1 (en) | 2002-07-15 | 2004-02-02 | Sulzer Chemtech Usa, Inc. | Assembly of crossing elements and method of constructing same |
| US6610798B1 (en) * | 2002-10-08 | 2003-08-26 | Nova Chemical Inc. | Controlled suspension polymerization process without mechanical agitation |
| JP2005255910A (ja) * | 2004-03-12 | 2005-09-22 | Hitachi Chem Co Ltd | 高分子粒子分散物とその製造方法 |
| US6943223B1 (en) * | 2004-04-27 | 2005-09-13 | Nova Chemicals Inc. | Controlled shear and turbulence flow pattern within a liquid in a vessel |
| GB0506278D0 (en) * | 2005-03-29 | 2005-05-04 | British American Tobacco Co | Porous carbon materials and smoking articles and smoke filters therefor incorporating such materials |
| US20090273105A1 (en) * | 2005-05-23 | 2009-11-05 | Cornell Research Foundation | Method and system for performing an interfacial reaction in a microfluidic device |
-
2007
- 2007-10-04 RU RU2009117384/04A patent/RU2466931C2/ru not_active IP Right Cessation
- 2007-10-04 WO PCT/GB2007/003759 patent/WO2008043983A2/en not_active Ceased
- 2007-10-04 CN CN200780037656.9A patent/CN101952199B/zh not_active Expired - Fee Related
- 2007-10-04 US US12/444,839 patent/US8383703B2/en not_active Expired - Fee Related
- 2007-10-04 KR KR1020097009577A patent/KR101482283B1/ko not_active Expired - Fee Related
- 2007-10-04 JP JP2009531895A patent/JP5358443B2/ja not_active Expired - Fee Related
- 2007-10-04 CA CA2665052A patent/CA2665052C/en not_active Expired - Fee Related
- 2007-10-04 EP EP07824015.7A patent/EP2054342B1/en not_active Not-in-force
- 2007-10-04 BR BRPI0719161-8A patent/BRPI0719161A2/pt not_active IP Right Cessation
- 2007-10-09 AR ARP070104458A patent/AR063179A1/es not_active Application Discontinuation
-
2013
- 2013-06-28 JP JP2013136644A patent/JP2013241605A/ja active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0042192A1 (en) * | 1980-06-13 | 1981-12-23 | Duolite International S.A. | Continuous production of polymer beads of controlled size |
| CN1159198A (zh) * | 1994-09-09 | 1997-09-10 | 帝国化学工业澳大利亚经营有限公司 | 聚合物珠粒及其制造方法 |
| CN1486790A (zh) * | 2002-09-05 | 2004-04-07 | 罗姆和哈斯公司 | 制备细小固体颗粒和分散体的方法 |
Non-Patent Citations (1)
| Title |
|---|
| J. M. ZALC et al..Mixing dynamics in the SMX static mixer as a function of injection location and flow ratio.《polymer engineering and science》.2003,第43卷(第4期),第875页-第890页. * |
Also Published As
| Publication number | Publication date |
|---|---|
| RU2009117384A (ru) | 2010-11-20 |
| CA2665052C (en) | 2014-12-09 |
| EP2054342B1 (en) | 2019-07-31 |
| KR101482283B1 (ko) | 2015-01-13 |
| KR20090081383A (ko) | 2009-07-28 |
| JP2013241605A (ja) | 2013-12-05 |
| EP2054342A2 (en) | 2009-05-06 |
| CN101952199A (zh) | 2011-01-19 |
| JP5358443B2 (ja) | 2013-12-04 |
| BRPI0719161A2 (pt) | 2014-02-04 |
| US20100086469A1 (en) | 2010-04-08 |
| JP2010511064A (ja) | 2010-04-08 |
| WO2008043983A2 (en) | 2008-04-17 |
| RU2466931C2 (ru) | 2012-11-20 |
| WO2008043983A3 (en) | 2010-03-25 |
| US8383703B2 (en) | 2013-02-26 |
| AR063179A1 (es) | 2008-12-30 |
| CA2665052A1 (en) | 2008-04-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140917 Termination date: 20191004 |