CN101919852A - In vitro anti-insect spray for pets and preparation and using methods thereof - Google Patents
In vitro anti-insect spray for pets and preparation and using methods thereof Download PDFInfo
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- CN101919852A CN101919852A CN2010101084129A CN201010108412A CN101919852A CN 101919852 A CN101919852 A CN 101919852A CN 2010101084129 A CN2010101084129 A CN 2010101084129A CN 201010108412 A CN201010108412 A CN 201010108412A CN 101919852 A CN101919852 A CN 101919852A
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Abstract
The invention discloses an in vitro anti-insect spray for pets and preparation and using methods thereof. The in vitro anti-insect spray for pets comprises 0.1 to 70 weight parts of insecticidal active ingredient and 15 to 170 weight parts of aid, wherein the insecticidal active ingredient is a mixture of rotenone and chlorantraniliprole. The in vitro anti-insect spray for pets is directly sprayed to the pets or ambient environment, and is used for killing external parasites which are parasitic on the pets or potential injurious insects in the ambient environment of the pets. The in vitro anti-insect spray for pets is convenient to use, and has obvious effect of preventing and controlling the external parasites of livestock or the pets, such as tick, flea, louse and mite.
Description
Technical field
The invention belongs to washing and insecticidal technology field, relate to a kind of the pet body epizoa is had prevent and the medicament of killing action, especially relate to a kind of vitro anti-insect spray for pets and preparation thereof and using method.
Background technology
Along with the acceleration of Chinese society expanding economy and urbanization process, the upsurge of raising pets is surging forward in China city.Especially since 2004, the house pet industry development impetus of China is swift and violent.According to conservative estimation, the number of animals raised of pet dog only, the whole nation just has nearly 1,000 ten thousand.
According to investigations, have from consumer on the proportion of house pet, the accessed object of pet feeding Canis familiaris L. accounts for 36.8% of pet feeding family, the pet feeding cat account for 22.4% of pet feeding family, this shows that pet dog and cat are the main house pet types that China raises.
Because the hair of Canis familiaris L. and cat is abundant, long-term again kiss the earth, thereby be subject to parasitic invasions such as louse, flea, demodicid mite, easily suffer from fungoid and bacteroidal dermatosis, as eczema, dermatitis, skin pruritus etc.Simultaneously, Canis familiaris L. and cat are all liked wide space, and the nature of strolling are arranged away, and they miss potter ground activities such as meadow, shrub, rubbish heap, and these places are concentrated infection districts of flea, cattle Ticks, louse, infectious disease.Spring, summer, warm, moist weather provided the chance of breeding for insecticides such as flea, tick, acarians.Secondly, in China big and medium-sized cities, the common people about 85% stay in the apartment type house, the space is limited, therefore in the park or the public recreating facility of sub-district often can see owner with loved house pet stroll with stroll, these cats and Canis familiaris L., when kiss the earth or other infected article, or in the mutual process of playing, play may self with vermin and germina infection give other house pet.Owner when getting close to house pet, house pet also may be some sick and worm infect to the mankind, thereby form the disease of infecting both domestic animals and human, as acarid, acarid is that house pet is carried the vermin of returning when playing outside easily, but immediate contagion is given the mankind.And cat scratch disease is to propagate the bacterial infectious disease that Bartonellaehenselae causes by cat flea between cat, and the mankind can be by directly or indirectly contact is infected.
Vermiform mite, acaricide, Ticks, flea are the common several ectozoaes of cat, dog, and wherein vermiform mite is run the endobiosis life concurrently.These several parasites are not only caused direct infringement to pet body, but also are the communication medias of some disease pathogen.
At present, domestic and international main method to external parasite preventing and treatings such as cattle Ticks, flea, demodicid mites is that chemosynthesis medicaments such as subcutaneous injection avilamycin and ivermectin etc., external use fluorine worm cyanogen, phoxim, coumafos, metrifonate are mixed with the bathing of house pet with medicament, medicine liquid spray and drop etc.These products have effect preferably to the part vermin of house pet, but price is all quite expensive, and part organophosphorus pesticide toxicity is higher, and are dangerous to house pet.
Summary of the invention
The objective of the invention is to remedy the deficiencies in the prior art, a kind of vitro anti-insect spray for pets is provided, safe and effective, especially to cattle Ticks, acarid, flea and louse earlier etc. the common vermin of house pet have the medicament of prevention and killing action, and easy to use, have no side effect.
Another object of the present invention provides the preparation method of described spray.
Purpose of the present invention is achieved by following technical proposals:
A kind of vitro anti-insect spray for pets is provided,, comprises other adjuvant of 0.1～70 part of active insecticidal components and 15～170 parts according to the parts by weight meter.
Described active insecticidal components is the mixture of rotenone (rotenone) and Rynaxypyr (chlorantraniliprole), mixed proportion is that the mass ratio of rotenone and Rynaxypyr is 1～40: 1～40, the mass ratio that preferred mixed proportion is rotenone and Rynaxypyr is 1～10: 1～10, and more preferred version is that the mass ratio of rotenone and fluorine worm nitrile Rynaxypyr is 1～7: 1～7.
Described adjuvant comprises several in organic solvent, surfactant, antifreezing agent, anti-photodissociation agent, stabilizing agent, antioxidant or the dispersant.The ratio of weight and number of described various adjuvant is:
Organic solvent: surfactant (or emulsifying agent): antifreezing agent: anti-photodissociation agent: stabilizing agent: antioxidant: dispersant=1～30 part: 2～20 parts: 1～10 part: 1～10 part: 1～10 part: 0.5～10 part: 10～80 parts.
Described organic solvent is selected from one or more of following substances: methanol, acetone, Ketohexamethylene, N, dinethylformamide, dimethyl sulfoxide, N-Methyl pyrrolidone, DMC dimethyl carbonate, isobutanol, isobutyl acetate, benzene, dimethylbenzene, naphthalane, gasoline, kerosene, machine oil, propylene glycol, propylene glycol, petroleum ether, Oleum Cinnamomi, eucalyptus oil, citronella oil, Oleum lavandula angustifolia, Sassafras oil, linalool, Fructus Coriandri oil or Semen Sinapis wet goods.
Described emulsifying agent or surfactant are selected from one or more of following substances: NPE, or calcium dodecyl benzene sulfonate, or alkyl polyoxyethylene ether phosphate ester, or alkyl polyoxypropylene ether phosphate, or NPE phosphate ester, or fatty alcohol-polyoxyethylene ether series (AEO), or C12 alkyl (EO) 3 ether sodium sulfates (AES), or olefin sulfonic acid (AOS), or lauric acid amide of ethanol (6501), or styryl phenyl polyoxyethylene ether, or castor oil polyoxyethylene ether, or one or more mixture in the surfactant materials known altogether of this area staff.
Described antifreezing agent is selected from one or more of following substances: ethylene glycol, glycerol, sorbitol or ethanol.
Described anti-photodissociation agent is selected from one or more of following substances: amino this formic acid, Oleum Ricini, pyrogallic acid, citric acid, lignosulfonates, UV-P (2-(2 '-hydroxyl-5 '-aminomethyl phenyl) benzotriazole), BP-12 (are had another name called UV-531, Octabenzone,) or BP-3 (having another name called UV-9,2-hydroxyl-4-methoxy benzophenone).
Described stabilizing agent is selected from one or more of following substances: epoxidized soybean oil, pyrogallol, sodium sorbate, sodium benzoate, eugenol, citric acid, pyrogallic acid are sad, Oleum Ricini, salicylic acid, olive oil or epoxidized linseed.
Described antioxidant is selected from one or more of following compositions: vitamin E, vitamin C, beta-carotene, BHA (Butylated hydroxyanisole), BHT (2,6 ditertiary butyl p cresol), citric acid, methoxybenzene or P-hydroxybenzoic acid.
Described dispersant is selected from one or more of following compositions: ethanol, ethyl acetate or deionized water.
Preferably, vitro anti-insect spray for pets comprises each components of following parts by weight:
Active insecticidal components: organic solvent: surfactant: antifreezing agent: anti-photodissociation agent: stabilizing agent: antioxidant: dispersant=0.1～50 part: 1～30 part: 1～20 part: 1～10 part: 0.1～10 part: 1～10 part: 0.1～10 part: 10～80 parts.
The present invention provides the preparation method of described vitro anti-insect spray for pets simultaneously, earlier with the former powder of rotenone or crystal and the former medicinal solvent dissolving of Rynaxypyr, adding surfactant stirs, adding dispersant in proportion mixes, add antifreezing agent, anti-photodissociation agent, stabilizing agent, antioxidant and dispersant then successively, stir while adding evenly.
The using method of spray of the present invention is: hold this product during use, apart from 10～20 centimetres of house pet vertical dimensions, contrary tippy tea direction begins spray gently, to the whole house pet health of spraying covering.In the process of spray, note mobile containers, make spray can evenly cover animal skin, till animal skin tippy tea portion humidity, gently grab fur and touch pet skin by spray.Perhaps directly spray of the present invention is sprayed on house pet life and active environment.
The invention has the beneficial effects as follows:
Rotenone and Rynaxypyr are mixed and can increase drug effect any technology report is not arranged as yet, more rotenone and fluorine worm nitrile Rynaxypyr are not mixed and are applied to kill the ectozoic reports of pet body such as demodicid mite, Ticks, flea, louse as the effective active composition, the present invention discovers, adopt suitable proportioning, rotenone and fluorine worm nitrile Rynaxypyr mixture are applied to house pet, the pet body epizoa had good toxic effect, both are mixed to use and can reduce dosage, increase drug effect; Widen the scope of application of medicament, delay pest resistance to insecticide and take place.
The outer parasite killing spray of pet body of the present invention selects for use the mixture of rotenone (rotenone) and low toxicity ultra high efficiency insecticide Rynaxypyr (chlorantraniliprole) to add that suitable adjuvant prepares, to ectozoic prevention of pet body and killing effect excellences such as cattle Ticks, acarids, its preferred component proportioning is that the commercially available outer antiparasitic agents of the pet body with effective ingredient such as chlorine worm nitrile, Imidacloprid, ivermectins is more excellent to the ectozoic prevention of pet bodies such as cattle Ticks and killing effect.Spray of the present invention is easy to use, and good disinsection effect is to people and pet safe.
The specific embodiment
Further describe the present invention below in conjunction with specific embodiment, but content of the present invention is not limited thereto.
Embodiment 1
According to the parts by weight meter, prepare following each component:
A component: 4 parts of the former medicines of Rynaxypyr, 0.1 part in former powder of rotenone or crystal, 5 parts of solvent methanols, 1 part of 3 parts+phenethyl of surfactant calcium dodecyl benzene sulfonate phenol polyethenoxy ether; 50 parts of dispersant ethanol.
B component: 5 parts of antifreeze glycols, 0.1 part of anti-photodissociation agent Oleum Ricini; 1 part of stabilizing agent citric acid; 1 part of antioxidant epoxidized soybean oil.
The adding essence that also can depend on actual need adds according to 0.5% of gross weight.
Preparation process is as follows:
(1) takes by weighing each component by consumption;
(2) earlier with the former powder of rotenone or crystal and the former medicinal solvent dissolving of Rynaxypyr, add emulsifying agent, dispersant successively, stir A;
(3) antifreezing agent, anti-photodissociation agent, stabilizing agent, antioxidant and essence are added among the A successively stir promptly.
The using method of vitro anti-insect spray for pets of the present invention: hold this product during use, apart from 10～20 centimetres of house pet vertical dimensions, contrary tippy tea direction begins spray gently, to the whole house pet health of spraying covering.In the process of spray, note mobile containers, make spray can evenly cover animal skin, till animal skin tippy tea portion humidity, gently grab fur and touch pet skin by spray.
Embodiment 2
According to the parts by weight meter, prepare following each component:
A component: 10 parts of the former medicines of Rynaxypyr, 1 part in former powder of rotenone or crystal, solvent N, 15 parts of dinethylformamides, 3 parts in 5 parts+triphenyl vinyl phenol of emulsifying agent triphenyl vinyl phenol polyoxyethylene poly-oxygen propylene aether polyoxyethylene polyoxypropylene ether; 40 parts of dispersant ethanol.
B component: 5 parts of antifreezing agent glycerol, anti-photodissociation agent UV-P (1 part of 2-(2 '-hydroxyl-5 '-aminomethyl phenyl); 1.5 parts of stabilizing agent citric acids; 0.5 part of antioxidant BHA (Butylated hydroxyanisole).
The adding essence that also can depend on actual need adds according to 0.5% of gross weight.Preparation method and using method are with embodiment 1.
Embodiment 3
According to the parts by weight meter, prepare following each component:
A component: 7 parts of the former medicines of Rynaxypyr, 1 part in former powder of rotenone or crystal, 12 parts of solvent dimethyl sulfoxide, 8 parts of emulsifying agent fatty alcohol-polyoxyethylene ether (AEO7); 60 parts of dispersant ethanol.
The B component: 5 parts of antifreezing agent sorbitol, anti-photodissociation agent BP-12 (has another name called UV-531, chemical name: Octabenzone) 0.6 part; 3 parts in stabilizing agent olive oil; 0.1 part of antioxidant epoxidized linseed.
The adding essence that also can depend on actual need adds according to 0.3% of gross weight.Preparation method and using method are with embodiment 1.
Embodiment 4
According to the parts by weight meter, prepare following each component:
A component: 4 parts of the former medicines of Rynaxypyr, 1 part in former powder of rotenone or crystal, 8 parts of solvent N-Methyl pyrrolidone, 7 parts of emulsifying agent styryl phenyl polyoxyethylene ether; 65 parts of dispersant ethanol.
The B component: 5 parts of antifreezing agent sorbitol, anti-photodissociation agent BP-12 (has another name called UV-531, chemical name: Octabenzone) 0.5 part; 3 parts of stabilizing agent sodium sorbates; 0.3 part of antioxidant eugenol.
The adding essence that also can depend on actual need adds according to 0.8% of gross weight.Preparation method and using method are with embodiment 1.
Embodiment 5
With the boophilus microplus is example, and present embodiment provides the different proportionings of rotenone and Rynaxypyr to the parasitic killing effect of house pet, and concrete outcome is as shown in table 1.
Test method adopts the medicine infusion process of standard.Earlier determine general concentration range through trial test, all medicines all half-and-half are diluted to the variable concentrations gradient with distilled water, do not suck blood 10 of young Tickss of every group of boophilus microplus in test, 3 repetitions of every processing.Draw the 1ml medicine and add boophilus microplus and do not suck blood in the young Ticks, dipping 5s-10min with the medicine sucking-off, wipes away the medicinal liquid of dried Ticks body surface with filter paper, and being transferred to the bottom has in the drying basin of water, room temperature, and relative humidity remains on 80-85%.Behind the 24h, observe its death condition.Be provided with distilled water and normal control group in the test.If the mortality rate of matched group is at 5-20% Abbott formula correction.Judge the dead boophilus microplus young Ticks of not sucking blood with following program: the one, direct observation, each limb inertia of boophilus microplus; The 2nd, under anatomical lens, cannot see each limb activity of boophilus microplus; The 3rd, under anatomical lens, slightly contact with toothpick, also cannot see each limb activity of boophilus microplus.The mortality rate computing formula:
The different proportionings with Rynaxypyr of table 1 rotenone are to the killing effect of cattle Ticks
A represents Rynaxypyr; B represents rotenone
Table 2 toxicity test result of calculation
A represents Rynaxypyr; B represents rotenone
With 30 fleas (adult of cat flea), 5 kittens (wherein in contrast) on one's body in the parasitism respectively.After one day, evenly be sprayed on one's body the kitten with little aerosol apparatus, till kitten hair on one's body is moistening with the medicament in embodiment 1,2,3 and 4, the kitten of contrast is only sprayed clear water on one's body, sprayed back 1 day and 3 days, and, calculated prevention effect by catching the parasitic flea number of flea comb counting.Calculate control rate according to following formula, the result is according to following standard evaluation.
| Evaluation criterion | Control rate (%) |
| A | 100 |
| B | 99-90 |
| C | 89-80 |
| D | 79-50 |
| E | ＜50 |
Experimental result shows that the prevention effect of 1,2,3 and 4 pairs of kitten epizoite insects of the embodiment of the invention all reaches A.
Claims (8)
1. parasite killing host, it is characterized in that for rotenone and Rynaxypyr be to be mixed with the mixture that obtain at 1～40: 1～40 according to mass ratio.
2. according to the described parasite killing host of claim 1, it is characterized in that described rotenone: the mass ratio of Rynaxypyr is 1～10: 1～10.
3. according to the described parasite killing host of claim 1, it is characterized in that described rotenone: the mass ratio of Rynaxypyr is 1～7: 1～7.
4. the application of a claim 1,2 or 3 described parasite killing hosts, it is characterized in that being applied to prepare vitro anti-insect spray for pets, according to the parts by weight meter, described vitro anti-insect spray for pets comprises other adjuvant of 0.1～70 part of described parasite killing host of claim 1 and 15～170 parts; Described adjuvant comprises organic solvent, surfactant, antifreezing agent, anti-photodissociation agent, stabilizing agent, antioxidant and/or dispersant.
5. according to the described application of claim 4, it is characterized in that described vitro anti-insect spray for pets comprises that the ratio of weight and number of each component is:
Active insecticidal components: solvent: surfactant: antifreezing agent: anti-photodissociation agent: stabilizing agent: antioxidant: dispersant=0.1～50 part: 1～30 part: 1～20 part: 1～10 part: 0.1～10 part: 1～10 part: 0.1～10 part: 10～80 parts.
6. according to the described application of claim 4, it is characterized in that described solvent is selected from one or more of following substances: methanol, acetone, Ketohexamethylene, N, dinethylformamide, dimethyl sulfoxide, N-Methyl pyrrolidone, DMC dimethyl carbonate, isobutanol, isobutyl acetate, benzene, dimethylbenzene, naphthalane, gasoline, kerosene, machine oil, propylene glycol, propylene glycol, petroleum ether, Oleum Cinnamomi, eucalyptus oil, citronella oil, Oleum lavandula angustifolia, Sassafras oil, linalool, Fructus Coriandri oil or mustard oil;
Described surfactant is selected from one or more of following substances: one or more mixture of NPE, calcium dodecyl benzene sulfonate, alkyl polyoxyethylene ether phosphate ester, alkyl polyoxypropylene ether phosphate, NPE phosphate ester, fatty alcohol-polyoxyethylene ether series, C12 alkyl (EO) 3 ether sodium sulfates (AES), olefin sulfonic acid (AOS), lauric acid amide of ethanol, styryl phenyl polyoxyethylene ether or castor oil polyoxyethylene ether;
Described antifreezing agent is selected from one or more of following substances: ethylene glycol, glycerol, sorbitol, ethanol;
Described anti-photodissociation agent is selected from one or more of following compositions: para-amino benzoic acid, Oleum Ricini, pyrogallic acid, citric acid, lignosulfonates, UV-P, BP-12 or BP-3;
Described stabilizing agent is selected from one or more of following substances: epoxidized soybean oil, pyrogallol, sodium sorbate, sodium benzoate, eugenol, citric acid, pyrogallic acid are sad, Oleum Ricini, salicylic acid, olive oil or epoxidized linseed;
Described antioxidant is selected from one or more of following substances: vitamin E, vitamin C, beta-carotene, Butylated hydroxyanisole, 2,6 ditertiary butyl p cresol, citric acid, methoxybenzene or P-hydroxybenzoic acid;
Described dispersant is selected from one or more of following substances: ethanol, ethyl acetate or deionized water.
7. the preparation method of the described vitro anti-insect spray for pets of claim 4, it is characterized in that it being with the former powder of rotenone or crystal and the former medicinal solvent dissolving of Rynaxypyr, adding surfactant stirs, adding dispersant in proportion mixes, add antifreezing agent, anti-photodissociation agent, stabilizing agent, antioxidant and/or dispersant then successively, stir while adding evenly.
8. the using method of the described vitro anti-insect spray for pets of claim 4, it is characterized in that 10～20 centimetres of distance house pet vertical dimensions, contrary tippy tea direction begins to spray described spray gently, evenly cover animal skin to spray, till animal skin tippy tea portion humidity, gently grab fur and touch pet skin by spray; Perhaps directly spray of the present invention is sprayed on house pet life and active environment.
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101856027A (en) * | 2010-06-02 | 2010-10-13 | 扬州大学 | Pesticide preparation for controlling diamond back moth and other vegetable insect pests |
| CN102550573A (en) * | 2012-01-30 | 2012-07-11 | 华南理工大学 | Chlorantraniliprole and rotenone compound suspending agent and its preparation method |
| CN104398529A (en) * | 2014-10-27 | 2015-03-11 | 武汉中博绿亚生物科技有限公司 | Washing agent for assisting to kill pet body surface mites and preparation method thereof |
| CN105412004A (en) * | 2015-12-03 | 2016-03-23 | 湖北美天生物科技股份有限公司 | Anti-parasite composition for treating and protecting animals |
| CN105682669A (en) * | 2013-09-06 | 2016-06-15 | 马斯公司 | Oral anti-parasitic composition |
| CN105688168A (en) * | 2016-03-19 | 2016-06-22 | 上海申亚动物保健品阜阳有限公司 | Pet all-in-one insect expelling spray and preparation method thereof |
| CN113367118A (en) * | 2021-05-14 | 2021-09-10 | 中国农业科学院上海兽医研究所(中国动物卫生与流行病学中心上海分中心) | Application of Chinese cinnamon essential oil |
| CN115720902A (en) * | 2021-09-01 | 2023-03-03 | 郑州赛科药业科技有限公司 | Traditional Chinese medicine spray for treating ectoparasites of pets |
| CN117771182A (en) * | 2024-02-22 | 2024-03-29 | 中国农业大学 | External SU3327 spray for pets and preparation method and application thereof |
| CN117771182B (en) * | 2024-02-22 | 2024-05-31 | 中国农业大学 | External SU3327 spray for pets and preparation method and application thereof |
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| UA94777C2 (en) * | 2006-12-14 | 2011-06-10 | Ишихара Санджай Кайша, Лтд. | Insecticidal composition and method for controlling insects |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101856027A (en) * | 2010-06-02 | 2010-10-13 | 扬州大学 | Pesticide preparation for controlling diamond back moth and other vegetable insect pests |
| CN102550573A (en) * | 2012-01-30 | 2012-07-11 | 华南理工大学 | Chlorantraniliprole and rotenone compound suspending agent and its preparation method |
| CN105682669A (en) * | 2013-09-06 | 2016-06-15 | 马斯公司 | Oral anti-parasitic composition |
| US11497785B2 (en) | 2013-09-06 | 2022-11-15 | Mars, Incorporated | Oral anti-parasitic composition |
| CN104398529A (en) * | 2014-10-27 | 2015-03-11 | 武汉中博绿亚生物科技有限公司 | Washing agent for assisting to kill pet body surface mites and preparation method thereof |
| CN105412004A (en) * | 2015-12-03 | 2016-03-23 | 湖北美天生物科技股份有限公司 | Anti-parasite composition for treating and protecting animals |
| CN105412004B (en) * | 2015-12-03 | 2019-01-08 | 湖北美天生物科技股份有限公司 | It is a kind of for treating and protecting the antiparasitic composition of non-food stuff animal |
| CN105688168A (en) * | 2016-03-19 | 2016-06-22 | 上海申亚动物保健品阜阳有限公司 | Pet all-in-one insect expelling spray and preparation method thereof |
| CN113367118A (en) * | 2021-05-14 | 2021-09-10 | 中国农业科学院上海兽医研究所(中国动物卫生与流行病学中心上海分中心) | Application of Chinese cinnamon essential oil |
| CN115720902A (en) * | 2021-09-01 | 2023-03-03 | 郑州赛科药业科技有限公司 | Traditional Chinese medicine spray for treating ectoparasites of pets |
| CN117771182A (en) * | 2024-02-22 | 2024-03-29 | 中国农业大学 | External SU3327 spray for pets and preparation method and application thereof |
| CN117771182B (en) * | 2024-02-22 | 2024-05-31 | 中国农业大学 | External SU3327 spray for pets and preparation method and application thereof |
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| CN101919852B (en) | 2013-06-19 |
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