CN101919419B - Pollution-free efficient plant growth regulator and preparation method thereof - Google Patents

Pollution-free efficient plant growth regulator and preparation method thereof Download PDF

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CN101919419B
CN101919419B CN 200910022913 CN200910022913A CN101919419B CN 101919419 B CN101919419 B CN 101919419B CN 200910022913 CN200910022913 CN 200910022913 CN 200910022913 A CN200910022913 A CN 200910022913A CN 101919419 B CN101919419 B CN 101919419B
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plant growth
growth regulator
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pollution
chinese medicine
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CN101919419A (en
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郭海桥
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Guo Haiqiao
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Abstract

The invention discloses a pollution-free efficient plant growth regulator and a preparation method thereof. The pollution-free efficient plant growth regulator is prepared from earthworm, radix angelicae pubescentis, 5-nitroguaiacol sodium, rehmanniae praeparatum, phellodendron amurense and grifola according to certain weight proportion by the steps of processing raw materials, soaking in classes, juicing, purifying, carrying out mixing reaction, separately encapsulating, packaging, and the like. The plant growth regulator of the invention can effectively promote plant growth and development and the absorption and running of nutritional substances, promote the early maturing of crops, improve the crop yield by more than 20 percent and optimize the quality of the crops. Meanwhile, various bacteria in a plant body can be inhibited and killed, and the drought and cold resistant capability of the crops is improved. The invention has the advantages of obvious drug effect, easy degradation and no residual pollution, has simple preparation method and low cost and can be accepted by wide consumers.

Description

A kind of pollution-free efficient plant growth regulator and preparation method thereof
Technical field
The present invention relates to technical field of pesticide, relate in particular to a kind of pollution-free efficient plant growth regulator and preparation method thereof.
Background technology
At present, the plant growth regulator that uses on the agricultural is mainly chemical synthesis preparation, and it is precocious to promoting crop, and raising crop yield aspect effect is obvious.But most plant growth regulator function singlenesses can not improve quality, and the environmental pollution that excessive use causes is also day by day serious, residual component enters in the body by food chain, has side effects, and is too fast such as Juvenile development, the side effect that early sexual maturity brings, increasingly significant.For this reason, numerous scientific research personnel utilize plant to go out the various plants growth regulator for the raw material develop, cloudlike tongue element lactone, jasmonic etc., but it is as product, are still chemosynthesis, still have the pollution to environment.In recent years, also there are some scientific research personnel to attempt in the plant corpus of screening, extracting the direct sample preparation of mixture, utilize the interior active active principle of plant corpus to reach the purpose of coordinate plant growth.This series products has easy degraded, the advantage that noresidue is polluted, but the drug effect sluggish causes regulating effect not good, affects it and applies.So, choose the little chemicals of high energy plant material and the side effect research and development pollution-free efficient plant growth regulator that combines and seem very necessary.
Technology contents
The object of the present invention is to provide pollution-free efficient plant growth regulator that a kind of Chinese medicine and chemical composition combine and preparation method thereof.
Plant growth regulator of the present invention is made by the raw material of following weight parts:
Earthworm 18-28 part; Levisticum 15-23 part;
5-nitroguaiacol sodium salt 15-25 part; Dried rhizome of rehmannia 18-28 part;
Golden cypress 15-28 part; Umbellate pore furgus 15-28 part.
The preferred weight of each raw material (part) proportioning is in this plant growth regulator:
25 parts of earthworms; 20 parts of levisticums;
20 parts of 5-nitroguaiacol sodium salts; 25 parts in the dried rhizome of rehmannia;
20 parts of golden cypresses; 20 parts of umbellate pore furgus.
The preparation process of plant growth regulator of the present invention is as follows:
A) raw material is processed proportioning in accordance with regulations and is chosen drying, clean traditional Chinese medicinal material raw materials earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, umbellate pore furgus, each Chinese medicine material is put into respectively liquor potassic permanganate soaked 10-20 minute, carries out sterilization treatment; The content of regulation proportioning is dissolved in greater than 95% the former powder of 5-nitroguaiacol sodium salt disappears moltenly in the water of its 70-75 times weight, stir, place for subsequent use;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 20-26 hour, places in the cool after the taking-up 10-12 hour;
C) squeeze the juice to purify and each Chinese medicine material is put into respectively crusher squeeze juice, each juice that squeezes is crossed respectively 200 orders and 100 mesh sieve impurity eliminations, then placed in the cool respectively 25-30 hour, for subsequent use;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5-nitroguaiacol sodium salt solution that configures are inserted in the reaction vessel and are mixed, and after stirring, maintain the temperature under 15-20 ℃, place and react in 70-72 hour;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, liquid gets product.
Using method: with the finished product liquid by 1: after 300-500 doubly is watered dilution, carry out foliage-spray.
The raw material of plant growth regulator of the present invention forms and the amount ranges of each raw material is that the inventor went through 16 years, through repeatedly research, and screening from hundreds of traditional Chinese medicinal material raw materials and chemical substance and going out, and repeatedly verify and determine through field trial.The performance that forms each raw material of this plant growth regulator is:
Earthworm is the dry body of huge earthworm animal Pheretima aspergillum Pheretima asprgillum of section (perrier) or allolobophora caliginosa trapezoides Allolobophora caliginosa (Savigny) trapezoids (Ant.Duges).It is salty, cold in nature to distinguish the flavor of.Main component is lumbricin, lumbrifebrine, choline, amino acid etc.Crops are had enhancing, promote the effect that Nutrient Absorption and recovery are grown.
Levisticum is the root of samphire Angelica pubescens Angelica pubecens Maxim.f.biserratashan et yuan..Flavor is hot, bitter, slightly warm in nature.Contain levisticum lactones, flavonoids etc.Have and keep preferably the interior moisture of plant object and face upward the bacterium bactericidal action.
The piece root of radix rehmanniae recen Scrophulariaceae herbaceos perennial glutinous rehmannia Rehmannia glutinosa Libosch..It is sweet, bitter, cold in nature to distinguish the flavor of.Crops are had the preferably conversion opposite sex, promote normal healthy and strong growth.
Golden cypress is the bark of rutaceae lodh bark Phellodendron chinense schneid. or cork tree Phellodendron amurense rupr.Bitter, cold in nature.Contain the compositions such as jamaicin, phellodendrine, obakunone.Have bactericidal action, can effectively strengthen the disease resistance ability of crops.
The umbellate pore furgus flavor is sweet, light, and property is flat.The function clearing damp and promoting diuresis.But be used for crops Effective Raise crop immunocompetence, promote plant growth.
The 5-nitroguaiacol sodium salt is a kind of powerful cell-activating agent, with can rapid permeability after the plant contact in plant corpus, promote the protoplasm of cell to flow, improve cell viability, accelerate plant establishment and germinate, promote growth, reproduction and result, help fertilization.Share with above all medicines, can not only be transported to the position that plants needs to each drug component timely and effectively, and drug effect is significantly improved.
The present invention's plant growth regulator will can be used for traditional Chinese medicine and chemical raw material that the mankind cure the disease and combine, make each medicine effect fully produce synergy, not only effectively absorption, the running of Promoting plant growth growth and nutriment, promote crop precocious, and can increase substantially crop yield more than 20%, crop quality is optimized.Simultaneously, also can kill the multiple germ in the plant corpus, improve drought resisting, the cold tolerance of crop.Have the drug effect performance rapidly, easily degraded, the advantage that noresidue is polluted, and the preparation method is simple, and with low cost, for consumers in general can bear.
Embodiment
The below narrates three embodiment of the present invention:
Embodiment 1
Take by weighing clean, dry Chinese medicine material: earthworm 20kg, levisticum 22kg, dried rhizome of rehmannia 26kg, golden cypress 18kg, umbellate pore furgus 25kg take by weighing the former powder 18kg of 5-nitroguaiacol sodium salt of content 95%.
The preparation method:
A) raw material is processed traditional Chinese medicinal material raw materials earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, the umbellate pore furgus of above-mentioned weight is put into respectively liquor potassic permanganate immersion 10 minutes, carries out sterilization treatment; The former powder of 5-nitroguaiacol sodium salt of the content 95% of above-mentioned weight is dissolved in disappears moltenly in the water of its 75 times of weight, stir, place for subsequent use;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 20 hours, places in the cool after the taking-up 12 hours;
C) squeeze the juice to purify and each Chinese medicine material is put into respectively crusher squeeze juice, each juice that squeezes is crossed respectively 200 orders and 100 mesh sieve impurity eliminations, then placed in the cool respectively 25 hours, for subsequent use;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5-nitroguaiacol sodium salt solution that configures are put into reaction vessel and are mixed, and after stirring, temperature remains on 20 ℃, places and reacts in 70 hours;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, liquid gets product.
Example: 300 mu of nuisanceless booth vegetables base, Fan Jiayu village, Hejin City of Shanxi Province bavin local, used this conditioning agent to the experiment situation of cucumber, tomato, eggplant, gift watermelon, foreign muskmelon, green capsicum in 2008:
To above each crop, all begin to spray this agent from Seedling Stage, before the florescence, above-mentioned finished product liquid is watered dilution by 1: 500 times sprays, sprayed once in per 15 days, through observing, each crop chlorophyll increases obviously, and blade is plump, seedling is sturdy, and growth situation obviously strengthens advance flowering period; From each crop enters the florescence, spray by 1: 400 times of dilution, sprayed once in per ten days, Hua Mi, percentage of fertile fruit is high, without any sick mark, all the growing way development is neat behind the setting, and the cucumber maturation is long large and straight afterwards, after growing up to the base near do not use this agent plastic tent cucumber compare, single weight increases more than 20%, go on the market in advance more than 10 days, prolong a wheat harvesting period vegetative period, receive more than two batches more, every mu of income reaches more than 35200 yuan, takes in more than 8000 yuan than near every mu of the preferably booth of not using this agent the base more; Fruit is bright and clean mellow and full after the tomato maturation, and without malformed fruit, near the booth in base of more not using this agent goes on the market more than 15 days in advance, and volume increase is more than 20%, and more than 14100 yuan of mu incomes are not more used near the better booth of this agent and taken in nearly 3000 yuan more; Gift watermelon, foreign muskmelon grow up to rear curcumbitate circle, individual large, the fruit marshalling, and near near do not use this agent the base booth curcumbitate circle length differs, individual little, fruit is arranged uneven, and Time To Market obviously lags behind, and is significantly shorter than the base booth that sprays this agent vegetative period, the mu income differences attracts near the canopy master in base and peasant household to come to visit more than 5000 yuan frequently; Eggplant, when spicy begins to go on the market, near the booth in base that does not spray this agent there is no bud with veriety and forms sign, the booth that fruit after growing up to does not spray this agent is with veriety on average about long one-inch, and the fruiting quantities difference is obvious, the mu income reaches respectively more than 14200 yuan and more than 13100 yuan, takes in more than 25% than near the better booth that does not spray this agent the base more.This conditioning agent is after use in this base, and the peasant household near village, town requires one after another for medicine, and in the process of the test, the expert Shi Yulong of Pinglu County, Shanxi Province agriculture vegetable repeatedly investigates, and experimental result is greatly gasp in admirationd, requires in the Pinglu County ten thousand mu of Vegetable Bases to apply.
Example: the high Xiaoyi of the Hancheng City Qiao Zi of Shaanxi Province profound township king villager, used this conditioning agent to spray the Chinese prickly ash situation in 2008:
Last year since be subjected to cold in the late spring and spring drought impact, large quantities of Chinese prickly ash underproduction are serious.And five mu of Chinese prickly ashes that I plant, because from March 20, the dilution of the above-mentioned conditioning agent after namely beginning 1: 300 times be watered every ten days foliage-spray Chinese prickly ashes once there is no the impact that is subject to natural calamity, the green pepper leaf keeps blackish green always, not anti-reflection of bud increases, and percentage of fertile fruit is apparently higher than near the green pepper garden that does not spray this conditioning agent, and the green pepper grain expands rapidly behind the setting, every pawl 60-80 grain, the green pepper rate that falls also only has about 3%, and the tree without the green pepper pawl also had the green pepper pawl to generate in several years, and anosis worm trail resembles.And near green pepper garden of not using this conditioning agent, every pawl only has the 30-40 grain, and the green pepper quantity that falls is large, and aphid, wax are situated between more.These five mu of Chinese prickly ash lovely lusters after the maturation, skin depth meat is rich, more than the dried green pepper 80kg of mu air dry, than increasing production nearly 20 kilograms former years, all reach one-level Chinese prickly ash standard, mu income reaches more than 1600 yuan, and near the management of not using this conditioning agent preferably green pepper garden mu income has more more than 600 yuan.
Implementation column 2
Take by weighing clean, dry Chinese medicine material: earthworm 26kg, levisticum 18kg, dried rhizome of rehmannia 20kg, golden cypress 25kg, umbellate pore furgus 18kg take by weighing the former powder 22kg of 5-nitroguaiacol sodium salt of content 98%.
The preparation method:
A) raw material is processed traditional Chinese medicinal material raw materials earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, the umbellate pore furgus of above-mentioned weight is put into respectively liquor potassic permanganate immersion 20 minutes, carries out sterilization treatment; The former powder of 5-nitroguaiacol sodium salt of the content 98% of above-mentioned weight is dissolved in disappears moltenly in the water of its 70 times of weight, stir, place for subsequent use;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 26 hours, places in the cool after the taking-up 10 hours;
C) squeeze the juice to purify and each Chinese medicine material is put into respectively crusher squeeze juice, each juice that squeezes is crossed respectively 200 orders and 100 mesh sieve impurity eliminations, then placed in the cool respectively 30 hours, for subsequent use;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5-nitroguaiacol sodium salt solution that configures are put into reaction vessel and are mixed, and after stirring, temperature remains on 15 ℃, places and reacts in 72 hours;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, liquid gets product.
Example: longevity temple villager high ferro prestige in the Hancheng City Zhi Yang town, Shaanxi Province, the situation of above-mentioned conditioning agent was not used in 500 mu of peach gardens contracting of thread gold in 2008:
Application method: from the florescence, above-mentioned finished product liquid is watered dilution by 1: 300 times, sprayed once every ten days.
Performance: spray first about rear ten days, leaf exhibition elongation, thickness increase, and after spraying for two, three times, tree vigo(u)r obviously strengthens, and fruit-setting rate is high, and Fruit is fast, and tree is upper without worm.By after the continuous dispenser of the method, fructescence in advance, go on the market in advance about 15 days than the same veriety of not using on a small quantity this conditioning agent in the garden, and fruit shape is good, does not have askew peach, look red, face light, mouthfeel are good, inferior peach is also larger than the morning peach of not spraying this conditioning agent, and the mu volume increase is more than 30%, and commodity rate reaches more than 95, about 5000 yuan of incomes per mu are than more than 1500 yuan of the receipts of Duoing per mu of not using this conditioning agent.
Example: one group of villager Yuan Qimin of Hancheng City Zhi Chuan town Lv Zhuan, used this conditioning agent to spray the apple orchard situation in 2009:
April 10 was watered dilution with above-mentioned finished product liquid by 1: 400 times and begins to spray, and sprayed continuously at present three times, and tree vigo(u)r is strong, and percentage of fertile fruit is high, and Fruit is obvious, and fruit shape is good, and the orchard that does not spray this conditioning agent is on every side compared with it, and difference is very obvious.
Embodiment 3
Take by weighing clean, dry Chinese medicine material: earthworm 25kg, levisticum 20kg, dried rhizome of rehmannia 25kg, golden cypress 20kg, umbellate pore furgus 20kg take by weighing the former powder 20kg of 5-nitroguaiacol sodium salt of content 98%.
The preparation method:
A) raw material is processed traditional Chinese medicinal material raw materials earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, the umbellate pore furgus of above-mentioned weight is put into respectively liquor potassic permanganate immersion 15 minutes, carries out sterilization treatment; The former powder of 5-nitroguaiacol sodium salt of the content 98% of above-mentioned weight is dissolved in disappears moltenly in the water of its 72 times of weight, stir, place for subsequent use;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 24 hours, places in the cool after the taking-up 10 hours;
C) squeeze the juice to purify and each Chinese medicine material is put into respectively crusher squeeze juice, each juice that squeezes is crossed respectively 200 orders and 100 mesh sieve impurity eliminations, then placed in the cool respectively 28 hours, for subsequent use;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5-nitroguaiacol sodium salt solution that configures are put into reaction vessel and are mixed, and after stirring, temperature remains on 18 ℃, places and reacts in 72 hours;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, liquid gets product.
The experimenter: the old villager Malin in the Hancheng City Zhi Chuan south of a town, this conditioning agent situation on probation in wheatland: planted two mu of wheats last year, one mu has been used above-mentioned conditioning agent, one mu is not used, and adopts at random the fringe contrast after the maturation, uses the wheat head of this conditioning agent, be four Mai Shan, 67 of average 11 rows, full grains, it is high to contain the face rate, and output is 1125 jin, does not use the wheat head of this conditioning agent, average three Mai Shan, 36 of 7 rows, and the little insatiable hunger of grain, output is 787 jin.Application process is: from the wheat flowering, spray once after above-mentioned finished product liquid being watered dilution by 1: 400 times in ten days.
The experimenter: the old villager in the Hancheng City Zhi Chuan south of a town, Shaanxi Province is permitted sharp virtue, try out above-mentioned conditioning agent situation at Crops ': after receiving custard squash last year, the tomato of in half mu of booth, planting again, planted seedling on April 12, began dead seedling on the 18th, fill the gaps with seedlings continuously, continuous dead seedling, prepare to abandon no matter the time, April 30, spray once after above-mentioned finished product liquid on probation was watered dilution by 1: 500, do not have again dead seedling, filled spray once May 10 again subsequently, do not play again any agricultural chemicals and bactericide, last year, tomato came along fine, and bloomed that it is all better than former years to bear fruit, and output is than increasing more than 30% former years.
Experimenter: the northern old villager horse light in Hancheng City Zhi Chuan town, Shaanxi Province, try out above-mentioned conditioning agent situation at plastic tent cucumber: this year, one mu of plastic tent cucumber of planting is subject to the downy mildew invasion and attack, still of no avail after the various sterilization agent on probation, melon is little and curved, turns white, there is not commodity value, April 21 sprayed above-mentioned conditioning agent on probation after seven days by 1: 400 times of dilution, and climing the backing down of cucumber begins to extract new branch out, grown new leaf, demutation in dead, after more than 20 day, begin again the setting of blooming on new long cucumber is climing, now sold two batches of cucumber, every batch two, 3,000 yuan of incomes, at present, melon is climing also in continuity, and income is arranged every day.

Claims (3)

1. a pollution-free efficient plant growth regulator is characterized in that, it is to be made by the raw material of following weight parts:
Earthworm 18-28 part; Levisticum 15-23 part;
5-nitroguaiacol sodium salt 15-25 part; Dried rhizome of rehmannia 18-28 part;
Golden cypress 15-28 part; Umbellate pore furgus 15-28 part.
2. plant growth regulator according to claim 1 is characterized in that, the weight proportion of each raw material is:
25 parts of earthworms; 20 parts of levisticums;
20 parts of 5-nitroguaiacol sodium salts; 25 parts in the dried rhizome of rehmannia;
20 parts of golden cypresses; 20 parts of umbellate pore furgus.
3. the preparation method of claim 1 or 2 described plant growth regulator is characterized in that, described preparation method may further comprise the steps:
A) raw material is processed proportioning in accordance with regulations and is chosen drying, clean traditional Chinese medicinal material raw materials earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, umbellate pore furgus, each Chinese medicine material is put into respectively liquor potassic permanganate soaked 10-20 minute, carries out sterilization treatment; The content of regulation proportioning is dissolved in greater than 95% the former powder of 5-nitroguaiacol sodium salt disappears moltenly in the water of its 70-75 times weight, stir, place for subsequent use;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 20-26 hour, places in the cool after the taking-up 10-12 hour;
C) squeeze the juice to purify and each Chinese medicine material is put into respectively crusher squeeze juice, each juice that squeezes is crossed respectively 200 orders and 100 mesh sieve impurity eliminations, then placed in the cool respectively 25-30 hour, for subsequent use;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5-nitroguaiacol sodium salt solution that configures are inserted in the reaction vessel and are mixed, and after stirring, maintain the temperature under 15-20 ℃, place and react in 70-72 hour;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, liquid gets product.
CN 200910022913 2009-06-11 2009-06-11 Pollution-free efficient plant growth regulator and preparation method thereof Expired - Fee Related CN101919419B (en)

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Application Number Priority Date Filing Date Title
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103734192A (en) * 2013-10-22 2014-04-23 兰在明 Plant growth regulator
CN107006517A (en) * 2017-04-12 2017-08-04 江苏金凤凰农化有限公司 A kind of composition and application process that peach shot hole is treated based on guaiacol

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