CN101919419A - Pollution-free efficient plant growth regulator and preparation method thereof - Google Patents

Pollution-free efficient plant growth regulator and preparation method thereof Download PDF

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Publication number
CN101919419A
CN101919419A CN2009100229132A CN200910022913A CN101919419A CN 101919419 A CN101919419 A CN 101919419A CN 2009100229132 A CN2009100229132 A CN 2009100229132A CN 200910022913 A CN200910022913 A CN 200910022913A CN 101919419 A CN101919419 A CN 101919419A
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plant growth
growth regulator
chinese medicine
parts
pollution
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CN101919419B (en
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郭海桥
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Guo Haiqiao
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SHAANXI HANCHENG YUJIAN CHEMICAL CO Ltd
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Abstract

The invention discloses a pollution-free efficient plant growth regulator and a preparation method thereof. The pollution-free efficient plant growth regulator is prepared from earthworm, radix angelicae pubescentis, 5-nitroguaiacol sodium, rehmanniae praeparatum, phellodendron amurense and grifola according to certain weight proportion by the steps of processing raw materials, soaking in classes, juicing, purifying, carrying out mixing reaction, separately encapsulating, packaging, and the like. The plant growth regulator of the invention can effectively promote plant growth and development and the absorption and running of nutritional substances, promote the early maturing of crops, improve the crop yield by more than 20 percent and optimize the quality of the crops. Meanwhile, various bacteria in a plant body can be inhibited and killed, and the drought and cold resistant capability of the crops is improved. The invention has the advantages of obvious drug effect, easy degradation and no residual pollution, has simple preparation method and low cost and can be accepted by wide consumers.

Description

A kind of pollution-free efficient plant growth regulator and preparation method thereof
Technical field
The present invention relates to technical field of pesticide, relate in particular to a kind of pollution-free efficient plant growth regulator and preparation method thereof.
Background technology
At present, the plant growth regulator that uses on the agricultural is mainly chemical synthesis preparation, and it is to promoting the crop precocity, and raising crop yield aspect effect is obvious.But most plant growth regulator function singlenesses can not improve quality, and the environmental pollution that excessive use causes is also serious day by day, residual component enters in the body by food chain, has side effects, and grows too fast as the teenager, the side effect that early sexual maturity brings, increasingly significant.For this reason, numerous scientific research personnel utilize plant successfully to develop the various plants growth regulator for raw material, cloudlike the plain lactone of tongue, jasmonic etc., but it is as product, are still chemosynthesis, still have the pollution to environment.In recent years, also there are some scientific research personnel to attempt in the plant corpus of screening, extracting the direct sample preparation of mixture, utilize the interior active active principle of plant corpus to reach the purpose of coordinate plant growth.This series products has easy degraded, the advantage that noresidue is polluted, but the drug effect sluggish causes regulating effect not good, affects it and applies.So, choose the little chemicals of high energy plant material and the side effect research and development pollution-free efficient plant growth regulator that combines and seem very necessary.
Technology contents
The object of the present invention is to provide pollution-free efficient plant growth regulator that a kind of Chinese medicine and chemical composition combine and preparation method thereof.
Plant growth regulator of the present invention is made by the raw material of following weight parts:
Earthworm 18-28 part; Levisticum 15-23 part;
5 nitroguaiacol sodium 15-25 part; Dried rhizome of rehmannia 18-28 part;
Golden cypress 15-28 part; Umbellate pore furgus 15-28 part.
The preferred weight of each raw material (part) proportioning is in this plant growth regulator:
25 parts of earthworms; 20 parts of levisticums;
20 parts in 5 nitroguaiacol sodium; 25 parts in the dried rhizome of rehmannia;
20 parts of golden cypresses; 20 parts of umbellate pore furgus.
The preparation process of plant growth regulator of the present invention is as follows:
A) raw material is handled proportioning in accordance with regulations and is chosen drying, clean traditional Chinese medicine raw material earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, umbellate pore furgus, each Chinese medicine material is put into liquor potassic permanganate respectively soaked 10-20 minute, carries out sterilization treatment; The content of regulation proportioning is dissolved in greater than 95% the former powder of 5 nitroguaiacol sodium disappears moltenly in the water of its 70-75 times weight, stir, place standby;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 20-26 hour, places in the cool after the taking-up 10-12 hour;
C) squeeze the juice to purify and each Chinese medicine material is put into crusher respectively squeeze juice, each juice that squeezes is crossed 200 orders and 100 mesh sieve impurity eliminations respectively, placed in the cool respectively 25-30 hour then, standby;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5 nitroguaiacol sodium solution that configures are inserted in the reaction vessel and are mixed, and after stirring, maintain the temperature under 15-20 ℃, place and react in 70-72 hour;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, soup gets product.
Using method: with the finished product soup by 1: 300-500 carries out foliage-spray after doubly converting water dilution.
The raw material of plant growth regulator of the present invention is formed and the amount ranges of each raw material is that the inventor went through 16 years, through research repeatedly, and screening from hundreds of traditional Chinese medicine raw materials and chemical substance and going out, and verify repeatedly and determine through field trial.The performance of forming each raw material of this plant growth regulator is:
Earthworm is the dry body of huge earthworm animal Pheretima aspergillum Pheretima asprgillum of section (perrier) or allolobophora caliginosa trapezoides Allolobophora caliginosa (Savigny) trapezoids (Ant.Duges).It is salty, cold in nature to distinguish the flavor of.Main component is lumbricin, lumbrifebrine, choline, amino acid etc.Crops are had enhancing, promote the effect that Nutrient Absorption and recovery are grown.
Levisticum is the root of the heavy peristome Radix Angelicae Sinensis of samphire Angelica pubecens Maxim.f.biserratashan et yuan..Flavor is hot, bitter, slightly warm in nature.Contain levisticum lactones, flavonoids etc.Have and keep the interior moisture of plant object preferably and face upward the bacterium bactericidal action.
The piece root of radix rehmanniae recen Scrophulariaceae herbaceos perennial glutinous rehmannia Rehmannia glutinosa Libosch..It is sweet, bitter, cold in nature to distinguish the flavor of.Crops are had the better conversion opposite sex, promote normal healthy and strong growth effect.
Golden cypress is the bark of rutaceae lodh bark Phellodendron chinense schneid. or cork tree Phellodendron amurense rupr.Bitter, cold in nature.Contain compositions such as jamaicin, phellodendrine, obakunone.Have bactericidal action, can effectively strengthen the disease resistance ability of crops.
The umbellate pore furgus flavor is sweet, light, and property is flat.The function clearing damp and promoting diuresis.Be used for crops and can effectively improve the crop immunocompetence, promote plant growth.
5 nitroguaiacol sodium is a kind of powerful cell-activating agent, with can rapid permeability after the plant contact in plant corpus, promote the protoplasm of cell to flow, improve cell viability, accelerate plant establishment and germinate, promote growth, reproduction and result, help fertilization solid.Share with above all medicines, can not only be transported to the required position of plant to each drug component timely and effectively, and drug effect is significantly improved.
The present invention's plant growth regulator will can be used for traditional Chinese medicine and chemical raw material that the mankind cure the disease and combine, make each medicine effect fully produce synergy, not only can effectively promote absorption, the running of growth and development of plants and nutriment, promote the crop precocity, and can increase substantially crop yield more than 20%, crop quality is optimized.Simultaneously, also can kill the multiple germ in the plant corpus, improve drought resisting, the cold tolerance of crop.Have the drug effect performance rapidly, easily degraded, the advantage that noresidue is polluted, and the preparation method is simple, and with low cost, for consumers in general can bear.
Embodiment
Narrate three embodiment of the present invention below:
Embodiment 1
Take by weighing clean, dry traditional Chinese medicine raw material: earthworm 20kg, levisticum 22kg, dried rhizome of rehmannia 26kg, golden cypress 18kg, umbellate pore furgus 25kg take by weighing the former powder 18kg of 5 nitroguaiacol sodium of content 95%.
The preparation method:
A) raw material is handled traditional Chinese medicine raw material earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, the umbellate pore furgus of above-mentioned weight is put into liquor potassic permanganate immersion 10 minutes respectively, carries out sterilization treatment; The former powder of 5 nitroguaiacol sodium of the content 95% of above-mentioned weight is dissolved in disappears moltenly in the water of its 75 times of weight, stir, place standby;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 20 hours, places in the cool after the taking-up 12 hours;
C) squeeze the juice to purify and each Chinese medicine material is put into crusher respectively squeeze juice, each juice that squeezes is crossed 200 orders and 100 mesh sieve impurity eliminations respectively, placed in the cool respectively 25 hours then, standby;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5 nitroguaiacol sodium solution that configures are put into reaction vessel and are mixed, and after stirring, temperature remains on 20 ℃, places and reacts in 70 hours;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, soup gets product.
Example: 300 mu of nuisanceless booth vegetables base, Fan Jiayu village, bavin local, Hejin City, Shanxi Province, used the experiment situation of this conditioning agent in 2008 to cucumber, tomato, eggplant, gift watermelon, foreign muskmelon, green capsicum:
To above each crop, all begin seedling stage since the childhood to spray this agent, before the florescence, above-mentioned finished product soup is converted the water dilution by 1: 500 times spray, sprayed once in per 15 days, through observing, each crop chlorophyll increases obviously, the blade plumpness, seedling is sturdy, and growth situation obviously strengthens advance flowering period; Enter the florescence from each crop, spray by 1: 400 times of dilution, sprayed once in per ten days, Hua Mi, the percentage of fertile fruit height, there is not any sick mark, all the growing way development is neat behind the setting, and is long big and straight after the cucumber maturation, grows up near do not use this agent back and the base plastic tent cucumber and compares, single weight increases more than 20%, go on the market in advance more than 10 days, prolong a wheat harvesting period vegetative period, overcharge more than two batches, surplus every mu of income reaches 35200 yuan, overcharge more than 8000 yuan than near every mu of the booth preferably of not using this agent the base; Fruit is bright and clean mellow and full after the tomato maturation, no malformed fruit, more do not use the base of this agent near booth go on the market in advance more than 15 days, volume increase is more than 20%, surplus the mu income 14100 yuan, more do not use near the better booth of this agent and overcharges into nearly 3000 yuan; Gift watermelon, foreign muskmelon grow up to back curcumbitate circle, individual big, the fruit marshalling, and near near do not use this agent the base booth curcumbitate circle length differs, individual little, fruit is arranged uneven, and Time To Market obviously lags behind, and is significantly shorter than the base booth that sprays this agent vegetative period, the mu income differences attracts near canopy master in base and peasant household to come to visit more than 5000 yuan frequently; Eggplant, when spicy begins to go on the market, near the booth in base that does not spray this agent does not still have bud with veriety and forms sign, the booth that fruit after growing up to does not spray this agent with the on average long one-inch of veriety about, and the quantity difference is obvious as a result, the mu income reaches more than 14200 yuan and more than 13100 yuan respectively, overcharges more than 25% than near the better booth that does not spray this agent the base.This conditioning agent is after use in this base, and the peasant household near village, town requires one after another for medicine, and in the process of the test, the expert Shi Yulong of Pinglu County, Shanxi Province agriculture vegetable repeatedly investigates, and experimental result is greatly gasp in admirationd, requirement is applied in ten thousand mu of vegetables bases in the Pinglu County.
Example: the high Xiaoyi of the Hancheng City Qiao Zi of Shaanxi Province profound township king villager, used this conditioning agent to spray the Chinese prickly ash situation in 2008:
Last year since be subjected to cold in the late spring and spring drought impact, large quantities of Chinese prickly ash underproduction are serious.And five mu of Chinese prickly ashes that I plant, because from March 20, promptly begin with 1: the 300 times of dilution of converting the above-mentioned conditioning agent behind the water once not to be subjected to the influence of natural calamity basically every ten days foliage-spray Chinese prickly ashes, the green pepper leaf keeps blackish green always, not anti-reflection of bud increases, and percentage of fertile fruit is apparently higher than near the green pepper garden that does not spray this conditioning agent, and the green pepper grain expands rapidly behind the setting, every pawl 60-80 grain, the green pepper rate that falls also only has about 3%, and the tree of several years no green pepper pawls also has the green pepper pawl to generate, and anosis worm trail resembles.And near green pepper garden of not using this conditioning agent, every pawl only has the 30-40 grain, and the green pepper quantity that falls is big, and aphid, wax are situated between more.These five mu of Chinese prickly ash lovely lusters after the maturation, skin depth meat is rich, and the mu cold is dried more than the green pepper 80kg, than increasing production nearly 20 kilograms former years, all reach one-level Chinese prickly ash standard, surplus mu income reaches 1600 yuan, near management of not using this conditioning agent is surplus mu income in green pepper garden has more 600 preferably yuan.
Implementation column 2
Take by weighing clean, dry traditional Chinese medicine raw material: earthworm 26kg, levisticum 18kg, dried rhizome of rehmannia 20kg, golden cypress 25kg, umbellate pore furgus 18kg take by weighing the former powder 22kg of 5 nitroguaiacol sodium of content 98%.
The preparation method:
A) raw material is handled traditional Chinese medicine raw material earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, the umbellate pore furgus of above-mentioned weight is put into liquor potassic permanganate immersion 20 minutes respectively, carries out sterilization treatment; The former powder of 5 nitroguaiacol sodium of the content 98% of above-mentioned weight is dissolved in disappears moltenly in the water of its 70 times of weight, stir, place standby;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 26 hours, places in the cool after the taking-up 10 hours;
C) squeeze the juice to purify and each Chinese medicine material is put into crusher respectively squeeze juice, each juice that squeezes is crossed 200 orders and 100 mesh sieve impurity eliminations respectively, placed in the cool respectively 30 hours then, standby;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5 nitroguaiacol sodium solution that configures are put into reaction vessel and are mixed, and after stirring, temperature remains on 15 ℃, places and reacts in 72 hours;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, soup gets product.
Example: longevity temple villager high ferro prestige in the Hancheng City Zhi Yang town, Shaanxi Province, the situation of above-mentioned conditioning agent was not used in 500 mu of peach gardens contracting of thread gold in 2008:
Application method: from the florescence, above-mentioned finished product soup is converted the water dilution by 1: 300 times, sprayed once every ten days.
Performance: spray first about back ten days, leaf exhibition elongation, thickness increase, and after spraying for two, three times, tree vigo(u)r obviously strengthens, and fruit-setting rate height, fruit expand soon, and the last no worm of tree.By after the continuous dispenser of this method, fructescence in advance, go on the market in advance about 15 days than the same veriety of not using this conditioning agent in the garden on a small quantity, and fruit shape is good, does not have askew peach, look red, face light, mouthfeel are good, inferior peach is also bigger than the morning peach of not spraying this conditioning agent, and the mu volume increase is more than 30%, and commodity rate reaches more than 95, about 5000 yuan of incomes per mu, than do not use this conditioning agent per mu overcharge 1500 surplus yuan.
Example: one group of villager Yuan Qimin of Hancheng City Zhi Chuan town Lv Zhuan, used this conditioning agent to spray the apple orchard situation in 2009:
April 10, above-mentioned finished product soup is converted the water dilution by 1: 400 times begin to spray, spray continuously at present three times, tree vigo(u)r is strong, and the percentage of fertile fruit height, and fruit expands obviously, and fruit shape is good, and the orchard that does not spray this conditioning agent is on every side compared with it, and difference is very obvious.
Embodiment 3
Take by weighing clean, dry traditional Chinese medicine raw material: earthworm 25kg, levisticum 20kg, dried rhizome of rehmannia 25kg, golden cypress 20kg, umbellate pore furgus 20kg take by weighing the former powder 20kg of 5 nitroguaiacol sodium of content 98%.
The preparation method:
A) raw material is handled traditional Chinese medicine raw material earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, the umbellate pore furgus of above-mentioned weight is put into liquor potassic permanganate immersion 15 minutes respectively, carries out sterilization treatment; The former powder of 5 nitroguaiacol sodium of the content 98% of above-mentioned weight is dissolved in disappears moltenly in the water of its 72 times of weight, stir, place standby;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 24 hours, places in the cool after the taking-up 10 hours;
C) squeeze the juice to purify and each Chinese medicine material is put into crusher respectively squeeze juice, each juice that squeezes is crossed 200 orders and 100 mesh sieve impurity eliminations respectively, placed in the cool respectively 28 hours then, standby;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5 nitroguaiacol sodium solution that configures are put into reaction vessel and are mixed, and after stirring, temperature remains on 18 ℃, places and reacts in 72 hours;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, soup gets product.
The experimenter: the old villager Malin in the Hancheng City Zhi Chuan south of a town, this conditioning agent situation on probation in wheatland: planted two mu of wheats last year, one mu has been used above-mentioned conditioning agent, one mu is not used, and adopts the fringe contrast after the maturation at random, uses the wheat head of this conditioning agent, be four Mai Shan, 67 of average 11 rows, full grains, contain face rate height, output is 1125 jin, does not use the wheat head of this conditioning agent, average three Mai Shan, 36 of 7 rows, and the little insatiable hunger of grain, output is 787 jin.Application process is: from the wheat flowering, spray once after above-mentioned finished product soup being converted the water dilution by 1: 400 times in ten days.
The experimenter: the old villager in the Hancheng City Zhi Chuan south of a town, Shaanxi Province is permitted sharp virtue, trying out above-mentioned conditioning agent situation on the booth tomato: after receiving custard squash last year, the tomato of in half mu of booth, planting again, planted seedling on April 12, began dead seedling on the 18th, fill the gaps with seedlings continuously, continuously dead seedling, prepare to abandon no matter the time, April 30, above-mentioned finished product soup on probation sprays once after converting the water dilution by 1: 500, does not have dead seedling again, fills spray once May 10 again subsequently, do not play any agricultural chemicals and bactericide again, last year, tomato came along fine, and bloomed that it is all better than former years to bear fruit, and output is than increasing more than 30% former years.
Experimenter: the northern old villager horse light in Hancheng City Zhi Chuan town, Shaanxi Province, try out above-mentioned conditioning agent situation at plastic tent cucumber: this year, one mu of plastic tent cucumber of planting is subjected to the downy mildew invasion and attack, still of no avail after the various sterilization agent on probation, melon is little and curved, turns white, there is not commodity value, April 21 sprayed above-mentioned conditioning agent on probation after seven days by 1: 400 times of dilution, and the climing new branch of beginning extraction that backs down of cucumber has grown new leaf, demutation in dead, after more than 20 day, begin the setting of blooming again on new long cucumber is climing, now sold two batches of cucumber, every batch two, 3,000 yuan of incomes, at present, melon is climing also in continuity, and income is all arranged every day.

Claims (3)

1. a pollution-free efficient plant growth regulator is characterized in that, it is to be made by the raw material of following weight parts:
Earthworm 18-28 part; Levisticum 15-23 part;
5 nitroguaiacol sodium 15-25 part; Dried rhizome of rehmannia 18-28 part;
Golden cypress 15-28 part; Umbellate pore furgus 15-28 part.
2. plant growth regulator according to claim 1 is characterized in that, the weight of each raw material (part) proportioning is:
25 parts of earthworms; 20 parts of levisticums;
20 parts in 5 nitroguaiacol sodium; 25 parts in the dried rhizome of rehmannia;
20 parts of golden cypresses; 20 parts of umbellate pore furgus.
3. the preparation method of claim 1 or 2 described plant growth regulator is characterized in that, described preparation method may further comprise the steps:
A) raw material is handled proportioning in accordance with regulations and is chosen drying, clean traditional Chinese medicine raw material earthworm, levisticum, the dried rhizome of rehmannia, golden cypress, umbellate pore furgus, each Chinese medicine material is put into liquor potassic permanganate respectively soaked 10-20 minute, carries out sterilization treatment; The content of regulation proportioning is dissolved in greater than 95% the former powder of 5 nitroguaiacol sodium disappears moltenly in the water of its 70-75 times weight, stir, place standby;
B) classification is soaked each traditional Chinese medicine will carry out after the sterilization treatment and is inserted respectively in the distilled water and soaked 20-26 hour, places in the cool after the taking-up 10-12 hour;
C) squeeze the juice to purify and each Chinese medicine material is put into crusher respectively squeeze juice, each juice that squeezes is crossed 200 orders and 100 mesh sieve impurity eliminations respectively, placed in the cool respectively 25-30 hour then, standby;
D) hybrid reaction whole Chinese medicine juices that will squeeze and the 5 nitroguaiacol sodium solution that configures are inserted in the reaction vessel and are mixed, and after stirring, maintain the temperature under 15-20 ℃, place and react in 70-72 hour;
E) the enfeoffment packing is taken out the liquid after the hybrid reaction, through after the assay was approved, and the enfeoffment packing, soup gets product.
CN 200910022913 2009-06-11 2009-06-11 Pollution-free efficient plant growth regulator and preparation method thereof Expired - Fee Related CN101919419B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103734192A (en) * 2013-10-22 2014-04-23 兰在明 Plant growth regulator
CN107006517A (en) * 2017-04-12 2017-08-04 江苏金凤凰农化有限公司 A kind of composition and application process that peach shot hole is treated based on guaiacol

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
汪接清: "介绍酒精对部分中药的防虫方法", 《中国中药杂志》 *
王树元: "温经养营汤治疗寒湿性坐骨神经痛", 《山东医药》 *
郑国庆等: "周围神经疾病三则例析", 《中医药学刊》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103734192A (en) * 2013-10-22 2014-04-23 兰在明 Plant growth regulator
CN107006517A (en) * 2017-04-12 2017-08-04 江苏金凤凰农化有限公司 A kind of composition and application process that peach shot hole is treated based on guaiacol

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Granted publication date: 20130417