CN101912419B - Instant donkey-hide glue powder and preparation method thereof - Google Patents
Instant donkey-hide glue powder and preparation method thereof Download PDFInfo
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- CN101912419B CN101912419B CN2010102601071A CN201010260107A CN101912419B CN 101912419 B CN101912419 B CN 101912419B CN 2010102601071 A CN2010102601071 A CN 2010102601071A CN 201010260107 A CN201010260107 A CN 201010260107A CN 101912419 B CN101912419 B CN 101912419B
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Abstract
The invention relates to instant donkey-hide glue powder and a preparation method thereof. The preparation method for the instant donkey-hide glue powder comprises the following steps: heating and dissolving finished donkey-hide glue in water, adding a proper amount of tween-20, glycerin monostearate and a proper amount of sweetener according to a proportion, drying under the conditions of low temperature and vacuum, and smashing to obtain a finish product. The finished product instant donkey-hide glue powder retains original active constituents and color of the donkey-hide glue and dispersibility thereof is reduced from 154s to 15s, thereby obviously improving the instant of the donkey-hide glue powder in water and effectively removing the original fishy smell of the donkey-hide glue. The method has less equipment investment, simple and practicable technology, stable product property, convenient eating and high economic benefit, and is an ideal method for producing the instant donkey-hide glue powder.
Description
Technical field
The invention belongs to Colla Corii Asini powder preparation field, be specifically related to a kind of instant ass-hide gelatin powder and preparation method thereof.
Background technology
Colla Corii Asini is China's Chinese medicine, is to boil the glue that forms after the skin unhairing by the equine species donkey.The traditional Chinese medical science thinks that Colla Corii Asini sweet in the mouth, property are flat, and nourishing YIN and moistening the lung is enriched blood, stopped blooding, and multiple hemorrhages such as Colla Corii Asini is applicable to asthenia spitting of blood, haematemesis, hematuria, has blood in stool, metrorrhagia also are used for YIN damaged by pathogenic heat, the dysphoria and insomnia due to the deficiency of YIN imbalance; Colla Corii Asini energy nourishing YIN to lower pathogenic fire also is used for lung-dryness syndrome due to deficiency of YIN, and cough expectorant is few, dry laryngopharynx.Record Colla Corii Asini in " herbal classic " " collapse in the main trusted subordinate, the extremely voluminous symptoms like malaria of labor, waist stomachache, extremities aching pain, woman's hematochezia, antiabortive ".Put down in writing Colla Corii Asini in the Compendium of Material Medica and " treat haematemesis, epistaxis, loss of fecundity, metrorrhagia, leukorrhagia, tire all diseases in preceding puerperal; Cough due to consumptive disease, dyspnea with rapid respiration, consumptive lung disease spitting bloody pus and blood YIN nourishing are removed wind and are moisturized the lung heat clearing of reducing phlegm ".
Colla Corii Asini is the treasure in motherland's medicine treasure-house, contains abundant collagen protein, polypeptide and several amino acids, is traditional Chinese medical science hematonic commonly used, has significant curative effect and magical nutritious tonifying effect, is subjected to the welcome of users at home and abroad deeply.But traditional Colla Corii Asini mainly is the Colla Corii Asini piece that becomes certain specification through very long working procedure processing, must heat stewedization when taking, and brings very big inconvenience to user.And slow, the easily conglomeration of melting speed when reconstituting with hot water of traditional Colla Corii Asini powder, dispersibility is low, instant capacity is poor, organoleptic quality is not good.
As primary raw material, can make several formulations with Colla Corii Asini in conjunction with other Chinese medicines or other health nutrient compositions.Though Colla Corii Asini product and the technology applied for a patent are more, be 200710016052.8 patent disclosure as application number " instant ass-hide gelatin powder and preparation thereof and preparation method ", but formula for a product is different with the present invention, and dry run adopts is the extruding puffing method, and the raising of product instant capacity and the removal of fishy smell fail to reach rational effect; Application number be 03139055.2 patent disclosure " instant e-jiao granules and preparation method thereof ", formula for a product is also different with the present invention, product belongs to granule rather than Colla Corii Asini powder, the course of processing does not adopt vacuum drying technique yet; Application number be 88105312.0 patent disclosure " powder quick dissolving donkey-hide gelatin ", but formula for a product is also different with the present invention, what the course of processing adopted is microwave drying, rather than vacuum drying.
Though several " instant ass-hide gelatins ", " instant Colla Corii Asini " have occurred in producing at present, because the problem of Technology, the instant capacity of Colla Corii Asini is not still effectively solved.The primary raw material donkey skin of adding Colla Corii Asini production is subject to the occurring in nature contamination by micro, can generate alkaline total volatile basic nitrogen after the fermentation corruption, occurs unusual taste when taking, and allows consumer be difficult to accept, and this problem is also effectively solved so far.
Summary of the invention
The technical problem to be solved in the present invention is: at the shortcoming and the deficiency of prior art existence, it is simple to the invention discloses a kind of technology, with short production cycle, equipment investment is few, the preparation method of the instant ass-hide gelatin powder of energy-conserving and environment-protective adopts the Colla Corii Asini powder of this method preparation to keep original sepia of Colla Corii Asini and gloss, no fishy smell, have the organoleptic quality height, and dispersibility, instant capacity advantages of higher.
At above-mentioned technical problem, the present invention proposes following technical scheme:
1) takes by weighing 100 parts of Colla Corii Asini by mass fraction, 1.2-1.6 part tween 20,0.4-0.8 part molecular distillation glyceryl monostearate and 0.05-0.1 part sweeting agent;
2) tween 20 and the molecular distillation glyceryl monostearate that takes by weighing got the compound emulsion agent solution with its quality 1.5-2 hot water dissolving of 80-100 ℃ doubly;
3) sweeting agent that takes by weighing is got edulcorant aqueous solution with the water dissolution of 1-2 times of quality;
4) Colla Corii Asini that takes by weighing is added in the water of 1.5-2.5 times of quality, heat then, stir Colla Corii Asini is dissolved, continuing heating concentrates the Colla Corii Asini that dissolves, the temperature of Colla Corii Asini is controlled at 85-100 ℃ in the concentration process, behind Colla Corii Asini simmer down to paste, slowly add compound emulsion agent solution and edulcorant aqueous solution successively, and make Colla Corii Asini and the abundant emulsifying of emulsifying agent by stirring, Colla Corii Asini after the emulsifying is continued down to concentrate at 85-100 ℃, when Colla Corii Asini becomes sticky thick and hang on the chamber wall easily, stop to heat donkey-hide gelatin mate;
5) donkey-hide gelatin mate is carried out low-temperature vacuum drying, vacuum drying condition is: the atmosphere temperature is 40-56 ℃ in the confined chamber, and vacuum is 60-600Pa, dried donkey-hide gelatin mate is pulverized and is crossed 60 mesh sieves and promptly get instant ass-hide gelatin powder.
Described sweeting agent is a sucralose;
The charge of donkey-hide gelatin mate is no more than 1000g in described vacuum drying every square metre of drying area, and be 90-120 minute drying time;
The instant ass-hide gelatin powder that described step 5) obtains was sterilized 2-3 minute under the 2450MHz microwave exposure.
By the instant donkey-hide glue powder that preparation method of the present invention is made, press mass fraction by 100 parts of Colla Corii Asini, 1.2-1.6 part tween 20,0.4-0.8 part molecular distillation glyceryl monostearate and 0.05-0.1 part sweeting agent are formed.
Beneficial effect of the present invention is embodied in: the preparation method of instant ass-hide gelatin powder of the present invention adopts vacuum drying method under lower baking temperature and higher vacuum degree condition Colla Corii Asini to be carried out drying, the moisture of Colla Corii Asini powder is not higher than 3%, the effective ingredient of Colla Corii Asini itself destroys few, total nitrogen content is up to more than 70%, Colla Corii Asini pink colour pool is attractive in appearance, the bulkiness height, instant capacity is good, use the boiled water Instant Drinks, dissolution time is no more than 15s, simultaneously, the total volatile basic nitrogen that is fishy smell in the Colla Corii Asini can access effective volatilization, removes the original fishy smell of Colla Corii Asini to greatest extent; It is raw material that the preparation method of instant ass-hide gelatin powder of the present invention adopts finished product Colla Corii Asini piece, and process equipment is simple, and processing technique is easy, and properties of product are stable, and the manufacturing enterprise that is suitable for various scales uses, and is good in economic efficiency.
The specific embodiment
The invention will be further described below in conjunction with embodiment.
Embodiment 1:
1) takes by weighing 100 parts of Colla Corii Asini by mass fraction, 1.5 parts of tween 20s, 0.4 part of molecular distillation glyceryl monostearate and 0.08 part of Sweetener Sucralose;
2) tween 20 that takes by weighing and molecular distillation glyceryl monostearate are got the compound emulsion agent solution with the hot water dissolving of 1.5 times 80-100 ℃ of its quality;
3) sweeting agent that takes by weighing is got edulcorant aqueous solution with the water dissolution of 1 times of quality;
4) Colla Corii Asini that takes by weighing is added in the water of 1.5 times of quality, heat then, stir Colla Corii Asini is dissolved, continuing heating concentrates the Colla Corii Asini that dissolves, the temperature of Colla Corii Asini is controlled at 90 ℃ in the concentration process, behind Colla Corii Asini simmer down to paste, slowly add compound emulsion agent solution and edulcorant aqueous solution successively, and make the abundant emulsifying of Colla Corii Asini by stirring, the Colla Corii Asini after the emulsifying is continued down to concentrate at 90 ℃, when Colla Corii Asini becomes sticky thick and hang on the chamber wall easily, stop to heat donkey-hide gelatin mate;
5) with the donkey-hide gelatin mate vacuum drying, vacuum drying condition is: the atmosphere temperature is 56 ℃ in the confined chamber, vacuum is 60Pa, the charge of donkey-hide gelatin mate is no more than 1000g in every square metre of drying area, and be 60 mesh sieves were pulverized and crossed to dried donkey-hide gelatin mate in 100 minutes promptly to get instant ass-hide gelatin powder drying time.
The instant ass-hide gelatin powder that step 5) obtains was sterilized 2-3 minute under the 2450MHz microwave exposure.
By the instant donkey-hide glue powder that preparation method of the present invention is made, press mass fraction by 100 parts of Colla Corii Asini, 1.5 parts of tween 20s, 0.4 part of molecular distillation glyceryl monostearate and 0.08 part of sweeting agent are formed.
Finished product is slightly pleasantly sweet, no fishy smell, and dispersibility is 14s, and total nitrogen content is not less than 70%, and moisture is not higher than 3%.
Embodiment 2:
1) takes by weighing 100 parts of Colla Corii Asini by mass fraction, 1.3 parts of tween 20s, 0.6 part of molecular distillation glyceryl monostearate and 0.05 part of Sweetener Sucralose;
2) tween 20 that takes by weighing and molecular distillation glyceryl monostearate are got the compound emulsion agent solution with the hot water dissolving of 2 times 80-100 ℃ of its quality;
3) sweeting agent that takes by weighing is got edulcorant aqueous solution with the water dissolution of 2 times of quality;
4) Colla Corii Asini that takes by weighing is added in the water of 2 times of quality, heat then, stir Colla Corii Asini is dissolved, continuing heating concentrates the Colla Corii Asini that dissolves, the temperature of Colla Corii Asini is controlled at 85 ℃ in the concentration process, behind Colla Corii Asini simmer down to paste, slowly add compound emulsion agent solution and edulcorant aqueous solution successively, and make the abundant emulsifying of Colla Corii Asini by stirring, the Colla Corii Asini after the emulsifying is continued down to concentrate at 85 ℃, when Colla Corii Asini becomes sticky thick and hang on the chamber wall easily, stop to heat donkey-hide gelatin mate;
5) with the donkey-hide gelatin mate vacuum drying, vacuum drying condition is: the atmosphere temperature is 40 ℃ in the confined chamber, vacuum is 60Pa, the charge of donkey-hide gelatin mate is no more than 1000g in every square metre of drying area, and be 60 mesh sieves were pulverized and crossed to dried donkey-hide gelatin mate in 110 minutes promptly to get instant ass-hide gelatin powder drying time.
The instant ass-hide gelatin powder that step 5) obtains was sterilized 2-3 minute under the 2450MHz microwave exposure.
By the instant donkey-hide glue powder that preparation method of the present invention is made, press mass fraction by 100 parts of Colla Corii Asini, 1.3 parts of tween 20s, 0.6 part of molecular distillation glyceryl monostearate and 0.05 part of sweeting agent are formed.
Finished product is pleasantly sweet, no fishy smell, and dispersibility is 15s, and total nitrogen content is not less than 70%, and moisture is not higher than 3%.
Embodiment 3:
1) takes by weighing 100 parts of Colla Corii Asini by mass fraction, 1.6 parts of tween 20s, 0.5 part of molecular distillation glyceryl monostearate and 0.07 part of Sweetener Sucralose;
2) tween 20 that takes by weighing and molecular distillation glyceryl monostearate are got the compound emulsion agent solution with the hot water dissolving of 1.8 times 80-100 ℃ of its quality;
3) sweeting agent that takes by weighing is got edulcorant aqueous solution with the water dissolution of 1.5 times of quality;
4) Colla Corii Asini that takes by weighing is added in the water of 1.8 times of quality, heat then, stir Colla Corii Asini is dissolved, continuing heating concentrates the Colla Corii Asini that dissolves, the temperature of Colla Corii Asini is controlled at 100 ℃ in the concentration process, behind Colla Corii Asini simmer down to paste, slowly add compound emulsion agent solution and edulcorant aqueous solution successively, and make the abundant emulsifying of Colla Corii Asini by stirring, the Colla Corii Asini after the emulsifying is continued down to concentrate at 100 ℃, when Colla Corii Asini becomes sticky thick and hang on the chamber wall easily, stop to heat donkey-hide gelatin mate;
5) with the donkey-hide gelatin mate vacuum drying, vacuum drying condition is: the atmosphere temperature is 45 ℃ in the confined chamber, vacuum is 100Pa, the charge of donkey-hide gelatin mate is no more than 1000g in every square metre of drying area, and be 60 mesh sieves were pulverized and crossed to dried donkey-hide gelatin mate in 90 minutes promptly to get instant ass-hide gelatin powder drying time.
The instant ass-hide gelatin powder that step 5) obtains was sterilized 2-3 minute under the 2450MHz microwave exposure.
By the instant donkey-hide glue powder that preparation method of the present invention is made, press mass fraction by 100 parts of Colla Corii Asini, 1.6 parts of tween 20s, 0.5 part of molecular distillation glyceryl monostearate and 0.07 part of sweeting agent are formed.
Finished product is pleasantly sweet, no fishy smell, and dispersibility is 14s, and total nitrogen content is not less than 70%, and moisture is not higher than 3%.
Embodiment 4:
1) takes by weighing 100 parts of Colla Corii Asini by mass fraction, 1.4 parts of tween 20s, 0.7 part of molecular distillation glyceryl monostearate and 0.09 part of Sweetener Sucralose;
2) tween 20 that takes by weighing and molecular distillation glyceryl monostearate are got the compound emulsion agent solution with the hot water dissolving of 1.6 times 80-100 ℃ of its quality;
3) sweeting agent that takes by weighing is got edulcorant aqueous solution with the water dissolution of 1.8 times of quality;
4) Colla Corii Asini that takes by weighing is added in the water of 2.3 times of quality, heat then, stir Colla Corii Asini is dissolved, continuing heating concentrates the Colla Corii Asini that dissolves, the temperature of Colla Corii Asini is controlled at 95 ℃ in the concentration process, behind Colla Corii Asini simmer down to paste, slowly add compound emulsion agent solution and edulcorant aqueous solution successively, and make the abundant emulsifying of Colla Corii Asini by stirring, the Colla Corii Asini after the emulsifying is continued down to concentrate at 95 ℃, when Colla Corii Asini becomes sticky thick and hang on the chamber wall easily, stop to heat donkey-hide gelatin mate;
5) with the donkey-hide gelatin mate vacuum drying, vacuum drying condition is: the atmosphere temperature is 52 ℃ in the confined chamber, vacuum is 300Pa, the charge of donkey-hide gelatin mate is no more than 1000g in every square metre of drying area, and be 60 mesh sieves were pulverized and crossed to dried donkey-hide gelatin mate in 120 minutes promptly to get instant ass-hide gelatin powder drying time.
The instant ass-hide gelatin powder that step 5) obtains was sterilized 2-3 minute under the 2450MHz microwave exposure.
By the instant donkey-hide glue powder that preparation method of the present invention is made, press mass fraction by 100 parts of Colla Corii Asini, 1.4 parts of tween 20s, 0.7 part of molecular distillation glyceryl monostearate and 0.09 part of sweeting agent are formed.
Finished product is slightly pleasantly sweet, no fishy smell, and dispersibility is 15s, and total nitrogen content is not less than 70%, and moisture is not higher than 3%.
Embodiment 5:
1) takes by weighing 100 parts of Colla Corii Asini by mass fraction, 1.2 parts of tween 20s, 0.8 part of molecular distillation glyceryl monostearate and 0.1 part of Sweetener Sucralose;
2) tween 20 that takes by weighing and molecular distillation glyceryl monostearate are got the compound emulsion agent solution with the hot water dissolving of 1.7 times 80-100 ℃ of its quality;
3) sweeting agent that takes by weighing is got edulcorant aqueous solution with the water dissolution of 1.3 times of quality;
4) Colla Corii Asini that takes by weighing is added in the water of 2.5 times of quality, heat then, stir Colla Corii Asini is dissolved, continuing heating concentrates the Colla Corii Asini that dissolves, the temperature of Colla Corii Asini is controlled at 93 ℃ in the concentration process, behind Colla Corii Asini simmer down to paste, slowly add compound emulsion agent solution and edulcorant aqueous solution successively, and make the abundant emulsifying of Colla Corii Asini by stirring, the Colla Corii Asini after the emulsifying is continued down to concentrate at 93 ℃, when Colla Corii Asini becomes sticky thick and hang on the chamber wall easily, stop to heat donkey-hide gelatin mate;
5) with the donkey-hide gelatin mate vacuum drying, vacuum drying condition is: the atmosphere temperature is 50 ℃ in the confined chamber, vacuum is 500Pa, the charge of donkey-hide gelatin mate is no more than 1000g in every square metre of drying area, and be 60 mesh sieves were pulverized and crossed to dried donkey-hide gelatin mate in 105 minutes promptly to get instant ass-hide gelatin powder drying time.
The instant ass-hide gelatin powder that step 5) obtains was sterilized 2-3 minute under the 2450MHz microwave exposure.
By the instant donkey-hide glue powder that preparation method of the present invention is made, press mass fraction by 100 parts of Colla Corii Asini, 1.2 parts of tween 20s, 0.8 part of molecular distillation glyceryl monostearate and 0.1 part of sweeting agent are formed.
Finished product is slightly pleasantly sweet, no fishy smell, and dispersibility is 15s, and total nitrogen content is not less than 70%, and moisture is not higher than 3%.
The present invention heats finished product Colla Corii Asini piece that to add a certain amount of tween 20, molecular distillation glyceryl monostearate and an amount of sweeting agent in proportion after dissolving be sucralose in water, crushed after being dried makes finished product under the cryogenic vacuum condition again.Finished product had both kept Colla Corii Asini original active ingredients and color and luster, again dispersibility had been shortened to 15s from original 154s, had significantly improved the instant capacity of Colla Corii Asini powder in water, and the original fishy smell of Colla Corii Asini is effectively removed.Finished product is slightly pleasantly sweet, no fishy smell, and total nitrogen content is not less than 70%, and moisture is not higher than 3%.
Claims (5)
1. the preparation method of an instant ass-hide gelatin powder is characterized in that may further comprise the steps:
1) takes by weighing 100 parts of Colla Corii Asini by mass fraction, 1.2-1.6 part tween 20,0.4-0.8 part molecular distillation glyceryl monostearate and 0.05-0.1 part sweeting agent;
2) tween 20 and the molecular distillation glyceryl monostearate that takes by weighing got the compound emulsion agent solution with its quality 1.5-2 hot water dissolving of 80-100 ℃ doubly;
3) sweeting agent that takes by weighing is got edulcorant aqueous solution with the water dissolution of 1-2 times of quality;
4) Colla Corii Asini that takes by weighing is added in the water of 1.5-2.5 times of quality, heat then, stir Colla Corii Asini is dissolved, continuing heating concentrates the Colla Corii Asini that dissolves, the temperature of Colla Corii Asini is controlled at 85-100 ℃ in the concentration process, behind Colla Corii Asini simmer down to paste, slowly add compound emulsion agent solution and edulcorant aqueous solution successively, and make Colla Corii Asini and the abundant emulsifying of emulsifying agent by stirring, Colla Corii Asini after the emulsifying is continued down to concentrate at 85-100 ℃, when Colla Corii Asini becomes sticky thick and hang on the chamber wall easily, stop to heat donkey-hide gelatin mate;
5) donkey-hide gelatin mate is carried out low-temperature vacuum drying, vacuum drying condition is: the atmosphere temperature is 40-56 ℃ in the confined chamber, and vacuum is 60-600Pa, dried donkey-hide gelatin mate is pulverized and is crossed 60 mesh sieves and promptly get instant ass-hide gelatin powder.
2. the preparation method of instant ass-hide gelatin powder according to claim 1, it is characterized in that: described sweeting agent is a sucralose.
3. the preparation method of instant ass-hide gelatin powder according to claim 1, it is characterized in that: the charge of donkey-hide gelatin mate is no more than 1000g in described vacuum drying every square metre of drying area, and be 90-120 minute drying time.
4. according to the preparation method of the described a kind of instant ass-hide gelatin powder of claim 1, it is characterized in that: the instant ass-hide gelatin powder that described step 5) obtains was sterilized 2-3 minute under the 2450MHz microwave exposure.
5. the instant ass-hide gelatin powder made of the preparation method of instant ass-hide gelatin powder according to claim 1, it is characterized in that: press mass fraction by 100 parts of Colla Corii Asini, 1.2-1.6 part tween 20,0.4-0.8 part molecular distillation glyceryl monostearate and 0.05-0.1 part sweeting agent are formed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102601071A CN101912419B (en) | 2010-08-23 | 2010-08-23 | Instant donkey-hide glue powder and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102601071A CN101912419B (en) | 2010-08-23 | 2010-08-23 | Instant donkey-hide glue powder and preparation method thereof |
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| Publication Number | Publication Date |
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| CN101912419A CN101912419A (en) | 2010-12-15 |
| CN101912419B true CN101912419B (en) | 2011-12-28 |
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Families Citing this family (5)
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| CN103598606B (en) * | 2013-10-30 | 2015-03-25 | 辽宁鹿滋堂生物科技有限公司 | Instantly soluble deer glue radix astragali powder and preparation method thereof |
| CN106074862A (en) * | 2016-08-26 | 2016-11-09 | 山东东阿东盛阿胶产品科技开发有限公司 | A kind of Colla Corii Asini powder of suppressing the hyperactive liver improving eyesight and preparation method thereof |
| CN108926524B (en) * | 2018-01-30 | 2020-07-17 | 东阿阿胶股份有限公司 | Instant gelatin product block and preparation method thereof |
| CN109453122A (en) * | 2018-12-25 | 2019-03-12 | 东阿阿胶股份有限公司 | A kind of glue class Chinese-medicine oral cavity dissolution formulation and preparation method |
| CN111671092A (en) * | 2020-06-09 | 2020-09-18 | 北京东升制药有限公司 | Preparation method of instant donkey-hide gelatin |
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