CN101903095B - 制备胺的方法 - Google Patents

制备胺的方法 Download PDF

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Publication number
CN101903095B
CN101903095B CN200880122274.0A CN200880122274A CN101903095B CN 101903095 B CN101903095 B CN 101903095B CN 200880122274 A CN200880122274 A CN 200880122274A CN 101903095 B CN101903095 B CN 101903095B
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China
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catalyst
process according
weight
calculated
ammonia
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Expired - Fee Related
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CN200880122274.0A
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English (en)
Chinese (zh)
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CN101903095A (zh
Inventor
P·库巴内克
W·麦格莱恩
E·施瓦布
J-P·梅尔德
M·尤利乌斯
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BASF SE
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BASF SE
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/835—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with germanium, tin or lead
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16—Reducing
    • B01J37/18—Reducing with gases containing free hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
    • C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/06—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by halogen atoms or nitro radicals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
CN200880122274.0A 2007-12-21 2008-12-10 制备胺的方法 Expired - Fee Related CN101903095B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP07150408.8 2007-12-21
EP07150408 2007-12-21
PCT/EP2008/067183 WO2009080507A1 (de) 2007-12-21 2008-12-10 Verfahren zur herstellung eines amins

Publications (2)

Publication Number Publication Date
CN101903095A CN101903095A (zh) 2010-12-01
CN101903095B true CN101903095B (zh) 2013-07-10

Family

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Family Applications (1)

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CN200880122274.0A Expired - Fee Related CN101903095B (zh) 2007-12-21 2008-12-10 制备胺的方法

Country Status (6)

Country Link
US (1) US8278489B2 (enExample)
EP (1) EP2225029B1 (enExample)
JP (1) JP5528349B2 (enExample)
CN (1) CN101903095B (enExample)
TW (1) TW200936547A (enExample)
WO (1) WO2009080507A1 (enExample)

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CN101489979B (zh) * 2006-07-14 2015-04-08 巴斯夫欧洲公司 生产胺的方法
CN101903096B (zh) * 2007-12-21 2013-04-03 巴斯夫欧洲公司 生产胺的方法
EP2225030B1 (de) * 2007-12-21 2012-04-18 Basf Se Verfahren zur herstellung eines amins
WO2009080506A1 (de) * 2007-12-21 2009-07-02 Basf Se Verfahren zur herstellung eines amins
CN102159311B (zh) * 2008-09-19 2013-07-10 巴斯夫欧洲公司 使用铝-铜催化剂连续制备胺的方法
CN102203054B (zh) 2008-11-05 2014-07-30 巴斯夫欧洲公司 生产n，n-取代的3-氨基丙-1-醇的方法
US8466323B2 (en) 2008-12-19 2013-06-18 Basf Se Process for preparing pure triethanolamine (TEOA)
DE102008063308B4 (de) 2008-12-29 2013-03-07 Basf Se Verfahren zur Herstellung von Toluylendiamin durch Hydrierung von Dinitrotoluol
JP2012526741A (ja) 2009-05-14 2012-11-01 ビーエーエスエフ ソシエタス・ヨーロピア 芳香族アミンの製造方法
KR101753921B1 (ko) 2009-07-10 2017-07-04 바스프 에스이 수소의 전기화학적 분리에 의한 탄화수소의 아미노탄화수소로의 직접 아미노화 방법
US8642810B2 (en) 2009-07-10 2014-02-04 Basf Se Method for the direct amination of hydrocarbons into amino hydrocarbons, including electrochemical separation of hydrogen and electrochemical reaction of the hydrogen into water
SG181100A1 (en) 2009-12-03 2012-07-30 Basf Se Catalyst and method for producing an amine
EP2506965B1 (de) 2009-12-03 2016-11-09 Basf Se Katalysator und verfahren zur herstellung eines amins
US8637668B2 (en) 2010-06-15 2014-01-28 Basf Se Process for preparing a cyclic tertiary methylamine
US8933223B2 (en) 2010-10-14 2015-01-13 Basf Se Process for preparing a cyclic tertiary amine
JP5879123B2 (ja) * 2011-12-27 2016-03-08 花王株式会社 ３級アミンの製造方法
WO2013178534A1 (de) 2012-06-01 2013-12-05 Basf Se Verfahren zur herstellung eines mono-n-alkyl-piperazins
IN2014DN10668A (enExample) 2012-06-01 2015-08-28 Basf Se
US8884015B2 (en) 2012-06-01 2014-11-11 Basf Se Process for the preparation of a mono-N-alkypiperazine
US8981093B2 (en) 2012-06-06 2015-03-17 Basf Se Process for preparing piperazine
EP2858978A1 (de) 2012-06-06 2015-04-15 Basf Se Verfahren zur herstellung von piperazin
WO2013182465A1 (de) 2012-06-06 2013-12-12 Basf Se Verfahren zur herstellung von piperazin
US9315479B2 (en) 2012-07-13 2016-04-19 Basf Se Process for preparing pyrrolidine
EP2872494B1 (de) * 2012-07-13 2016-06-15 Basf Se Verfahren zur herstellung von pyrrolidin
WO2014184039A1 (de) 2013-05-16 2014-11-20 Basf Se Verfahren zur herstellung von n-alkyl-piperazinen
US11274072B2 (en) 2017-11-30 2022-03-15 Basf Se Process for the continuous preparation of 1,2-propylene diamine (1,2-PDA) and dimethyldiethylene triamine (DMDETA)
EP3765451B1 (de) 2018-03-15 2022-02-23 Basf Se Verfahren zum entfernen von methoxyethanol aus einem methoxyethanol und morpholin enthaltenden gemisch
WO2021110472A1 (de) * 2019-12-03 2021-06-10 Basf Se Verfahren zur herstellung von aminen an einem kupferhaltigen katalysator
CN111118899A (zh) * 2019-12-26 2020-05-08 安徽元琛环保科技股份有限公司 一种滤料用抗硫酸氢铵整理剂的制备方法与应用
US20250074865A1 (en) 2022-01-14 2025-03-06 Basf Se Method for the manufacture or conversion of alkanolamines
CN117358239A (zh) * 2022-06-30 2024-01-09 中国石油化工股份有限公司 烷基二胺的制备方法
WO2025157662A1 (en) * 2024-01-26 2025-07-31 Basf Se Process for the manufacture of chemical products and passivation of heterogeneous metal catalysts

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Also Published As

Publication number Publication date
JP2011506529A (ja) 2011-03-03
WO2009080507A1 (de) 2009-07-02
US8278489B2 (en) 2012-10-02
JP5528349B2 (ja) 2014-06-25
EP2225029B1 (de) 2016-08-03
CN101903095A (zh) 2010-12-01
US20110054167A1 (en) 2011-03-03
EP2225029A1 (de) 2010-09-08
TW200936547A (en) 2009-09-01

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Granted publication date: 20130710

Termination date: 20191210