CN101869541B - Skin care product comprising plant extract and preparation method thereof - Google Patents
Skin care product comprising plant extract and preparation method thereof Download PDFInfo
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- CN101869541B CN101869541B CN2010102302652A CN201010230265A CN101869541B CN 101869541 B CN101869541 B CN 101869541B CN 2010102302652 A CN2010102302652 A CN 2010102302652A CN 201010230265 A CN201010230265 A CN 201010230265A CN 101869541 B CN101869541 B CN 101869541B
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Abstract
The invention belongs to the technical field of skin care products and particularly relates to a skin care product comprising a plant extract and a preparation method thereof. The key points of the invention are that firstly an organic solvent extraction method or a steam distillation method is adopted to extract clove volatile oil and safflower volatile oil; then water is added into pseudo-ginseng and the mixture of clove and safflower which are subjected to volatile oil extraction so as to extract active ingredients of pseudo-ginseng, clove and safflower; the extracted clove volatile oil, extracted safflower volatile oil and the active ingredients of the pseudo-ginseng, clove and safflower are added into other effective ingredients according to a certain proportion to prepare the skin care product of the invention. The skin care product of the invention has the advantages of simple preparation method, natural product, no toxic or side effect, civilian price and better curative effect on pachylosis and rhagadia.
Description
Technical field
The invention belongs to technical field of skin care, be specifically related to a kind of skin care item that contain plant extract and preparation method thereof.
Background technology
Along with greatly enriching of socioeconomic continuous progress and material life; Skin care item; No longer be to have only the rich or the thing that has of the talent inside the city in the past, skin care item have been come into common people or common peasant's friends, because ordinary people and friend peasant are engaged in outwork mostly; More be easy to generate skin problem, more need draw attention and obtain care.Skin care item are playing great effect aspect the lifting of the spirit of giving people, image.At first, it has the function of skin maintenance, can strengthen the elasticity and the vigor of skin, and often use can make the people young, beautiful.Secondly, it has strengthened people's self-confidence, has promoted people's fine image, has promoted social civilization.And at present, it is a feast for the eyes that the skin care item on the market can be said so, of a great variety, and characteristics are different.The maturation of the consumption concept of Along with people's, much human know gradually why expensive expensive goods is, might not be senior especially or rare because of the composition of product, and its research and development and advertising and publicity cost are also not necessarily much higher than low-and-medium-grade products.To some degree, they are expensive, only because market orientation is like this, so that the price of product can be described as is high utterly unjustifiable.And; People are also developed to the direction of " naturalization, nutrient laden, curative effectization " the requirement of skin care item, and from eighties of last century eighties, the skin expert just finds; In skin care item, add various natural materials; Skin is had certain moist effect, and have no side effect, particularly effective component extracting adds in the skin care item from plant.Therefore, naturalization of exploitation composition, the popular skin care item of price are trends of the times.
Summary of the invention
First purpose of the present invention provides a kind of skin care item that from Flos Caryophylli, Flos Carthami, extract volatile oil and from Flos Caryophylli, Flos Carthami, Radix Notoginseng, extract other active component that contain.
Second purpose of the present invention provides the method for preparing of these skin care item.
First purpose of the present invention is achieved in that this skin care item, and it consists of: component a, components b and amount of component b; Wherein, the composition of component a is: the hexadecanol of 4 ~ 6 weight portions, the lanoline of 5 ~ 10 weight portions; The white oil of 2 ~ 3 weight portions, the Cera Flava of 5 ~ 7 weight portions, the azone of 0.5 ~ 1 weight portion; The squalane of 3 ~ 5 weight portions, the vaseline of 0 ~ 2 weight portion, the dimethyl-silicon of 0 ~ 1 weight portion; The Flos Caryophylli of 10 ~ 15 weight portions, Flos Carthami extract, the Radix Notoginseng extract of 5 ~ 10 weight portions; The composition of components b is: the potassium sorbate of 2 ~ 3 weight portions, and the glycerol of 10 ~ 20 weight portions, the propylene glycol of 2 ~ 7 weight portions, the dibenzylatiooluene of 0.05 ~ 0.15 weight portion, making total weight portion is 100 deionized water; The composition of amount of component b is: the Flos Caryophylli of 1 ~ 3 weight portion, Flos Carthami volatile oil, the essence of 0.02 weight portion, the antiseptic of 0.02 weight portion.
Said Flos Caryophylli extract contains eugenol, syringone, oleanolic acid, flavone, vitamin; Flos Carthami extract contains carthamone, neocarthamin, saffloside, Carthamus yellow, flavone; Radix Notoginseng extract contains ginseng saponin, arasaponin, Radix Notoginseng flavone, Quercetin, β-steroid, polypeptide element, polysaccharide and ferrum, rubidium, strontium; Said Flos Caryophylli volatile oil contains eugenol, acetyleugenol, syringone, eugenin, oleanolic acid, flavone; Flos Carthami volatile oil contains Palmic acid, myristic acid, lauric acid, stearic acid, arachidic acid, oleic acid.
Second purpose of the present invention is achieved in that this method for preparing comprises the step of following order:
(1) extraction step of Flos Caryophylli, Flos Carthami volatile oil: can adopt the organic solvent extraction method, after soon Flos Caryophylli, Flos Carthami are distinguished drying, pulverizing, petroleum ether reflux, extract, three times; Merge extractive liquid,, concentrating under reduced pressure, extractum with dissolve with ethanol after; Hold over night; Centrifugal, the supernatant concentrating under reduced pressure gets volatile oil; Also can adopt steam distillation, soon after Flos Caryophylli, Flos Carthami drying, the pulverizing, add the water of 5 ~ 10 times of amounts, preimpregnation is after 1 ~ 2 hour, and the reuse steam distillation carries out volatile oil and extracts;
Said Flos Caryophylli, Flos Carthami volatile oil can extract respectively, extract simultaneously after also can the two being mixed;
(2) extraction step of Flos Caryophylli, Flos Carthami, pseudo-ginseng activity composition: add 3 ~ 5 times of water gagings in the Flos Caryophylli behind Radix Notoginseng and extraction volatile oil, the Flos Carthami mixture; Decocted 2 ~ 3 hours; Filter, the ethanol precipitation that in filtrating, adds equivalent is removed impurity, and filtrating is condensed into dense extracting solution or extractum;
Said Flos Caryophylli, Flos Carthami, pseudo-ginseng activity composition can extract respectively, extract simultaneously after also can the three being mixed;
(3) prepare component a, the step of components b and amount of component b:
The composition of component a is: the hexadecanol of 4 ~ 6 weight portions, the lanoline of 5 ~ 10 weight portions, the white oil of 2 ~ 3 weight portions; The Cera Flava of 5 ~ 7 weight portions, the azone of 0.5 ~ 1 weight portion, the squalane of 3 ~ 5 weight portions; The vaseline of 0 ~ 2 weight portion; The dimethyl-silicon of 0 ~ 1 weight portion, the Flos Caryophylli of 10 ~ 15 weight portions, Flos Carthami extract, the Radix Notoginseng extract of 5 ~ 10 weight portions;
The composition of components b is: the potassium sorbate of 2 ~ 3 weight portions, and the glycerol of 10 ~ 20 weight portions, the propylene glycol of 2 ~ 7 weight portions, the dibenzylatiooluene of 0.05 ~ 0.15 weight portion, making total weight portion is 100 deionized water;
The composition of amount of component b is: the Flos Caryophylli of 1 ~ 3 weight portion, Flos Carthami volatile oil, the essence of 0.02 weight portion, the antiseptic of 0.02 weight portion;
(4) with component a, components b respectively be heated under the stirring 75 ℃ ~ 85 ℃ become homogeneous phases after, component a is added in the emulsifying pot, insulation is at 80 ℃; Evacuation is opened the homogenizing blender, and the control stir speed (S.S.) is 3000 rev/mins; Components b is joined in the emulsifying pot fast, continue to stir 5 minutes;
(5) stop heating, continue to stir, treat to add amount of component b when temperature is reduced to 50 ℃, open vacuum pump, evacuation continued to be cooled to 40 ℃ after 15 ~ 20 minutes, and with Fructus Citri Limoniae acid for adjusting pH value to 6.0 ~ 7.0, discharging promptly gets product.
Genus Syringa Myrtaceae syzygium species plant among the present invention is a kind of medicine food dual purpose plant.It is Oleum Caryophylli that the Flos Caryophylli alabastrum contains volatile oil, mainly contains eugenol, acetyleugenol, syringone, eugenin, oleanolic acid, flavone etc. in the oil; It has anti-respiratory system and urinary system infection, improves weak body constitution and anemia, blood circulation promoting, and treatment skin ulcer and wound inflammation improve effects such as coarse skin, skin whitening.
Flos Caryophylli extract then contains eugenol, syringone, oleanolic acid, flavone, vitamin etc., and skin is had the nourishing protective effect, can strengthen the immunity of skin, the elasticity of protection epidermis cell and skin, delaying decrepitude of skin.
Flos Carthami among the present invention is drafted a document this plant for the Compositae Flos Carthami.Contain carthamone, neocarthamin, saffloside, Carthamus yellow, flavone and Flos Carthami wet goods in the Flos Carthami, then comprise Palmic acid, myristic acid, lauric acid, stearic acid, arachidic acid, oleic acid etc. in the safflower oil.Flos Carthami has slight excited heart, increases the effect of coronary flow and myocardial nutrition property blood flow; Ability fortifying fibre protein dissolution reduces WBV.Flos Carthami ethanol extract and water extract have antiinflammatory action.
Radix Notoginseng among the present invention belongs to the Araliaceae herbaceos perennial.The chemical constituent of Radix Notoginseng is similar with Radix Ginseng, mainly contains ginseng saponin, arasaponin and Radix Notoginseng flavone, and other still have 20 kinds of trace element such as Quercetin, β-steroid, polypeptide element and polysaccharide and ferrum, rubidium, strontium.Radix Notoginseng has the effect of dissipating blood stasis hemostasis, subduing swelling and relieving pain.
The eugenol that contains in the skin care item of the present invention, syringone, oleanolic acid, carthamone, neocarthamin, saffloside, Carthamus yellow, Palmic acid, myristic acid, lauric acid, stearic acid, arachidic acid, oleic acid, flavone, ginseng Saponin class, arasaponin, Radix Notoginseng flavone, vitamin etc.; Have effects such as heat-clearing and toxic substances removing, the subcutaneous blood capillary circulation of promotion; Skin there is the nourishing protective effect, make the ruddy beauty of skin, and fragrant odour is sweet and refreshing; Can strengthen simultaneously the immunity of skin; The elasticity of protection epidermis cell and skin, control chapped skin, delaying decrepitude of skin.Skin care item of the present invention have the popular characteristics of naturalization, curative effectization and price.
Product of the present invention is carried out human body skin smear proof test, the time is 30 days (winter), and number on probation is 260 people.On probation through 260 volunteers one month by a definite date; Show that the present invention not only has nutrition to skin and moistens effect; And skin had good moisture preserving, clean skin, anti-ly chaps, repairs effect such as skin, especially the dry and cracked wound to skin has excellent repairing healing effect; And anaphylaxis does not take place, safety non-toxic, the crowd who is suitable for various skin matter uses.
Product beta test result of the present invention is following:
(1) aspect pachylosis degree of improvement effect:
Routine number on probation: 18 ~ 30 years old crowd, women 60 people, male 20 people; 30 ~ 45 years old crowds, women 60 people, male 20 people; Crowd more than 45 years old, women 20 people, male 20 people.Totally 200 people.
Above-mentioned person on probation, every day, each used once sooner or later, used continuously 30 days.
All triers' skin coarseness all has clear improvement, and skin becomes Paint Gloss simultaneously; Wherein 192 trier's skin softness increase, and all the other 8 application on human skin flexibilities do not have significant change.
(2) preserve moisture, aspect the whitening effect:
Routine number on probation: 18 ~ 30 years old crowd, women 60 people, male 20 people; 30 ~ 45 years old crowds, women 60 people, male 20 people; Crowd more than 45 years old, women 20 people, male 20 people.Totally 200 people.
Above-mentioned person on probation, every day, each used once sooner or later, used continuously 30 days.
185 routine triers' skin wet property has clear improvement, and the skin-whitening effect is obvious, and skin becomes Paint Gloss, delicate simultaneously; All the other 15 application on human skin wettabilities, the no significant change of whitening.
(3) aspect the anti-effect of chapping:
Routine number on probation: 18 ~ 30 years old crowd, women 60 people, male 20 people; 30 ~ 45 years old crowds, women 60 people, male 20 people; Crowd more than 45 years old, women 20 people, male 20 people.Totally 200 people.
Above-mentioned person on probation, every day, each used once sooner or later, used continuously 30 days.
It is obvious that all triers' pachylosis improves degree, and skin becomes Paint Gloss, delicate simultaneously, and chapped skin does not appear in all triers.
(4) aspect reparation chapped skin effect:
Routine number on probation: 18 ~ 30 years old crowd, women 10 people, male 10 people; 30 ~ 45 years old crowds, women 10 people, male 10 people; Crowd more than 45 years old, women 10 people, male 10 people.Totally 60 people.
Above-mentioned person on probation's skin has dry and cracked wound, and every day, each used once sooner or later, used continuously 30 days.
All triers' chapped skin wound is basic the healing fully in one week of the product that uses this invention back, and skin becomes Paint Gloss, delicate simultaneously, and all triers' dry and cracked wound is healing fully in two weeks, and new chapped skin does not appear in all triers.
The specific embodiment
Below in conjunction with specific embodiment the present invention is described in further detail.
Embodiment 1: prepare hand cream of the present invention.
At first, carry out extraction and Flos Caryophylli, the Flos Carthami of Flos Caryophylli, Flos Carthami volatile oil, the extraction of pseudo-ginseng activity composition.The organic solvent extraction method is adopted in the extraction of Flos Caryophylli, Flos Carthami volatile oil, be about to Flos Caryophylli, Flos Carthami dry respectively, pulverize after, petroleum ether reflux, extract, three times, merge extractive liquid; Concentrating under reduced pressure, extractum with dissolve with ethanol after, hold over night; Centrifugal, the supernatant concentrating under reduced pressure gets volatile oil.
The leaching process of Flos Caryophylli, Flos Carthami, pseudo-ginseng activity composition is: add 3 times of water gagings in the Flos Caryophylli behind Radix Notoginseng and extraction volatile oil, the Flos Carthami mixture; Decocted 3 hours; Filter, the ethanol precipitation that in filtrating, adds equivalent is removed impurity, and filtrating is condensed into dense extracting solution or extractum.
Secondly, be ready to component a, components b and amount of component b.
Component and the weight portion of component a are: hexadecanol: 5; Lanoline: 5; White oil: 3; Cera Flava: 5;
Azone: 0.5; Squalane: 3; Flos Caryophylli, Flos Carthami extract: 10; Radix Notoginseng extract: 5.
The component and the weight portion of components b are: potassium sorbate: 2; Glycerol: 20; Propylene glycol: 3; Dibenzylatiooluene: 0.05; Add deionized water and make component a, components b and the total weight portion to 100 of amount of component b three.
The component and the weight portion of amount of component b are: Flos Caryophylli, Flos Carthami volatile oil: 1; Essence: 0.02; Propylparaben: 0.02.
The preparation process is following:
(1) component a, components b respectively be heated under the stirring 75 ℃ become homogeneous phases after, component a is added in the emulsifying pot, insulation is at 80 ℃; Evacuation is opened the homogenizing blender, and the control stir speed (S.S.) is 3000 rev/mins; Components b is joined in the emulsifying pot fast, continue to stir 5 minutes.
(2) stop heating, continue to stir, treat to add amount of component b when temperature is reduced to 50 ℃, open vacuum pump, evacuation continued to be cooled to 40 ℃ after 15 minutes, and with Fructus Citri Limoniae acid for adjusting pH value to 6.0, discharging promptly gets product.
Embodiment 2: prepare moisturizer of the present invention.
At first, carry out extraction and Flos Caryophylli, the Flos Carthami of Flos Caryophylli, Flos Carthami volatile oil, the extraction of pseudo-ginseng activity composition.
Steam distillation is adopted in the extraction of Flos Caryophylli, Flos Carthami volatile oil, soon after Flos Caryophylli, Flos Carthami drying, the pulverizing, adds the water of 5 times of amounts, and preimpregnation is after 2 hours, and the reuse steam distillation carries out volatile oil and extracts.
The leaching process of Flos Caryophylli, Flos Carthami, pseudo-ginseng activity composition is: add 5 times of water gagings in the Flos Caryophylli behind Radix Notoginseng and extraction volatile oil, the Flos Carthami mixture; Decocted 2 hours; Filter, the ethanol precipitation that in filtrating, adds equivalent is removed impurity, and filtrating is condensed into dense extracting solution or extractum.
Secondly, be ready to component a, components b and amount of component b.
Component and the weight portion of component a are: hexadecanol: 4; Lanoline: 10; White oil: 3; Cera Flava: 7; Azone: 1; Squalane: 3; Vaseline: 2.
The component and the weight portion of components b are: Flos Caryophylli, Flos Carthami extract: 12; Radix Notoginseng extract: 5; Potassium sorbate: 2; Glycerol: 10; Propylene glycol: 3; Dibenzylatiooluene: 0.05; Add deionized water and make component a, components b and the total weight portion to 100 of amount of component b three.
The component and the weight portion of amount of component b are: Flos Caryophylli, Flos Carthami volatile oil: 1; Essence: 0.02; Antiseptic: 0.02.
The preparation process is following:
(1) component a, components b respectively be heated under the stirring 85 ℃ become homogeneous phases after, component a is added in the emulsifying pot, insulation is at 80 ℃; Evacuation is opened the homogenizing blender, and the control stir speed (S.S.) is 3000 rev/mins; Components b is joined in the emulsifying pot fast, continue to stir 5 minutes.
(2) stop heating, continue to stir, treat to add amount of component b when temperature is reduced to 50 ℃, open vacuum pump, evacuation continued to be cooled to 40 ℃ after 20 minutes, and with Fructus Citri Limoniae acid for adjusting pH value to 7.0, discharging promptly gets product.
Embodiment 3: prepare cleaning and protecting skin article of the present invention.
At first, carry out extraction and Flos Caryophylli, the Flos Carthami of Flos Caryophylli, Flos Carthami volatile oil, the extraction of pseudo-ginseng activity composition.
Steam distillation is adopted in the extraction of Flos Caryophylli, Flos Carthami volatile oil, soon after Flos Caryophylli, Flos Carthami drying, the pulverizing, adds the water of 10 times of amounts, and preimpregnation is after 1 hour, and the reuse steam distillation carries out volatile oil and extracts.
The leaching process of Flos Caryophylli, Flos Carthami, pseudo-ginseng activity composition is: add 4 times of water gagings in the Flos Caryophylli behind Radix Notoginseng and extraction volatile oil, the Flos Carthami mixture; Decocted 2.5 hours; Filter, the ethanol precipitation that in filtrating, adds equivalent is removed impurity, and filtrating is condensed into dense extracting solution or extractum.
Secondly, be ready to component a, components b and amount of component b.
Component and the weight portion of component a are: hexadecanol: 4; Lanoline: 5; White oil: 2; Cera Flava: 5; Azone: 0.5; Squalane: 3; Vaseline: 2; Dimethyl-silicon: 1; Flos Caryophylli, Flos Carthami extract: 10; Radix Notoginseng extract: 5.
The component and the weight portion of components b are: potassium sorbate: 2; Glycerol: 10; Propylene glycol: 2; Dibenzylatiooluene: 0.05; Add deionized water and make component a, components b and the total weight portion to 100 of amount of component b three.
The component and the weight portion of amount of component b are: Flos Caryophylli, Flos Carthami volatile oil: 1; Essence: 0.02; Antiseptic: 0.02.
The preparation process is following:
(1) component a, components b respectively be heated under the stirring 80 ℃ become homogeneous phases after, component a is added in the emulsifying pot, insulation is at 80 ℃; Evacuation is opened the homogenizing blender, and the control stir speed (S.S.) is 3000 rev/mins; Components b is joined in the emulsifying pot fast, continue to stir 5 minutes.
(2) stop heating, continue to stir, treat to add amount of component b when temperature is reduced to 50 ℃, open vacuum pump, evacuation continued to be cooled to 40 ℃ after 18 minutes, and with Fructus Citri Limoniae acid for adjusting pH value to 6.5, discharging promptly gets product.
Embodiment 4: prepare the anti-protective skin cream of chapping of the present invention.
At first, carry out extraction and Flos Caryophylli, the Flos Carthami of Flos Caryophylli, Flos Carthami volatile oil, the extraction of pseudo-ginseng activity composition.
Steam distillation is adopted in the extraction of Flos Caryophylli, Flos Carthami volatile oil, soon after Flos Caryophylli, Flos Carthami drying, the pulverizing, adds the water of 8 times of amounts, and preimpregnation is after 1.5 hours, and the reuse steam distillation carries out volatile oil and extracts.
The leaching process of Flos Caryophylli, Flos Carthami, pseudo-ginseng activity composition is: add 5 times of water gagings in the Flos Caryophylli behind Radix Notoginseng and extraction volatile oil, the Flos Carthami mixture; Decocted 2 hours; Filter, the ethanol precipitation that in filtrating, adds equivalent is removed impurity, and filtrating is condensed into dense extracting solution or extractum.
Secondly, be ready to component a, components b and amount of component b.
Component and the weight portion of component a are: hexadecanol: 6; Lanoline: 10; White oil: 3; Cera Flava: 7; Azone: 0.5; Squalane: 3; Flos Caryophylli, Flos Carthami, Radix Notoginseng extract: 20.
The component and the weight portion of components b are: potassium sorbate: 2; Glycerol: 20; Propylene glycol: 7; Dibenzylatiooluene: 0.15; Add deionized water and make component a, components b and the total weight portion to 100 of amount of component b three.
The component and the weight portion of amount of component b are: Flos Caryophylli, Flos Carthami volatile oil: 3; Essence: 0.02; Propylparaben: 0.02.
The preparation process is following:
(1) component a, components b respectively be heated under the stirring 85 ℃ become homogeneous phases after, component a is added in the emulsifying pot, insulation is at 80 ℃; Evacuation is opened the homogenizing blender, and the control stir speed (S.S.) is 3000 rev/mins; Components b is joined in the emulsifying pot fast, continue to stir 5 minutes.
(2) stop heating, continue to stir, treat to add amount of component b when temperature is reduced to 50 ℃, open vacuum pump, evacuation continued to be cooled to 40 ℃ after 20 minutes, and with Fructus Citri Limoniae acid for adjusting pH value to 6, discharging promptly gets product.
Embodiment 5: prepare the anti-skin care item of chapping of the present invention.
At first, carry out extraction and Flos Caryophylli, the Flos Carthami of Flos Caryophylli, Flos Carthami volatile oil, the extraction of pseudo-ginseng activity composition.
The organic solvent extraction method is adopted in the extraction of Flos Caryophylli, Flos Carthami volatile oil, after being about to Flos Caryophylli and Flos Carthami combination drying, pulverizing, and petroleum ether reflux, extract, three times; Extracting solution concentrating under reduced pressure, extractum with dissolve with ethanol after, hold over night; Centrifugal, the supernatant concentrating under reduced pressure gets volatile oil.
The leaching process of Flos Caryophylli, Flos Carthami, pseudo-ginseng activity composition is: add 3 times of water gagings in the Flos Caryophylli behind Radix Notoginseng and extraction volatile oil, the Flos Carthami mixture; Decocted 3 hours; Filter, the ethanol precipitation that in filtrating, adds equivalent is removed impurity, and filtrating is condensed into dense extracting solution or extractum.
Secondly, be ready to component a, components b and amount of component b.
Component and the weight portion of component a are: hexadecanol: 4; Lanoline: 5; White oil: 2; Cera Flava: 5;
Azone: 0.5; Squalane: 3; Flos Caryophylli, Flos Carthami extract: 10; Radix Notoginseng extract: 5.
The component and the weight portion of components b are: potassium sorbate: 2; Glycerol: 10; Propylene glycol: 2; Dibenzylatiooluene: 0.05; Add deionized water and make component a, components b and the total weight portion to 100 of amount of component b three.
The component and the weight portion of amount of component b are: Flos Caryophylli, Flos Carthami volatile oil: 1; Essence: 0.02; Antiseptic: 0.02.
The preparation process is following:
(1) component a, components b respectively be heated under the stirring 75 ℃ become homogeneous phases after, component a is added in the emulsifying pot, insulation is at 80 ℃; Evacuation is opened the homogenizing blender, and the control stir speed (S.S.) is 3000 rev/mins; Components b is joined in the emulsifying pot fast, continue to stir 5 minutes.
(2) stop heating, continue to stir, treat to add amount of component b when temperature is reduced to 50 ℃, open vacuum pump, evacuation continued to be cooled to 40 ℃ after 15 minutes, and with Fructus Citri Limoniae acid for adjusting pH value to 7, discharging promptly gets product.
Claims (2)
1. skin care item that contain plant extract is characterized in that containing: component a, components b and amount of component b; Wherein, the composition of component a is: the hexadecanol of 6 weight portions, the lanoline of 10 weight portions; The white oil of 3 weight portions, the Cera Flava of 7 weight portions, the azone of 0.5 weight portion; The squalane of 3 weight portions, Flos Caryophylli extract, Flos Carthami extract and Radix Notoginseng extract amount to 20 weight portions; The composition of components b is: the potassium sorbate of 2 weight portions, and the glycerol of 20 weight portions, the propylene glycol of 7 weight portions, the dibenzylatiooluene of 0.15 weight portion makes the deionized water of the total weight portion to 100 of component a, components b and amount of component b three; The composition of amount of component b is: Flos Caryophylli volatile oil and Flos Carthami volatile oil amounts to 3 weight portions, the essence of 0.02 weight portion, the antiseptic propylparaben of 0.02 weight portion;
Its preparation method is:
(1) extraction step of Flos Caryophylli volatile oil and Flos Carthami volatile oil: adopt steam distillation, soon after Flos Caryophylli and Flos Carthami drying, the pulverizing, add the water of 8 times of amounts, preimpregnation 1.5 hours is carried out volatile oil and is extracted;
(2) extraction step of Flos Caryophylli extract, Flos Carthami extract and Radix Notoginseng extract: add 5 times of water gagings to Radix Notoginseng with in Flos Caryophylli after extracting volatile oil and the Flos Carthami mixture; Decocted 2 hours; Filter, the ethanol precipitation that in filtrating, adds equivalent is removed impurity, and filtrating is condensed into dense extracting solution or extractum;
(3) prepare component a, the step of components b and amount of component b:
The composition of component a is: the hexadecanol of 6 weight portions, and the lanoline of 10 weight portions, the white oil of 3 weight portions, the Cera Flava of 7 weight portions, the azone of 0.5 weight portion, the squalane of 3 weight portions, Flos Caryophylli extract, Flos Carthami extract and Radix Notoginseng extract amount to 20 weight portions;
The composition of components b is: the potassium sorbate of 2 weight portions, and the glycerol of 20 weight portions, the propylene glycol of 7 weight portions, the dibenzylatiooluene of 0.15 weight portion makes the deionized water of the total weight portion to 100 of component a, components b and amount of component b three;
The composition of amount of component b is: Flos Caryophylli volatile oil and Flos Carthami volatile oil amounts to 3 weight portions, the essence of 0.02 weight portion, the antiseptic propylparaben of 0.02 weight portion;
(4) with component a, components b respectively be heated under the stirring 85 ℃ become homogeneous phases after, component a is added in the emulsifying pot, insulation is at 80 ℃; Evacuation is opened the homogenizing blender, and the control stir speed (S.S.) is 3000 rev/mins; Components b is joined in the emulsifying pot fast, continue to stir 5 minutes;
(5) stop heating, continue to stir, treat to add amount of component b when temperature is reduced to 50 ℃, open vacuum pump, evacuation continued to be cooled to 40 ℃ after 20 minutes, and with Fructus Citri Limoniae acid for adjusting pH value to 6.0, discharging promptly gets product.
2. method for preparing the skin care item that contain plant extract according to claim 1 is characterized in that comprising the step of following order:
(1) extraction step of Flos Caryophylli volatile oil and Flos Carthami volatile oil: adopt steam distillation, soon after Flos Caryophylli and Flos Carthami drying, the pulverizing, add the water of 8 times of amounts, preimpregnation 1.5 hours is carried out volatile oil and is extracted;
(2) extraction step of Flos Caryophylli extract, Flos Carthami extract and Radix Notoginseng extract: add 5 times of water gagings to Radix Notoginseng with in Flos Caryophylli after extracting volatile oil and the Flos Carthami mixture; Decocted 2 hours; Filter, the ethanol precipitation that in filtrating, adds equivalent is removed impurity, and filtrating is condensed into dense extracting solution or extractum;
(3) prepare component a, the step of components b and amount of component b:
The composition of component a is: the hexadecanol of 6 weight portions, and the lanoline of 10 weight portions, the white oil of 3 weight portions, the Cera Flava of 7 weight portions, the azone of 0.5 weight portion, the squalane of 3 weight portions, Flos Caryophylli extract, Flos Carthami extract and Radix Notoginseng extract amount to 20 weight portions;
The composition of components b is: the potassium sorbate of 2 weight portions, and the glycerol of 20 weight portions, the propylene glycol of 7 weight portions, the dibenzylatiooluene of 0.15 weight portion makes the deionized water of the total weight portion to 100 of component a, components b and amount of component b three;
The composition of amount of component b is: Flos Caryophylli volatile oil and Flos Carthami volatile oil amounts to 3 weight portions, the essence of 0.02 weight portion, the antiseptic propylparaben of 0.02 weight portion;
(4) with component a, components b respectively be heated under the stirring 85 ℃ become homogeneous phases after, component a is added in the emulsifying pot, insulation is at 80 ℃; Evacuation is opened the homogenizing blender, and the control stir speed (S.S.) is 3000 rev/mins; Components b is joined in the emulsifying pot fast, continue to stir 5 minutes;
(5) stop heating, continue to stir, treat to add amount of component b when temperature is reduced to 50 ℃, open vacuum pump, evacuation continued to be cooled to 40 ℃ after 20 minutes, and with Fructus Citri Limoniae acid for adjusting pH value to 6.0, discharging promptly gets product.
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| CN101869541B true CN101869541B (en) | 2012-03-21 |
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| FR3032881A1 (en) * | 2015-02-24 | 2016-08-26 | Galephar M/F | COSMETIC OR DERMATOLOGICAL COMPOSITION FOR THE TREATMENT OF ALOPECIA |
| CN109512732A (en) * | 2017-11-24 | 2019-03-26 | 北京东方淼森生物科技有限公司 | Have effects that repair exterior-applied plant extract, cosmetics of skin barrier and preparation method thereof |
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| JP2008280271A (en) * | 2007-05-09 | 2008-11-20 | Oriza Yuka Kk | Agent for preventing photoaging of skin |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3032881A1 (en) * | 2015-02-24 | 2016-08-26 | Galephar M/F | COSMETIC OR DERMATOLOGICAL COMPOSITION FOR THE TREATMENT OF ALOPECIA |
| WO2016135098A1 (en) * | 2015-02-24 | 2016-09-01 | Galephar M/F | Cosmetic or dermatological composition for treating alopecia |
| CN109512732A (en) * | 2017-11-24 | 2019-03-26 | 北京东方淼森生物科技有限公司 | Have effects that repair exterior-applied plant extract, cosmetics of skin barrier and preparation method thereof |
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| CN101869541A (en) | 2010-10-27 |
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