CN101864630A - Production method of nanometer waterproof mercerized yarns - Google Patents
Production method of nanometer waterproof mercerized yarns Download PDFInfo
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Abstract
The invention relates to a production method of nanometer waterproof mercerized yarns, which can obtain mercerized cotton yarns with permanent waterproof effect and soft hand feeling. In addition, the invention has the advantages of processing time saving, energy source saving and processing process simplification. The invention has the technical scheme that the method comprises the processes of singeing, yarn reeling, mercerizing, kier bleaching, dyeing, soap washing, hot water washing, cold water washing, color fixation, softening, water squeezing, baking and rewinding. The invention is characterized in that the nanometer organic fluorine waterproof finishing agent process is carried out after the color fixation process, and the softening process and the subsequent processes thereof are carried out after the nanometer organic fluorine waterproof finishing agent process. The nanometer organic fluorine waterproof finishing agent process comprises the following concrete steps: placing the yarns into liquid in a yarn bundling dyeing machine to be processed; and then, using hot water for washing, wherein nanometer organic fluorine waterproof finishing agents are added into the liquid in the yarn bundling dyeing machine.
Description
Technical field
The present invention relates to the manufacture craft field of mercerized cotton yarn, be specially a kind of production method of nanometer waterproof mercerized yarns.
Background technology
Along with growth in the living standard, more and more higher for the requirement of garment material, especially more and more higher for the functional requirement of lining.Waterproof, grease proofing functional fabric more and more are subjected to liking of consumer.Generally on the lining of polyurethane, polyester, cotton/polyester, hairs, silk kind fabric, carry out water-proof finish, conventional water-proof aagent generally is the ammonium compounds or the linear polysiloxanes of aluminum sulfate, aliphatic acid chromium complex, long-chain fat hydrocarbon, employing is padded the mode that afterwards bakes earlier and form coating on lining, this method complexity, long flow path, power consumption have the characteristics of partly durable or fugitiveness greatly and only, and arrangement back lining or yarn feel are harder.
Summary of the invention
At the problems referred to above, the invention provides a kind of production method of nanometer waterproof mercerized yarns, it can obtain permanent waterproof, the soft mercerized cotton yarn of feel, and it has saving process time, energy savings and simplified processing process advantage.
Its technical scheme is such:
A kind of production method of nanometer waterproof mercerized yarns, it comprises singes, reeling, mercerising, boil and float, dyeing, soap, hot water wash, cold wash, fixation, soft, water squeezing, oven dry, rewinding technology, it is characterized in that: behind described color fixing process, carry out nanometer organic fluorine waterproof finishing agent technology, after described nanometer organic fluorine waterproof finishing agent technology, carry out described soft technology and subsequent technique thereof again, described nanometer organic fluorine waterproof finishing agent technology is specially and places the liquid of hank-dyeing machine to handle on yarn, reusable heat water washs afterwards, and the liquid in the described hank-dyeing machine adds nanometer organic fluorine waterproof finishing agent.
It is further characterized in that: the pH value of the liquid of described hank-dyeing machine: 4~5, the consumption 3%~6%(owf) of nanometer organic fluorine waterproof finishing agent, treatment temperature are wherein arranged: and 80 ℃~85 ℃, 10 minutes~30 minutes processing time;
The concrete processing technology of described mercerising is: yarn is in the mercerized yarn machine, according to the alkali concn in the treatment fluid be: 25 Baume degrees~30 Baume degrees, treatment fluid temperature: 18 ℃~22 ℃, apply tension force: length stretches 1%~6%, processing time: 6 minutes~7 minutes, washing temperature: 70 ℃;
The concrete steps of its whole processing technology are as follows:
1, singes
When on the yarn singeing machine, singing, 950 ℃~1050 ℃ of the temperature of singing, cotton yarn is 850 rev/mins~1100 rev/mins in the speed of service of jet-burner.To burn the lip-deep filoplume of cotton.Require the burner temperature even, the clean level basically identical of singing;
2, reeling
Cheese reeling after will singing on the reeling frame is yarn-like, and strand focuses on 250g/ strand~1000g/ strand;
3, mercerising
In mercerizing range, even by control mercerising alkali temperature, time, tension force, alkali concn, assurance yarn mercerising.Alkali concn in the treatment fluid is: 25 Baume degrees~30 Baume degrees, and the treatment fluid temperature: 18 ℃~22 ℃, the processing time: 6 minutes~7 minutes, tension force: stretch 1%~6%, washing temperature: 70 ℃;
4, boil and float
On hank-dyeing machine, boil and float liquid parameter: caustic soda 2.0g/L~5.0g/L, hydrogen peroxide 4.0g/L~7.0g/L, scouring agent 0.5g/L~2.0g/L, 95 ℃~100 ℃ of treatment temperatures, 30 minutes~45 minutes processing time;
5, dyeing
On hank-dyeing machine, dye, guarantee even dyeing by control dye dosage, saline and alkaline consumption, fixation time, concentration is 0.1%~13%(owf), salt consumption: 10g/L~80g/L, sodium carbonate amount 10g/L~20g/L, the time is 45 minutes~75 minutes;
6, soap
Yarn is at high temperature soaped in hank-dyeing machine, removes the loose colour on surface, soaping agent 2g/L~4g/L, 85 ℃~95 ℃ of temperature, 10 minutes~20 minutes time;
7, hot water wash
In hank-dyeing machine, add quantitative water, be warming up to 60 ℃~80 ℃, washed 10 minutes~20 minutes;
8, cold wash
In hank-dyeing machine, add quantitative room temperature cold water, move 5 minutes~10 minutes;
9, fixation
Use the color-fixing agent fixation, color-fixing agent concentration 2g/L~4g/L, 50~55 ℃ of temperature, 10 minutes~20 minutes time;
10, nanometer organic fluorine waterproof finishing agent is handled
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 4~5, and the consumption 3%~6%(owf) of nanometer organic fluorine waterproof finishing agent, treatment temperature is at 80 ℃~85 ℃, 10 minutes~30 minutes running time.
11, softness
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 5~7, and softener consumption 1.0%~3.0%(owf), 40 ℃~45 ℃ of treatment temperatures, 15 minutes~30 minutes running time;
12, water squeezing
Water squeezing in wringing machine makes the liquid carrying rate 80%~100% of yarn;
13, oven dry
In temperature is oven dry 4 hours~5 hours in 80 ℃ the dryer, and moisture is controlled at 8%~10%;
14, rewinding
Yarn with the reeled yarn shape on the rewinding car is twisted into a yarn shape.
After adopting method of the present invention, after yarn process mercerising, dyeing, the fixation, adopt organic fluorine waterproof finishing agent treatment process to handle again, carry out subsequent technique then, obtain waterproof evenly, the waterproof mercerized cotton yarn of permanent waterproof, this method has saving process time, energy savings and simplified processing process advantage, and that this mercerized cotton waterproof yarn with permanent waterproof function is applicable to is knitting, the processing of tatting, sweater and straight-bar machines kind fabric.
Description of drawings
Fig. 1 is a process flow diagram of the present invention.
The specific embodiment
Specific embodiment one:
A kind of processing method of 60S/2 waterproof mercerized cotton yarn:
1. singe
When on the yarn singeing machine, singing, 950 ℃ of the temperature of singing, the 60S/2 cotton yarn is 875 rev/mins in the speed of service of jet-burner, to burn the lip-deep filoplume of cotton, requires the burner temperature even, the clean level basically identical of singing;
2, reeling
Cheese reeling after will singing on the reeling frame is yarn-like, and strand focuses on the 250g/ strand;
3, mercerising
In mercerizing range, even by control mercerising alkali temperature, time, tension force, alkali concn, assurance yarn mercerising, the alkali concn in the treatment fluid is: 30 Baume degrees, treatment fluid temperature: 18 ℃, processing time: 6 minutes, tension force: stretch 3%, washing temperature: 70 ℃;
4, boil and float
On hank-dyeing machine, boil and float liquid parameter: caustic soda 3.0g/L, hydrogen peroxide 5.5g/L, scouring agent 0.5g/L, 95 ℃ of treatment temperatures, 30 minutes processing times;
5, dyeing
Dye on hank-dyeing machine, guarantee even dyeing by control dye dosage, saline and alkaline consumption, fixation time, concentration is 0.5%(owf), salt consumption: 10g/L, sodium carbonate amount 10g/L, the fixation time is 45 minutes;
6, soap
Yarn is at high temperature soaped in hank-dyeing machine, removes the loose colour on surface, soaping agent 2g/L, 95 ℃ of temperature, 20 minutes time;
7, hot water wash
In hank-dyeing machine, add quantitative water, be warming up to 80 ℃, washed 10 minutes;
8, cold wash
In hank-dyeing machine, add quantitative room temperature cold water, move 5 minutes;
9, fixation
Use the color-fixing agent fixation, color-fixing agent concentration 2g/L, 50 ℃ of temperature, 20 minutes time;
10, nanometer organic fluorine waterproof finishing agent is handled
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 4, the consumption 3%(owf of nanometer organic fluorine waterproof finishing agent), treatment temperature is at 82 ℃, 30 minutes running times.
11, softness
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 5, the softener consumption is 1.0%(owf), 40 ℃ of treatment temperatures, 20 minutes running times;
12, water squeezing
Water squeezing in wringing machine makes the liquid carrying rate 80%~100% of yarn;
13, oven dry
In temperature is oven dry 4 hours in 80 ℃ the dryer, and moisture is controlled at 8%;
14, rewinding
Yarn with the reeled yarn shape on the rewinding car is twisted into a yarn shape.
Specific embodiment two:
A kind of processing method of 70S/2 waterproof mercerized cotton yarn:
1, singes
When on the yarn singeing machine, singing, 1000 ℃ of the temperature of singing, the 70S/2 cotton yarn is 900 rev/mins in the speed of service of jet-burner, to burn the lip-deep filoplume of cotton.Require the burner temperature even, the clean level basically identical of singing;
2, reeling
Cheese reeling after will singing on the reeling frame is yarn-like, and strand focuses on the 500g/ strand;
3, mercerising
In mercerizing range, even by control mercerising alkali temperature, time, tension force, alkali concn, assurance yarn mercerising, the alkali concn in the treatment fluid is: 28 Baume degrees, treatment fluid temperature: 20 ℃, processing time: 6 minutes 30 seconds, tension force: stretch 6%, washing temperature: 70 ℃;
4, boil and float
On hank-dyeing machine, boil and float liquid parameter: caustic soda 3.5g/L, hydrogen peroxide 5.5g/L, scouring agent 1.5g/L, 98 ℃ of treatment temperatures, 45 minutes processing times.
5, dyeing
Dye on hank-dyeing machine, guarantee even dyeing by control dye dosage, saline and alkaline consumption, fixation time, concentration is 3.0%(owf), salt consumption: 40g/L, sodium carbonate amount 15g/L, the time is 60 minutes;
6, soap
Yarn is at high temperature soaped in hank-dyeing machine, removes the loose colour on surface, soaping agent 3.0g/L, 90 ℃ of temperature, 15 minutes time;
7, hot water wash
In hank-dyeing machine, add quantitative water, be warming up to 70 ℃, washed 15 minutes;
8, cold wash
In hank-dyeing machine, add quantitative room temperature cold water, move 7 minutes;
9, fixation
Use the color-fixing agent fixation, color-fixing agent concentration 3g/L, 50 ℃ of temperature, 15 minutes time;
10, nanometer organic fluorine waterproof finishing agent is handled
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 4.5, the consumption of nanometer organic fluorine waterproof finishing agent is 4.5%(owf), treatment temperature is at 80 ℃, 20 minutes running times.
11, softness
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 6, the softener consumption is 2.0%(owf), 45 ℃ of treatment temperatures, 20 minutes running times;
12, water squeezing
Water squeezing in wringing machine makes the liquid carrying rate 100% of yarn;
13, oven dry
In temperature is oven dry 4.5 hours in 80 ℃ the dryer, and moisture is controlled at 9%;
14, rewinding
Yarn with the reeled yarn shape on the rewinding car is twisted into a yarn shape.
Specific embodiment three:
A kind of processing method of 80S/2 waterproof mercerized cotton yarn:
1, singes
When on the yarn singeing machine, singing, 1050 ℃ of the temperature of singing, the 80S/2 cotton yarn is 1000 rev/mins in the speed of service of jet-burner, to burn the lip-deep filoplume of cotton.Require the burner temperature even, the clean level basically identical of singing;
2, reeling
Cheese reeling after will singing on the reeling frame is yarn-like, and strand focuses on the 1000g/ strand;
3, mercerising
In mercerizing range, even by control mercerising alkali temperature, time, tension force, alkali concn, assurance yarn mercerising, the alkali concn in the treatment fluid is: 25 Baume degrees, treatment fluid temperature: 22 ℃, processing time: 7 minutes, tension force: stretch 1%, washing temperature: 70 ℃;
4, boil and float
On hank-dyeing machine, boil and float liquid parameter: caustic soda 3.0g/L, hydrogen peroxide 5.0g/L, scouring agent 1.0g/L, 98 ℃ of treatment temperatures, 45 minutes processing times;
5, dyeing
Dye on hank-dyeing machine, guarantee even dyeing by control dye dosage, saline and alkaline consumption, fixation time, concentration is 10.0%(owf), salt consumption: 60g/L, sodium carbonate amount 20g/L, the time is 75 minutes;
6, soap
Yarn is at high temperature soaped in hank-dyeing machine, removes the loose colour on surface, soaping agent 3g/L, 95 ℃ of temperature, 20 minutes time;
7, hot water wash
In hank-dyeing machine, add quantitative water, be warming up to 95 ℃, washed 20 minutes;
8, cold wash
In hank-dyeing machine, add quantitative room temperature cold water, move 10 minutes;
9, fixation
Use the color-fixing agent fixation, color-fixing agent concentration 4g/L, 55 ℃ of temperature, 20 minutes time;
10, nanometer organic fluorine waterproof finishing agent is handled
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 5, the consumption of nanometer organic fluorine waterproof finishing agent is 6%(owf), treatment temperature is at 85 ℃, 10 minutes running times.
11, softness
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 7, the softener consumption is 3.0%(owf), 45 ℃ of treatment temperatures, 15 minutes running times;
12, water squeezing
Water squeezing in wringing machine makes the liquid carrying rate 100% of yarn;
13, oven dry
In temperature is oven dry 5 hours in 80 ℃ the dryer, and moisture is controlled at 10%;
14, rewinding
Yarn with the reeled yarn shape on the rewinding car is twisted into a yarn shape.
Owf: fabric is heavy relatively, and fabric herein is a yarn, and promptly yarn is heavy relatively.
Claims (4)
1. the production method of a nanometer waterproof mercerized yarns, it comprises singes, reeling, mercerising, boil and float, dyeing, soap, hot water wash, cold wash, fixation, soft, water squeezing, oven dry, rewinding technology, it is characterized in that: behind described color fixing process, carry out nanometer organic fluorine waterproof finishing agent technology, after described nanometer organic fluorine waterproof finishing agent technology, carry out described soft technology and subsequent technique thereof again, described nanometer organic fluorine waterproof finishing agent technology is specially and places the liquid of hank-dyeing machine to handle on yarn, reusable heat water washs afterwards, and the liquid in the described hank-dyeing machine adds nanometer organic fluorine waterproof finishing agent.
2. the production method of a kind of nanometer waterproof mercerized yarns according to claim 1, it is characterized in that: the pH value of the liquid of described hank-dyeing machine: 4~5, the consumption 3%~6%(owf) that nanometer organic fluorine waterproof finishing agent is wherein arranged, treatment temperature: 80 ℃~85 ℃, 10 minutes~30 minutes processing time.
3. the production method of a kind of nanometer waterproof mercerized yarns according to claim 2, it is characterized in that: the concrete processing technology of described mercerising is: yarn is in the mercerized yarn machine, according to the alkali concn in the treatment fluid be: 25 Baume degrees~30 Baume degrees, treatment fluid temperature: 18 ℃~22 ℃, apply tension force: length stretches 1%~6%, processing time: 6 minutes~7 minutes, washing temperature: 70 ℃.
4. the production method of a kind of nanometer waterproof mercerized yarns according to claim 1, it is characterized in that: the concrete steps of its whole processing technology are as follows:
A, singe
When on the yarn singeing machine, singing, 950 ℃~1050 ℃ of the temperature of singing, cotton yarn is 850 rev/mins~1100 rev/mins in the speed of service of jet-burner.To burn the lip-deep filoplume of cotton.Require the burner temperature even, the clean level basically identical of singing;
B, reeling
Cheese reeling after will singing on the reeling frame is yarn-like, and strand focuses on 250g/ strand~1000g/ strand;
C, mercerising
In mercerizing range, even by control mercerising alkali temperature, time, tension force, alkali concn, assurance yarn mercerising.Alkali concn in the treatment fluid is: 25 Baume degrees~30 Baume degrees, and the treatment fluid temperature: 18 ℃~22 ℃, the processing time: 6 minutes~7 minutes, tension force: stretch 1%~6%, washing temperature: 70 ℃;
D, boil and float
On hank-dyeing machine, boil and float liquid parameter: caustic soda 2.0g/L~5.0g/L, hydrogen peroxide 4.0g/L~7.0g/L, scouring agent 0.5g/L~2.0g/L, 95 ℃~100 ℃ of treatment temperatures, processing time 30min~45min;
E, dyeing
On hank-dyeing machine, dye, guarantee even dyeing by control dye dosage, saline and alkaline consumption, fixation time, concentration is 0.1%~13%(owf), salt consumption: 10g/L~80g/L, sodium carbonate amount 10g/L~20g/L, the time is 45min~75min;
F, soap
Yarn is at high temperature soaped in hank-dyeing machine, removes the loose colour on surface, soaping agent 2g/L~4g/L, 85 ℃~95 ℃ of temperature, time 10min~20min;
G, hot water wash
In hank-dyeing machine, add quantitative water, be warming up to 60 ℃~80 ℃, washing 10min~20min;
H, cold wash
In hank-dyeing machine, add quantitative room temperature cold water, operation 5min~10min;
I, fixation
Use the color-fixing agent fixation, color-fixing agent concentration 2g/L~4g/L, 50~55 ℃ of temperature, time 10min~20min;
J, nanometer organic fluorine waterproof finishing agent are handled
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 4~5, the consumption 3%~6%(owf) of nanometer organic fluorine waterproof finishing agent, treatment temperature is at 80 ℃~85 ℃, running time 10min~30min;
K, softness
Yarn is handled according to following technology in hank-dyeing machine: the pH value: 5~7, softener consumption 1.0%~3.0%(owf), 40 ℃~45 ℃ of treatment temperatures, running time 15min~30min;
L, water squeezing
Water squeezing in wringing machine makes the liquid carrying rate 80%~100% of yarn;
M, oven dry
In temperature is oven dry 4 hours~5 hours in 80 ℃ the dryer, and moisture is controlled at 8%~10%;
N, rewinding
Yarn with the reeled yarn shape on the rewinding car is twisted into a yarn shape.
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