CN101780023A - Chinese gooseberry seed oil speckle removing cosmetic and preparation method thereof - Google Patents
Chinese gooseberry seed oil speckle removing cosmetic and preparation method thereof Download PDFInfo
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- CN101780023A CN101780023A CN201010135602A CN201010135602A CN101780023A CN 101780023 A CN101780023 A CN 101780023A CN 201010135602 A CN201010135602 A CN 201010135602A CN 201010135602 A CN201010135602 A CN 201010135602A CN 101780023 A CN101780023 A CN 101780023A
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Abstract
The invention relates to a Chinese gooseberry seed oil speckle removing cosmetic and a preparation method thereof. The Chinese gooseberry seed oil adopts Chinese gooseberry fruit seed as raw material to be smashed and extracted by supercritical carbon dioxide and then to be undertaken the high-pressure homogenizing treatment, so the grain diameter of the Chinese gooseberry seed oil is less than 120nm. The speckle removing function of the Chinese gooseberry seed oil is firstly discovered, and the Chinese gooseberry seed oil has remarkable speckle removing effect on the senior plaque mainly because of rich nutrition. Compared with other cosmetics having the speckle removing function, the Chinese gooseberry seed oil has incomparable advantages with unique compositions and characteristics. As a novel cosmetic raw material having the speckle removing function, the Chinese gooseberry seed oil has high safety, good speckle removing effect and promising market prospect.
Description
Technical field
The present invention relates to a kind of be substrate with the Chinese gooseberry seed oil, have cosmetics of spot-removing function and preparation method thereof.
Technical background
The cosmetics with spot-removing function class of the Xiao Shouing active ingredient that adds chemical substance mostly or extract in the animal body in the market, speckle dispelling speed is fast, and effect is obvious, but exists hydrargyrum and other content of beary metal to exceed standard, human body there is bigger side effect, severe patient infringement health.From Chinese herbal medicine, natural plant material, extract the active component of its elite material, become the development trend of current cosmetic industry, have more safety, effect and stability as cosmetics.
The present invention relates to a kind of Chinese gooseberry seed oil speckle removing cosmetic and preparation method thereof.This cosmetic base material Chinese gooseberry seed oil with spot-removing function is to be raw material with the kiwi fruit seed, drying, pulverizing, supercritical CO
2Operations such as extraction are extracted and are formed, and handle through extra high pressure homogenize again, make the Chinese gooseberry seed oil particle diameter below 120nm.Chinese gooseberry seed oil is rich in multiple unsaturated fatty acid, flavonoid, phenols, vitamin, trace element-selenium, aminoacid and other bioactive substance, and wherein linolenic acid, linoleic acid content account for more than 75%.Form because of its special fatty acid, Chinese gooseberry seed oil has effects such as blood lipid regulation, vessel softening, slow down aging, has obtained development and application widely at nutrient and healthcare products and field of medicaments, but its application in cosmetic field is still announced first.Chinese gooseberry seed oil can be used as the raw material or the key component of cosmetics because of its natural origin and unique spot-removal function.
Chinese gooseberry seed oil is widely used in cosmetic field as a kind of novel cosmetic raw material resources with spot-removing function, and market potential is huge.
Summary of the invention
Purpose of the present invention: disclose a kind of Chinese gooseberry seed oil speckle removing cosmetic and preparation method thereof.
This invention finds that first Chinese gooseberry seed oil has spot-removal function, especially to senile plaque to dispel effect remarkable, mainly be based on the nutrition that it is rich in.Alpha-linolenic acid and linoleic acid can quicken the tyrosinase protein degraded as polyunsaturated fatty acid, and the activity of restraint of tyrosinase reduces melanic generation, reaches the effect of speckle dispelling.The extensive use of vitamin E in cosmetics is as antioxidant and free radical scavenger.Vitamin E and selenium have the collaborative function of removing free radical, and vitamin E and selenic content are all higher in a lot of speckle dispelling class cosmetics, because they can remove free radical effectively, and the activity of noncompetitive restraint of tyrosinase, thereby speckle dispelling effectively.Vitamin E still is important polyphenoils and a membrane stabilizer in the cell membrane, has the expansion blood capillary, improves blood circulation, removes mottle, makes the thin out effect of senile plaque.Selenium has many-sided physiological function as a kind of essential trace element, and wherein the most important thing is to remove body and produce too much reactive oxygen free radical, antioxidation, the powerful generation that suppresses lipid peroxide, the protection biological cell membrane prevents skin aging etc.Selenium is that use always, generally acknowledged defying age, the important factor of dispelling speckles and whitening face.Human body skin needs a certain amount of aminoacid to keep health, and aminoacid can improve the nutriture of skin, enhances metabolism, to the certain effect of desalination melanin.The Chinese gooseberry seed oil of pure natural is rich in above-mentioned multiple nutrients composition, can work in coordination with speckle dispelling each other, need not to add in addition other cosmetic materials.
Compare with other cosmetics with spot-removing function, Chinese gooseberry seed oil has its incomparable superiority with its special composition and characteristic.The first, content of polyunsaturated fatty acid height such as alpha-linolenic acid, linoleic acid also contain multiple nutrients compositions such as natural Vitamin E, trace element Se, and freckle effect is more remarkable; The second, composition is single, only just can reach the function of speckle dispelling with a kind of raw material of Chinese gooseberry seed oil, and speckle dispelling is safer; The 3rd, handle through extra high pressure homogenize, oil droplet size below 120nm, easier infiltration skin.Chinese gooseberry seed oil has vast market prospect as a kind of novel cosmetic raw material with spot-removing function.
The technological process of production of the present invention is as follows:
Kiwi fruit seed → drying → pulverizing → supercritical CO
2Extraction → oil-water separation → filtration → accurate drying → extra high pressure homogenize → allotment → ageing → check → fill → finished product
The specific embodiment
Chinese gooseberry seed oil speckle removing cosmetic
Formula for a product: Chinese gooseberry seed oil content 〉=99%, cosmetic essence＜1%.
Preparation method: the employing kiwi fruit seed is a raw material, through supercritical CO
2Extraction obtains Chinese gooseberry seed oil, through operations such as oil-water separation, filtration, accurate drying, extra high pressure homogenize processing, allotment, ageing, check, fills, promptly gets Chinese gooseberry seed oil speckle removing cosmetic (Chinese gooseberry seed oil content 〉=99%) again.
This product has been to have the caused by cosmetics for special use of spot-removing function in 2006 by the health ministry approval, and authentication code is made up special word [2006] No. 0631 for defending.According to Ministry of Public Health " cosmetics health standard ", this product has been carried out spot-removing function test, skin allergic reaction test, skin Phototoxicity experiment, repeatedly skin irritation test, the result show this product safety, non-stimulated, have a spot-removal function.
1, spot-removing function experiment
(1) experimenter's selection
Volunteer 30 people, women 20 people, male 10 people, 30～60 years old age, 43 ± 2.5 years old mean age, meet cosmetics human body proof test subject enrollment standard in " cosmetics health standard ", and spottiness on the face.
(2) test method: handling characteristics and the unified approach indicated according to this Product labelling allow direct use of experimenter be subjected to trial product, check weekly and once have or not whole body and local untoward reaction with understanding, grouping standard recording result detects experimenter's melanin value on the face simultaneously; Trier's self-appraisal is divided into satisfaction, is satisfied in the main and is unsatisfied with three kinds of results, and the record result is more than 4 weeks; Comprehensive above data is responsible for the doctor by test and is made produce effects, different conclusions such as effective and invalid, and wherein produce effects and effective accumulation calculating are tried the effective percentage of thing.
(3) result on trial
The spot-removing function result of the test sees Table 1.
Table 1 spot-removing function result of the test table
| Number | Sex | Initial melanin value | Melanin value after 10 days | Melanin value after 30 days | Conclusion |
| ??1 | The woman | ??257 | ??224 | ??186 | Be satisfied in the main |
| ??2 | The woman | ??248 | ??221 | ??205 | Dissatisfied |
| ??3 | The woman | ??264 | ??215 | ??184 | Satisfied |
| ??4 | The woman | ??246 | ??227 | ??164 | Be satisfied in the main |
| ??5 | The woman | ??249 | ??231 | ??152 | Be satisfied in the main |
| ??6 | The woman | ??258 | ??220 | ??148 | Satisfied |
| ??7 | The man | ??251 | ??246 | ??149 | Satisfied |
| ??8 | The man | ??254 | ??232 | ??138 | Satisfied |
| ??9 | The woman | ??228 | ??214 | ??122 | Satisfied |
| ??10 | The woman | ??236 | ??209 | ??131 | Be satisfied in the main |
| ??11 | The man | ??241 | ??213 | ??118 | Be satisfied in the main |
| ??12 | The man | ??234 | ??209 | ??187 | Dissatisfied |
| ??13 | The woman | ??218 | ??197 | ??117 | Satisfied |
| ??14 | The woman | ??235 | ??207 | ??121 | Be satisfied in the main |
| Number | Sex | Initial melanin value | Melanin value after 10 days | Melanin value after 30 days | Conclusion |
| ??15 | The man | ??247 | ??211 | ??118 | Satisfied |
| ??16 | The woman | ??258 | ??235 | ??163 | Be satisfied in the main |
| ??17 | The woman | ??218 | ??196 | ??127 | Satisfied |
| ??18 | The man | ??251 | ??224 | ??167 | Be satisfied in the main |
| ??19 | The woman | ??252 | ??234 | ??138 | Be satisfied in the main |
| ??20 | The woman | ??244 | ??215 | ??123 | Satisfied |
| ??21 | The woman | ??247 | ??221 | ??134 | Be satisfied in the main |
| ??22 | The man | ??228 | ??204 | ??126 | Satisfied |
| ??23 | The man | ??237 | ??198 | ??131 | Satisfied |
| ??24 | The woman | ??241 | ??216 | ??136 | Be satisfied in the main |
[0022]
The result shows that 28 people are satisfied with or are satisfied in the main the freckle effect that is tried thing among 30 experimenters, and effective percentage reaches 93%.
2, skin allergic reaction test
Adopt partial closure to be coated with the skin test method(s), Chinese gooseberry seed oil speckle removing cosmetic will be tried thing and will be coated on the Cavia porcellus unhairing district skin for trying thing, excite contact back 24h and 48h to observe dermoreaction.Result of the test sees Table 2.
Table 2 is tried thing to guinea pig skin allergy result of the test (BT method)
3, skin Phototoxicity experiment
Test preceding 18～24h, be equipped with 4 (numbering 1,2,3,4) unhairing districts in Cavia porcellus spinal column both sides, the every about 2cm * 2cm of unhairing area, 1,3 are positioned at the left side, and 2,4 are positioned at the right side.During test, animal is fixed on the special plank, the about 0.2ml of Chinese gooseberry seed oil speckle removing cosmetic is coated in the unhairing district 1,2,3,4 are not coated with.After being coated with speckle dispelling oil 30min 1,3 districts are covered with aluminium-foil paper, adhesive tape is fixed, and 2,4 districts are shone with the UV light source, and irradiation finishes the back and observes dermoreaction.Result of the test sees Table 3.
Table 3 is tried thing to guinea pig skin Phototoxicity experiment result
4, skin irritation test
24h before the test cuts tame rabbit back spinal column both sides forelock left and right each the about 3cm * 3cm of unhairing scope, application area 2.5cm * 2.5cm.Next day, with Chinese gooseberry seed oil speckle removing cosmetic 0.5ml all be applied in one and survey the skin of unhairing surface, the opposite side skin of unhairing is coated with the equivalent distilled water in contrast.Smear every day once, smeared continuously 14 days.All cropping before smearing every day, injured skin not, water is removed residual Chinese gooseberry seed oil speckle removing cosmetic, observed result behind the 1h.After the off-test, calculate the average integral of every animal every day and carry out the skin irritation intensity evaluation.Result of the test sees Table 4.
Table 4 is tried thing to white rabbit skin irritation result of the test repeatedly
5, the people shows consideration for to have a try and tests
Entrust the PLA Air Force General Hospital that Chinese gooseberry seed oil speckle removing cosmetic is carried out the human body patch test.Tried the thing Chinese gooseberry seed oil speckle removing cosmetic, the experimenter is totally 30 people, male 0 people, and women 30 people at 21～50 years old age, meet the experimenter and volunteer inclusion criteria.Speckle method for testing: select qualified speckle examination device for use, with closed patch test method, to be tried the about 0.03ml of thing (liquid) drips in speckle examination device on the filter paper, the external special adhesive tape sticks in the experimenter back, remove behind the 24h and tried thing, observe dermoreaction respectively at 0.5h, 24h, 48h behind the patch test, write down its result by dermoreaction grade scale in " cosmetics health standard ", testing result sees Table 5.
Table 5 cosmetics human body patch test
The result shows that 30 people have 0 example reaction to occur, and according to regulation in " cosmetics health standard " (2002 editions), Chinese gooseberry seed oil speckle removing cosmetic does not cause untoward reaction to human body skin.
Claims (2)
1. Chinese gooseberry seed oil speckle removing cosmetic and preparation method thereof.Indication Chinese gooseberry seed oil speckle removing cosmetic of the present invention is meant that primary raw material is a Chinese gooseberry seed oil in this cosmetics with spot-removing function, and it is to be raw material with the kiwi fruit seed, drying, pulverizing, supercritical CO
2Operations such as extraction are extracted and are formed, and handle through extra high pressure homogenize again, make the Chinese gooseberry seed oil particle diameter below 120nm.Chinese gooseberry seed oil is rich in multiple unsaturated fatty acid, flavonoid, phenols, vitamin, trace element-selenium, aminoacid and other bioactive substance, and wherein linolenic acid, linoleic acid content account for more than 75%.Chinese gooseberry seed oil can be used as the raw material or the key component of cosmetics because of its natural origin and unique spot-removing function, has the incomparable superiority of used oils and fats in other cosmetics.
The first, content of polyunsaturated fatty acid height such as alpha-linolenic acid, linoleic acid also contain multiple nutrients compositions such as natural Vitamin E, trace element Se, and freckle effect is more remarkable; The second, composition is single, only just can reach the function of speckle dispelling with a kind of raw material of Chinese gooseberry seed oil, and speckle dispelling is safer; The 3rd, handle through extra high pressure homogenize, oil droplet size below 120nm, easier infiltration skin.Chinese gooseberry seed oil has vast market prospect as a kind of novel cosmetic raw material with spot-removing function.
2. the preparation method of indication Chinese gooseberry seed oil speckle removing cosmetic of the present invention: the employing kiwi fruit seed is a raw material, through supercritical CO
2Extraction obtains Chinese gooseberry seed oil, through operations such as oil-water separation, filtration, accurate drying, extra high pressure homogenize processing, allotment, ageing, check, fills, promptly gets Chinese gooseberry seed oil speckle removing cosmetic (Chinese gooseberry seed oil content 〉=99%) again.
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| CN201010135602A CN101780023A (en) | 2010-03-30 | 2010-03-30 | Chinese gooseberry seed oil speckle removing cosmetic and preparation method thereof |
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| CN201010135602A CN101780023A (en) | 2010-03-30 | 2010-03-30 | Chinese gooseberry seed oil speckle removing cosmetic and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102988215A (en) * | 2013-01-05 | 2013-03-27 | 湖南奇异生物科技有限公司 | Skin care freckle-removing cream and method for preparing same |
| CN104083296A (en) * | 2014-06-27 | 2014-10-08 | 湖南奇异生物科技有限公司 | Eye mask for moisturizing and removing beverage and wrinkles and preparation method of eye mask |
| CN115518006A (en) * | 2022-03-07 | 2022-12-27 | 广州市万千粉丝化妆品有限公司 | Application of water-fat membrane for maintaining stable skin barrier in skin care product and preparation method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1710044A (en) * | 2005-06-06 | 2005-12-21 | 湖南老爹农业科技开发股份有限公司 | Supermicro kiwifruit nut oil preparing method |
| CN101547615A (en) * | 2006-10-13 | 2009-09-30 | 热尔韦·达诺尼公司 | New composition for improving skin quality and a process for preparing the same |
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2010
- 2010-03-30 CN CN201010135602A patent/CN101780023A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1710044A (en) * | 2005-06-06 | 2005-12-21 | 湖南老爹农业科技开发股份有限公司 | Supermicro kiwifruit nut oil preparing method |
| CN101547615A (en) * | 2006-10-13 | 2009-09-30 | 热尔韦·达诺尼公司 | New composition for improving skin quality and a process for preparing the same |
Non-Patent Citations (2)
| Title |
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| 《食品与机械》 20050731 李加兴 等 猕猴桃籽油的营养成分及其保健功能 第61、62和65页 1 第22卷, 第4期 * |
| 《食品与机械》 20050731 李加兴 等 猕猴桃籽油的营养成分及其保健功能 第61、62和65页 2 第22卷, 第4期 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102988215A (en) * | 2013-01-05 | 2013-03-27 | 湖南奇异生物科技有限公司 | Skin care freckle-removing cream and method for preparing same |
| CN104083296A (en) * | 2014-06-27 | 2014-10-08 | 湖南奇异生物科技有限公司 | Eye mask for moisturizing and removing beverage and wrinkles and preparation method of eye mask |
| CN115518006A (en) * | 2022-03-07 | 2022-12-27 | 广州市万千粉丝化妆品有限公司 | Application of water-fat membrane for maintaining stable skin barrier in skin care product and preparation method |
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Application publication date: 20100721 |