CN101638554A - Ultraviolet curing coating - Google Patents
Ultraviolet curing coating Download PDFInfo
- Publication number
- CN101638554A CN101638554A CN200910039379A CN200910039379A CN101638554A CN 101638554 A CN101638554 A CN 101638554A CN 200910039379 A CN200910039379 A CN 200910039379A CN 200910039379 A CN200910039379 A CN 200910039379A CN 101638554 A CN101638554 A CN 101638554A
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- ultraviolet
- curing paint
- acrylate
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Abstract
The invention relates to an ultraviolet curing coating which is characterized in that the ultraviolet curing coating comprises 1-35 wt% of epoxy acrylate, 1-35wt% of urethane acrylate, 20-50wt% of polyfunctional acrylate monomer, 1-15wt% of additive and 1-10wt% of photoinitiator. The coating formed by ultraviolet curing coating obtained by adopting the technical scheme has the advantages of good pollution resistibility, easy cleaning, high strength, strong adherence, high toughness and difficult stripping.
Description
Technical field
The present invention relates to a kind of ultraviolet-curing paint, specifically is a kind of ultraviolet-curing paint that is used on woodenware, plastics, metal such as floor, furniture, artwork, household electrical appliances, daily necessities, the electronic product.
Background technology
Ultraviolet-curing paint is since coming out, and just with its hardness height, solvent resistance is strong, and efficient, energy-conservation, the characteristic of environmental protection is attracting people's attention, and its Application Areas is also broad day by day.But existing ultraviolet-curing paint shows the non-constant of resistance to crocking when being applied in aspects such as floor, furniture, and anti-scratch ability is also very weak, does not also occur resistance to crocking ultraviolet-curing paint good, easy to clean, that have stronger anti-scratch ability on the market.
Summary of the invention
For overcoming the deficiencies in the prior art, the object of the present invention is to provide the ultraviolet-curing paint that a kind of resistance to crocking is good, easy to clean, anti-scratch, intensity is high, adhesive power is strong, snappiness is high, do not peel off.
For realizing above purpose, technical scheme of the present invention is:
A kind of ultraviolet-curing paint is characterized in that the composition of described ultraviolet-curing paint and content are:
Epoxy acrylate: 1～35wt%
Urethane acrylate: 1～35wt%
Multi-functional acrylate's monomer: 20～50wt%
Auxiliary agent: 1～15wt%
Light trigger: 1～10wt%
Also can do further perfect by the following technical programs:
Described epoxy acrylate is a bisphenol-a epoxy acrylate.
Described urethane acrylate is aliphatics or aromatic urethane acrylate.
Described multi-functional acrylate's monomer is tri (propylene glycol) diacrylate (TPGDA), Viscoat 295 (TMPTA), ethoxyquin Viscoat 295 (EO-TMPTA), pentaerythritol triacrylate (PET3A), dipentaerythritol acrylate (DPHA), 1, in 6-hexanediyl ester (HDDA), ethoxyquin-1,6 hexanediol diacrylate (EO-HDDA), neopentylglycol diacrylate (NPGDA), the third oxidation neopentylglycol diacrylate (PO-NPGDA) one or more.
Described auxiliary agent is one or more in the mute light powder handled of organo-siloxane, tetrafluoroethylene wax powder, wax, nano assistant, the fluorine-containing or pure fluorine auxiliary agent.
Described light trigger is: 2-methyl-2-hydroxyl-1-phenyl-acetone, 1-hydroxyl cyclic group phenyl ketone, 2,4, one or more mixture of 6-Three methyl Benzene formyl diphenyl phosphate oxidation, benzoin dimethylether, benzophenone (BP), active ammonia.
Preparation method's step of ultraviolet-curing paint of the present invention is:
(1) epoxy acrylate, 1～35wt% urethane acrylate, 20～50wt% multi-functional acrylate monomer and 1～10wt% light trigger that will account for total system 1～35wt% mixes, and is warming up to 40～50 ℃, is stirred to dissolving.
(2) add 1～15wt% auxiliary agent then in step (1), stir, cooling is filtered, and obtains ultraviolet-curing paint of the present invention.
Ultraviolet-curing paint of the present invention is greyish white or lark liquid, and solid content is greater than 95%, and lucifuge stores under the room temperature, and the time of guaranteeing the quality can reach about 1 year.
The formed coating of ultraviolet-curing paint that adopts technical solution of the present invention to obtain has following beneficial effect, and resistance to crocking is good, easy to clean, intensity is high, adhesive power is strong, toughness is high, be not easy to peel off.
Embodiment
Below in conjunction with embodiment the present invention is further described in detail, but is not limited to this.In following examples, unless otherwise indicated raw materials used, be commercially available industrial goods.
Embodiment 1
1, formula table 1
2, blending process:
(1) epoxy acrylate, urethane acrylate, multi-functional acrylate's monomer and light trigger are mixed, be warming up to 40～50 ℃, be stirred to dissolving.
(2) add auxiliary agent then in step (1), stir, cooling is filtered, and obtains ultraviolet-curing paint.
Embodiment 2
1, formula table 2
2, blending process: press the preparation of embodiment 1 blending process and get final product.
Embodiment 3
1, formula table 3
2, blending process: press the preparation of embodiment 1 blending process and get final product.
Real examination example 4
1, formula table 4
2, blending process: press the preparation of embodiment 1 blending process and get final product.
Check embodiment performance
1, testing method
(1) solidifies energy: adopt the test of UV energy meter;
(2) resistance to soiling: adopt the black permanent pen, smear, after five minutes, with dried cloth or with the paper handkerchief wiping that meets GB20810-2006 in film coated surface;
(3) anti-scratch ability: adopt Renminbi monobasic coin, contact with film coated surface, go the film coated surface of swiping with pressure then, estimate and evaluate outward appearance according to being coated with the membrane plane situation in 5 newton with the angle that favours film coated surface＜90 °.
2, detected result
Adopt line rod blade coating mode to be coated on first-class UV priming paint and the good substrate surface (coating thickness of priming paint is about 200 microns) of polishing, coating thickness is about 20 microns, and effect is as shown in table 5 below behind ultraviolet light polymerization:
Table 5
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Solidify energy (mj/c m 2) | ??360 | ??280 | ??260 | ??260 |
| Resistance to soiling | By | By | By | By |
| Anti-scratch ability | By | By | By | By |
By table 5 detected result as can be seen, the formed cured film of ultraviolet-curing paint of the present invention all has good resistance to soiling, anti-scratch ability simultaneously, be particularly suitable for often being subjected to oily material is smeared and the external force wearing and tearing as in the fields such as floor, furniture.
Claims (6)
1, a kind of ultraviolet-curing paint is characterized in that the composition of described ultraviolet-curing paint and content are:
Epoxy acrylate: 1～35wt%
Urethane acrylate: 1～35wt%
Multi-functional acrylate's monomer: 20～50wt%
Auxiliary agent: 1～15wt%
Light trigger: 1～10wt%
2, ultraviolet-curing paint according to claim 1 is characterized in that described epoxy acrylate is a bisphenol-a epoxy acrylate.
3, ultraviolet-curing paint according to claim 1 is characterized in that described urethane acrylate is aliphatics or aromatic urethane acrylate.
4, ultraviolet-curing paint according to claim 1, it is characterized in that described multi-functional acrylate's monomer is tri (propylene glycol) diacrylate, Viscoat 295, ethoxyquin Viscoat 295, pentaerythritol triacrylate, dipentaerythritol acrylate, 1, in 6-hexanediyl ester, ethoxyquin-1,6 hexanediol diacrylate, neopentylglycol diacrylate, the third oxidation neopentylglycol diacrylate one or more.
5, ultraviolet-curing paint according to claim 1 is characterized in that described auxiliary agent is one or more in the mute light powder handled of organo-siloxane, poly-tetrafluoro wax powder, wax, nano assistant, the fluorine-containing or pure fluorine auxiliary agent.
6, ultraviolet-curing paint according to claim 1, it is characterized in that described light trigger is 2-methyl-2-hydroxyl-1-phenyl-acetone, 1-hydroxyl cyclic group phenyl ketone, 2,4, one or more mixture in 6-Three methyl Benzene formyl diphenyl phosphate oxidation, benzoin dimethylether, benzophenone, the active ammonia.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910039379A CN101638554A (en) | 2009-05-06 | 2009-05-06 | Ultraviolet curing coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910039379A CN101638554A (en) | 2009-05-06 | 2009-05-06 | Ultraviolet curing coating |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101638554A true CN101638554A (en) | 2010-02-03 |
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ID=41613742
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910039379A Pending CN101638554A (en) | 2009-05-06 | 2009-05-06 | Ultraviolet curing coating |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101638554A (en) |
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| CN101892004A (en) * | 2010-07-22 | 2010-11-24 | 东北大学 | Ultraviolet-cured heat-resistant coating and preparation and application methods thereof |
| CN102051115A (en) * | 2010-12-14 | 2011-05-11 | 惠州市凯辉化工有限公司 | Ultraviolet light curing colored paint and preparation method thereof |
| CN102107548A (en) * | 2010-07-30 | 2011-06-29 | 张锦碧 | 9000UV vacuum coating paint |
| CN102146254A (en) * | 2011-05-10 | 2011-08-10 | 上海富臣化工有限公司 | UV (ultraviolet) roller-coating metal high-adhesion yellowing-resistant primer |
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| CN102199375A (en) * | 2010-03-26 | 2011-09-28 | 东莞市佩琦涂料有限公司 | Ultraviolet (UV) paint solidified by ultraviolet light |
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| CN103254728A (en) * | 2013-05-30 | 2013-08-21 | 广东邦固化学科技有限公司 | Dual-curing transparent and scrape-resistant protection layer on PVC (polyvinyl chloride) membrane |
| CN103602223A (en) * | 2013-10-24 | 2014-02-26 | 惠州市长润发涂料有限公司 | Antistick sand UV sanded roller painting primer |
| CN103627300A (en) * | 2013-11-12 | 2014-03-12 | 惠州市长润发涂料有限公司 | Ultraviolet (UV) laser roller coating woodware matt finish |
| CN104130675A (en) * | 2014-07-31 | 2014-11-05 | 东莞宏石功能材料科技有限公司 | Scraping-resistant UV matt varnish applied to matt membranes and preparation method thereof |
| CN104312419A (en) * | 2014-10-16 | 2015-01-28 | 山西大学 | Ultraviolet-curing glass coating with antibacterial function and preparation method thereof |
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2009
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| CN101892004A (en) * | 2010-07-22 | 2010-11-24 | 东北大学 | Ultraviolet-cured heat-resistant coating and preparation and application methods thereof |
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| CN106752754A (en) * | 2017-03-14 | 2017-05-31 | 浙江世窗光学薄膜制造有限公司 | A kind of gum polyurethane protective film and preparation method thereof |
| CN107118672A (en) * | 2017-06-29 | 2017-09-01 | 台昌树脂(佛山)有限公司 | Uv gloss oil and preparation method thereof |
| CN108977049A (en) * | 2018-06-27 | 2018-12-11 | 江苏宏泰高分子材料有限公司 | A kind of environment-friendly type photocuring thermostable high humidity PVD finishing coat and preparation method thereof |
| CN108977049B (en) * | 2018-06-27 | 2020-08-25 | 江苏宏泰高分子材料有限公司 | Environment-friendly photocuring ultrahigh-temperature-resistant high-humidity PVD (physical vapor deposition) finish paint and preparation method thereof |
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