CN101632709A - Antibacterial compound oil, essential oil of traditional Chinese medicine and aromatherapy products having antibacterial function - Google Patents

Antibacterial compound oil, essential oil of traditional Chinese medicine and aromatherapy products having antibacterial function Download PDF

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Publication number
CN101632709A
CN101632709A CN200910165042A CN200910165042A CN101632709A CN 101632709 A CN101632709 A CN 101632709A CN 200910165042 A CN200910165042 A CN 200910165042A CN 200910165042 A CN200910165042 A CN 200910165042A CN 101632709 A CN101632709 A CN 101632709A
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oil
chinese medicine
aromatherapy
percentage
weight
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CN101632709B (en
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黄永健
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ZHONGSHAN CITY ZHONGNAN CANDLE CO Ltd
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ZHONGSHAN CITY ZHONGNAN CANDLE CO Ltd
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  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The invention respectively discloses antibacterial compound oil, essential oil of a traditional Chinese medicine and aromatherapy products having antibacterial function. The antibacterial compound oil consists of 8%-15% of atractylis ovata extract, 2%-6% of patchouli extract, 3%-10% of argy wormwood leaf extract, 1%-3% of camphor leaf extract and 50%-80% of blumea balsamifera extract; and the essential oil of the traditional Chinese medicine comprises the following raw materials in percentage by weight: 70%-90% of the antibacterial compound oil and 10%-30% of peppermint oil. The prepared essential oil of the traditional Chinese medicine is fragrant and has the functions of bacteriostasis, disinfection and air purification. The essential oil of the traditional Chinese medicine is added to carriers of the aromatherapy products, thus the aromatherapy products having the antibacterial function can be prepared.

Description

A kind of compound antibacterial oil and Chinese medicine quintessence oil and fragrant product with bacteriostasis efficacy
Technical field
The Chinese medicine quintessence oil and the fragrant product that the present invention relates to a kind of compound antibacterial oil and have bacteriostasis efficacy.
Background technology
Quintessence oil is to refine the volatile flavor extract a kind of flower from plant, leaf, stem, root or the fruit, and common have Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil, a tea tree ethereal oil etc.Quintessence oil not only has the abnormal smells from the patient of fragrance, plays nervous, the bracing effect of releiving, and can also cooperate the treatment of medicine, mitigation symptoms, urges the into recovery of disease.Present quintessence oil is used for skin nursing mostly, does not occur having the quintessence oil of bacteriostasis efficacy on the market as yet.
The champignon product as aromatherapy volatile liquid, balsam, aromatherapy tallow candle etc., is to be added on prepared forming in certain carrier by the quintessence oil that will have aromatic odor.In the existing champignon product, employed quintessence oil is to adopt the essence of chemosynthesis to prepare mostly, yet the derived essential oil of this chemosynthesis can work the mischief to air and human body when volatilization.
Summary of the invention
The object of the present invention is to provide a kind of compound antibacterial oil.
Another object of the present invention is to provide a kind of Chinese medicine quintessence oil with bacteriostasis efficacy.
A further object of the present invention is to provide the fragrant product that adopts described Chinese medicine quintessence oil preparation, and prepared fragrant product has bacteriostasis efficacy, and can not work the mischief to environment and human body.
The objective of the invention is to be achieved through the following technical solutions:
A kind of compound antibacterial oil, form by the following extract that is obtained through the supercritical carbon dioxide low-temperature extraction:
Rhizoma Atractylodis extract 8%-15%;
Radix agastaches extract 2%-6%;
Folium Artemisiae Argyi extract 3%-10%;
Folium cinnamomi camphorae extract 1%-3%;
Herba Blumeae Balsamiferae extract 50%-80%.
A kind of Chinese medicine quintessence oil with bacteriostasis efficacy contains compound antibacterial oil of the present invention, comprises following composition by weight percentage:
Compound antibacterial oil 70%-90%;
Oleum menthae 10%-30%.
Chinese medicine quintessence oil of the present invention is added in the carrier of fragrant product, can prepare fragrant product, comprise aromatherapy volatile liquid, balsam, aromatherapy tallow candle etc. with bacteriostasis efficacy.
A kind of aromatherapy volatile liquid with bacteriostasis efficacy is prepared from by base fluid and Chinese medicine quintessence oil of the present invention, and the percentage by weight of each component is as follows:
Base fluid 70%-90%;
Chinese medicine quintessence oil 10%-30%.
Wherein, described base fluid comprises following composition by weight percentage:
Decanoyl/octanoyl glycerides 1%-5%;
Semen Myristicae isopropyl ester 13%-25%;
Low viscosity white mineral oil 70%-85%.
A kind of balsam with bacteriostasis efficacy is prepared from by mastic and Chinese medicine quintessence oil of the present invention, and the percentage by weight of each component is as follows:
Mastic 90%-96%;
Chinese medicine quintessence oil 4%-10%.
Wherein, described mastic comprises following composition by weight percentage:
Carrageenan 1%-4%;
Kazon 1%-5%;
Surfactant 2%-8%;
Water 85%-95%.
Described surfactant comprises following composition by weight percentage:
Propylene glycol 1%-15%;
Nonyl phenol polyethers-14 20%-60%;
Castor oil hydrogenated 25%-65%.
A kind of aromatherapy tallow candle with bacteriostasis efficacy is prepared from by bean wax and Chinese medicine quintessence oil of the present invention, and the percentage by weight of each component is as follows:
Bean wax 85%-95%;
Chinese medicine quintessence oil 5%-15%.
Wherein, described bean wax comprises following composition by weight percentage:
Hydrogenating glycerol fat 70%-90%;
Hydrogenated vegetable oils and fats 10%-30%.
Compound antibacterial oil of the present invention contains compositions such as Rhizoma Atractylodis, Herba Pogostemonis, Folium Artemisiae Argyi, Folium cinnamomi camphorae and Herba Blumeae Balsamiferae.Rhizoma Atractylodis all have significant deactivation to multiple virus (as influenza virus, mumps virus, silkworm virus etc.), antibacterial (as group B streptococcus, staphylococcus aureus, streptococcus pneumoniae etc.), fungus (as Aspergillus flavus etc.) and mycoplasma etc.Herba Pogostemonis also has the effect of resisting pathogenic microbes, and its flavones ingredient has inhibitory action to rhinovirus, and its volatile oil component also has certain inhibitory action to staphylococcus aureus.Folium Artemisiae Argyi has the blood of regulating the flow of vital energy, pursues effects such as cold-damp, hemostasis.Folium cinnamomi camphorae has effects such as expelling wind and removing dampness, pain relieving, parasite killing.Effects such as Herba Blumeae Balsamiferae has then that warming middle-JIAO is invigorated blood circulation, expelling wind and removing dampness and parasite killing.Therefore, the compound antibacterial oil of the present invention effect that has antibacterial sterilization, purify air.
Chinese medicine quintessence oil of the present invention not only contains described compound antibacterial oil, also contains compositions such as Herba Menthae.Herba Menthae then have clear away heart-fire soothe the spirit, effects such as suffering can be dispersed, hepatic cholagogic, antiinflammatory, antiviral.Therefore, the effect that Chinese medicine quintessence oil of the present invention not only has calmness, sleeping, calms the nerves, but also have the pure and fresh abnormal smells from the patient of fragrance.
Aromatherapy volatile liquid of the present invention is by being prepared from the base fluid that above-mentioned Chinese medicine quintessence oil is added to aromatherapy volatile liquid.This aromatherapy volatile liquid is when ingress of air, and Chinese medicine quintessence oil wherein is released in the air, thus the abnormal smells from the patient that gives out a sweet perfume, and bring into play antibacterial sterilization, effect such as purify air.
Balsam of the present invention is by being prepared from the mastic that above-mentioned Chinese medicine quintessence oil is added to balsam.This balsam is when ingress of air, and Chinese medicine quintessence oil wherein is released in the air, thus the abnormal smells from the patient that gives out a sweet perfume, and bring into play antibacterial sterilization, effect such as purify air.
Aromatherapy tallow candle of the present invention is to be prepared from by above-mentioned Chinese medicine quintessence oil is added in the bean wax.This aromatherapy tallow candle is heated when melting in burning, and Chinese medicine quintessence oil wherein is released in the air, thus the abnormal smells from the patient that gives out a sweet perfume, and bring into play antibacterial sterilization, effect such as purify air.In addition, aromatherapy tallow candle of the present invention uses modification bean wax as carrier, and that this modification bean wax has is natural, environmental protection, nontoxic, the advantage such as good that is shaped, and can not discharge toxic gas during burning, also can not influence the original fragrance of Chinese medicine quintessence oil.
The specific embodiment
Embodiment one: the preparation of compound antibacterial oil
Get Rhizoma Atractylodis, Herba Pogostemonis, Folium Artemisiae Argyi, Folium cinnamomi camphorae and Herba Blumeae Balsamiferae respectively, extract with supercritical carbon dioxide low-temperature extraction method, concrete steps are as follows: after respectively each raw material being cleaned up also fragmentation, put into extractor, improve the pressure of extractor and remain on uniform temperature, thereby make CO 2Liquefaction; At supercritical liq CO 2In the continuous extraction process, the oils composition in the raw material is dissolved in liquid CO 2In, become mixed solution and flow away, and be insoluble to CO 2Solid slag then be trapped in the extractor; Resulting mixed solution flows in the detached dowel, makes CO through cooling, blood pressure lowering 2Generating gasification, oils composition ooze out, thereby realize Oil-gas Separation, wherein gas CO 2Recycling use, the oils composition is trapped in the detached dowel to be removed; Receive the oils composition in the detached dowel,, after making with extra care, obtain the effective extract of each raw material with filtering behind the anhydrous sodium sulfate drying.
With the effective extract of above-mentioned each raw material, carry out the prescription compatibility according to following percentage by weight, promptly obtain compound antibacterial oil of the present invention:
Rhizoma Atractylodis extract 12%,
Radix agastaches extract 4%,
Folium Artemisiae Argyi extract 6%,
Folium cinnamomi camphorae extract 2%,
Herba Blumeae Balsamiferae extract 76%.
Embodiment two: the preparation of Chinese medicine quintessence oil
According to following percentage by weight,, promptly make the Chinese medicine quintessence oil with bacteriostasis efficacy of the present invention with embodiment one prepared compound antibacterial oil and Oleum menthae mix homogeneously:
Compound antibacterial oil 80%,
Oleum menthae 20%.
Prepared Chinese medicine quintessence oil carries out acute toxicity test by Traditional Chinese Medicine University Of Guangzhou's clinical pharmacology institute, and the result is as follows:
1. the oral acute toxicity test of mice: the LD of mice oral Chinese medicine quintessence oil 50Be 383.55g/kg, 95% the credible 294.68g/kg~499.31g/kg that is limited to.And the toxicity criterion of air freshener is: the malicious LD of the oral urgency of mice 50〉=5g/kg is judged to be nontoxic.The LD of this Chinese medicine quintessence oil 50Be higher than 76 times of nontoxic standard, so be judged to be nontoxic.
2. chmice acute toxicity on inhalation test: chmice acute sucks the LC of Chinese medicine quintessence oil 50Be 24863.99g/m 3, 95% the credible 16837.34g/m that is limited to 3~33387.46g/m 3And the toxicity criterion of air freshener is: chmice acute sucks (2h) LC 50>10000mg/m 3, the nontoxic level in true border.The LC of this Chinese medicine quintessence oil 50Be higher than 2486 times of nontoxic standard, so be judged to be nontoxic.
Prepared Chinese medicine quintessence oil is through check, and its fragrance, color and luster, refraction index, relative density, arsenic content, content of beary metal, pH value all meet request of national standard.
Embodiment three: the preparation of aromatherapy volatile liquid
Take by weighing each component according to following percentage by weight, behind each component mix homogeneously, make the base fluid of aromatherapy volatile liquid:
Decanoyl/octanoyl glycerides 2%,
Semen Myristicae isopropyl ester 20%,
Low viscosity white mineral oil 78%.
According to following percentage by weight, embodiment two prepared Chinese medicine quintessence oils are added in the prepared base fluid, behind the mix homogeneously, promptly make the aromatherapy volatile liquid with antibacterial disinfection efficacy of the present invention:
Base fluid 80%,
Chinese medicine quintessence oil 20%.
After testing, in the prepared aromatherapy volatile liquid of the present invention, its lead content is less than 5.0mg/kg, and arsenic content is less than 2.5mg/kg, and mercury content all meets the standard-required of GB7916-1987 less than 0.1mg/kg.
Embodiment four: the preparation of balsam
Take by weighing each component according to following percentage by weight:
Water 85%,
Carrageenan 1.5%,
Kazon 2.5%,
Surfactant 5%,
Chinese medicine quintessence oil 6%.
Described Chinese medicine quintessence oil is prepared from according to embodiment two described methods.
Described surfactant comprises following composition by weight percentage:
Propylene glycol 3%,
Nonyl phenol polyethers-14 47%,
Castor oil hydrogenated 50%,
Carrageenan is added to the water, heats while stirring, dissolve fully, and continue to be heated to 80 ℃, obtain water solution A until carrageenan.Surfactant is joined in the prepared Chinese medicine quintessence oil of embodiment two, after stirring, join in the prepared water solution A, 80 ℃ of following insulated and stirred.After treating that quintessence oil dissolves fully, add Kazon, continue to stir and dissolve fully, obtain mixed solution B until Kazon.After mixed solution B is cooled to 60 ℃, be poured in the preprepared container, treat that it cools off fully after, promptly make the balsam with antibacterial disinfection efficacy of the present invention.
After testing, in the prepared balsam of the present invention, its lead content is less than 5.0mg/kg, and arsenic content is less than 2.5mg/kg, and mercury content all meets the standard-required of GB7916-1987 less than 0.1mg/kg.
Embodiment five: the preparation of aromatherapy tallow candle
Take by weighing each component according to following percentage by weight:
Hydrogenating glycerol fat 72%,
Hydrogenated vegetable oils and fats 18%,
Chinese medicine quintessence oil 10%.
Described Chinese medicine quintessence oil is prepared from according to embodiment two described methods.
Place rustless steel container to heat in hydrogenating glycerol fat and hydrogenated vegetable oils and fats, melt fully, stir, obtain bean wax wax liquid A until it.Wax liquid A is continued to be heated to 80 ℃, under fully stirring, add the prepared Chinese medicine quintessence oil of embodiment two, obtain bean wax wax liquid B.B pours into the stainless steel mould of putting into the wax core in advance with wax liquid, and wherein, the temperature of stainless steel mould is between 65 ℃~69 ℃, and pouring into temperature is 75 ℃.After cooling, under 80 ℃, mend the end face of wax candle flat with wax liquid B.Depanning after cooling more promptly makes the aromatherapy tallow candle with antibacterial disinfection efficacy of the present invention.
After testing, in the prepared aromatherapy tallow candle of the present invention, its color and luster, abnormal smells from the patient, heat stability, light stability, combustibility and content of beary metal etc., all standard-required of accord with Q B/T2902-2007.

Claims (9)

1, a kind of compound antibacterial oil, form by the following extract that is obtained through the supercritical carbon dioxide low-temperature extraction:
Rhizoma Atractylodis extract 8%-15%;
Radix agastaches extract 2%-6%;
Folium Artemisiae Argyi extract 3%-10%;
Folium cinnamomi camphorae extract 1%-3%;
Herba Blumeae Balsamiferae extract 50%-80%.
2, a kind of Chinese medicine quintessence oil with bacteriostasis efficacy contains the described compound antibacterial oil of claim 1, comprises following composition by weight percentage:
Compound antibacterial oil 70%-90%;
Oleum menthae 10%-30%.
3, a kind of aromatherapy volatile liquid with bacteriostasis efficacy is characterized in that: described aromatherapy volatile liquid contains the described Chinese medicine quintessence oil of claim 2, and its percentage by weight is 10%-30%.
4, aromatherapy volatile liquid according to claim 3 is characterized in that: described aromatherapy volatile liquid also contains the base fluid that percentage by weight is 70%-90%; Described base fluid comprises following composition by weight percentage:
Decanoyl/octanoyl glycerides 1%-5%,
Semen Myristicae isopropyl ester 13%-25%,
Low viscosity white mineral oil 70%-85%.
5, a kind of balsam with bacteriostasis efficacy is characterized in that: described balsam contains the described Chinese medicine quintessence oil of claim 2, and its percentage by weight is 4%-10%.
6, balsam according to claim 5 is characterized in that: described balsam also contains the mastic that percentage by weight is 90%-96%; Described mastic comprises following composition by weight percentage:
Carrageenan 1%-4%,
Kazon 1%-5%,
Surfactant 2%-8%,
Water 85%-95%.
7, balsam according to claim 6 is characterized in that: described surfactant comprises following composition by weight percentage:
Propylene glycol 1%-15%;
Nonyl phenol polyethers-14 20%-60%;
Castor oil hydrogenated 25%-65%.
8, a kind of aromatherapy tallow candle with bacteriostasis efficacy is characterized in that: described aromatherapy tallow candle contains the described Chinese medicine quintessence oil of claim 2, and its percentage by weight is 5%-15%.
9, aromatherapy tallow candle according to claim 8 is characterized in that: described aromatherapy tallow candle also contains the bean wax that percentage by weight is 85%-95%; Described bean wax comprises following composition by weight percentage:
Hydrogenating glycerol fat 70%-90%,
Hydrogenated vegetable oils and fats 10%-30%.
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CN101632761A (en) 2010-01-27
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CN101633868B (en) 2012-08-22
CN101612364A (en) 2009-12-30

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