CN101554158B - Emamectin-benzoate and methomyl microemulsion and preparation method thereof - Google Patents
Emamectin-benzoate and methomyl microemulsion and preparation method thereof Download PDFInfo
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- CN101554158B CN101554158B CN200810103827XA CN200810103827A CN101554158B CN 101554158 B CN101554158 B CN 101554158B CN 200810103827X A CN200810103827X A CN 200810103827XA CN 200810103827 A CN200810103827 A CN 200810103827A CN 101554158 B CN101554158 B CN 101554158B
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- Prior art keywords
- methomyl
- microemulsion
- percent
- farming breast
- microemulsion according
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- 239000005916 Methomyl Substances 0.000 title claims abstract description 26
- UHXUZOCRWCRNSJ-QPJJXVBHSA-N methomyl Chemical compound CNC(=O)O\N=C(/C)SC UHXUZOCRWCRNSJ-QPJJXVBHSA-N 0.000 title claims abstract description 26
- 239000004530 micro-emulsion Substances 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- CXEGAUYXQAKHKJ-NSBHKLITSA-N emamectin B1a Chemical compound C1=C[C@H](C)[C@@H]([C@@H](C)CC)O[C@]11O[C@H](C\C=C(C)\[C@@H](O[C@@H]2O[C@@H](C)[C@H](O[C@@H]3O[C@@H](C)[C@H](NC)[C@@H](OC)C3)[C@@H](OC)C2)[C@@H](C)\C=C\C=C/2[C@]3([C@H](C(=O)O4)C=C(C)[C@@H](O)[C@H]3OC\2)O)C[C@H]4C1 CXEGAUYXQAKHKJ-NSBHKLITSA-N 0.000 title abstract 3
- 238000000593 microemulsion method Methods 0.000 title description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 9
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 7
- 150000003839 salts Chemical class 0.000 claims description 22
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 12
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 12
- 210000000481 breast Anatomy 0.000 claims description 10
- 238000009313 farming Methods 0.000 claims description 10
- AXTGDCSMTYGJND-UHFFFAOYSA-N 1-dodecylazepan-2-one Chemical compound CCCCCCCCCCCCN1CCCCCC1=O AXTGDCSMTYGJND-UHFFFAOYSA-N 0.000 claims description 6
- FIPWRIJSWJWJAI-UHFFFAOYSA-N Butyl carbitol 6-propylpiperonyl ether Chemical compound C1=C(CCC)C(COCCOCCOCCCC)=CC2=C1OCO2 FIPWRIJSWJWJAI-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 6
- 239000006184 cosolvent Substances 0.000 claims description 6
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 claims description 6
- 229960005235 piperonyl butoxide Drugs 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- 230000000740 bleeding effect Effects 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 3
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 3
- 235000011152 sodium sulphate Nutrition 0.000 claims description 3
- LNJXZKBHJZAIKQ-UHFFFAOYSA-N 1,1,1,2-tetrachloro-3-(2,3,3,3-tetrachloropropoxy)propane Chemical compound ClC(Cl)(Cl)C(Cl)COCC(Cl)C(Cl)(Cl)Cl LNJXZKBHJZAIKQ-UHFFFAOYSA-N 0.000 claims description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 2
- 241001272567 Hominoidea Species 0.000 claims description 2
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims description 2
- -1 Negel Chemical compound 0.000 claims description 2
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 2
- 150000008052 alkyl sulfonates Chemical class 0.000 claims description 2
- 239000004202 carbamide Substances 0.000 claims description 2
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 claims description 2
- 239000002612 dispersion medium Substances 0.000 claims description 2
- MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 claims description 2
- 229940043264 dodecyl sulfate Drugs 0.000 claims description 2
- 235000011187 glycerol Nutrition 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 239000003381 stabilizer Substances 0.000 claims description 2
- 241000238631 Hexapoda Species 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 6
- 239000000575 pesticide Substances 0.000 abstract description 6
- 241000607479 Yersinia pestis Species 0.000 abstract description 3
- 231100000053 low toxicity Toxicity 0.000 abstract description 2
- 230000002265 prevention Effects 0.000 abstract description 2
- 241000219193 Brassicaceae Species 0.000 abstract 1
- 241000500441 Plutellidae Species 0.000 abstract 1
- 230000002528 anti-freeze Effects 0.000 abstract 1
- 230000000295 complement effect Effects 0.000 abstract 1
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- 238000006748 scratching Methods 0.000 abstract 1
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- 239000002904 solvent Substances 0.000 abstract 1
- 239000012747 synergistic agent Substances 0.000 abstract 1
- 230000009885 systemic effect Effects 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 description 5
- 239000008367 deionised water Substances 0.000 description 4
- 229910021641 deionized water Inorganic materials 0.000 description 4
- 239000003814 drug Substances 0.000 description 4
- 238000003912 environmental pollution Methods 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 241000500437 Plutella xylostella Species 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 239000012669 liquid formulation Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000002574 poison Substances 0.000 description 3
- 231100000614 poison Toxicity 0.000 description 3
- 238000001228 spectrum Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 241000255967 Helicoverpa zea Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000003905 agrochemical Substances 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 239000002609 medium Substances 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 230000000361 pesticidal effect Effects 0.000 description 2
- 230000003449 preventive effect Effects 0.000 description 2
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 description 2
- 210000002784 stomach Anatomy 0.000 description 2
- 230000001988 toxicity Effects 0.000 description 2
- 231100000419 toxicity Toxicity 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- 241001124076 Aphididae Species 0.000 description 1
- 241001498622 Cixius wagneri Species 0.000 description 1
- 241000254173 Coleoptera Species 0.000 description 1
- 241001635274 Cydia pomonella Species 0.000 description 1
- 241000258937 Hemiptera Species 0.000 description 1
- 241000255777 Lepidoptera Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000409991 Mythimna separata Species 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 206010033799 Paralysis Diseases 0.000 description 1
- 241001414989 Thysanoptera Species 0.000 description 1
- 239000000642 acaricide Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000000035 biogenic effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- KXDHJXZQYSOELW-UHFFFAOYSA-N carbonic acid monoamide Natural products NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 description 1
- 239000000544 cholinesterase inhibitor Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- GCKZANITAMOIAR-XWVCPFKXSA-N dsstox_cid_14566 Chemical compound [O-]C(=O)C1=CC=CC=C1.C1=C[C@H](C)[C@@H]([C@@H](C)CC)O[C@]11O[C@H](C\C=C(C)\[C@@H](O[C@@H]2O[C@@H](C)[C@H](O[C@@H]3O[C@@H](C)[C@H]([NH2+]C)[C@@H](OC)C3)[C@@H](OC)C2)[C@@H](C)\C=C\C=C/2[C@]3([C@H](C(=O)O4)C=C(C)[C@@H](O)[C@H]3OC\2)O)C[C@H]4C1 GCKZANITAMOIAR-XWVCPFKXSA-N 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- BTCSSZJGUNDROE-UHFFFAOYSA-N gamma-aminobutyric acid Chemical compound NCCCC(O)=O BTCSSZJGUNDROE-UHFFFAOYSA-N 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 210000004894 snout Anatomy 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- KJAMZCVTJDTESW-UHFFFAOYSA-N tiracizine Chemical compound C1CC2=CC=CC=C2N(C(=O)CN(C)C)C2=CC(NC(=O)OCC)=CC=C21 KJAMZCVTJDTESW-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
Claims (7)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200810103827XA CN101554158B (en) | 2008-04-11 | 2008-04-11 | Emamectin-benzoate and methomyl microemulsion and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200810103827XA CN101554158B (en) | 2008-04-11 | 2008-04-11 | Emamectin-benzoate and methomyl microemulsion and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
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CN101554158A CN101554158A (en) | 2009-10-14 |
CN101554158B true CN101554158B (en) | 2012-07-25 |
Family
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Application Number | Title | Priority Date | Filing Date |
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CN200810103827XA Expired - Fee Related CN101554158B (en) | 2008-04-11 | 2008-04-11 | Emamectin-benzoate and methomyl microemulsion and preparation method thereof |
Country Status (1)
Country | Link |
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CN (1) | CN101554158B (en) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102428913B (en) * | 2011-11-11 | 2014-01-22 | 山东一览科技有限公司 | Microemulsion insecticide and production process thereof |
CN102742586B (en) * | 2012-06-20 | 2013-09-04 | 董志平 | New purposes of methomyl for control of athetis lepigone |
CN106034445A (en) * | 2016-05-31 | 2016-10-26 | 山东胜伟园林科技有限公司 | Method for carrying out original soil greening of drought and flood saline and alkaline lands through employing soil conditioner containing phethalanilic acid |
CN109769871A (en) * | 2019-03-20 | 2019-05-21 | 青岛市农业科学研究院 | A kind of biological pesticide pest repellant |
-
2008
- 2008-04-11 CN CN200810103827XA patent/CN101554158B/en not_active Expired - Fee Related
Non-Patent Citations (3)
Title |
---|
张莹等.两种蜜蜂头部乙酰胆碱酯酶对杀虫药剂敏感度比较.《农药学学报》.2005,(第03期), * |
曹辉辉等.0.2%高渗甲维盐乳油防治水稻二化螟田间药效试验.《现代农业科技(上半月刊)》.2006,(第08期), * |
顾春波等.山东省主要烟区烟(桃)蚜[Myzus persicae(Sulzer)]抗药性研究.《中国烟草学报》.2005,(第04期), * |
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Publication number | Publication date |
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CN101554158A (en) | 2009-10-14 |
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Owner name: BEIJING GREEN AGROSINO CORPORATION JIXI AGROSINO B Effective date: 20120611 |
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C41 | Transfer of patent application or patent right or utility model | ||
C56 | Change in the name or address of the patentee |
Owner name: BEIJING DASHIFENG BIOTECHNOLOGY CO., LTD. Free format text: FORMER NAME: BEIJING GREEN AGROSINO BIOENGINEERING TECHNOLOGY CO., LTD. |
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CP03 | Change of name, title or address |
Address after: 101109 Beijing horse town Huoxian village 1000 meters west of Tongzhou District Patentee after: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Address before: 101109 Beijing city Huoxian Town Industrial Zone Tongzhou District Kuo Hing Street No. 88-40 Patentee before: BEIJING GREEN AGROSINO BIOENGINEERING TECHNOLOGY Co.,Ltd. |
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TR01 | Transfer of patent right |
Effective date of registration: 20120611 Address after: 101109 Beijing horse town Huoxian village 1000 meters west of Tongzhou District Co-patentee after: BEIJING GREEN AGROSINO Corp. Patentee after: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Co-patentee after: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Co-patentee after: Beijing Agrosino Import and Export Co.,Ltd. Address before: 101109 Beijing horse town Huoxian village 1000 meters west of Tongzhou District Patentee before: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. |
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CP01 | Change in the name or title of a patent holder |
Address after: 101109 Tongzhou District County, Beijing, Ma Town Village 1000 meters West Co-patentee after: BEIJING GREEN AGROSINO CROP TECHNOLOGY CO.,LTD. Patentee after: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Co-patentee after: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Co-patentee after: Beijing Agrosino Import and Export Co.,Ltd. Address before: 101109 Tongzhou District County, Beijing, Ma Town Village 1000 meters West Co-patentee before: BEIJING GREEN AGROSINO Corp. Patentee before: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Co-patentee before: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Co-patentee before: Beijing Agrosino Import and Export Co.,Ltd. |
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Effective date of registration: 20180713 Address after: 061100 the Western District of Cangzhou Lingang Development Zone, Cangzhou, Hebei, and the east side of the four road. Co-patentee after: BEIJING GREEN AGROSINO CROP TECHNOLOGY CO.,LTD. Patentee after: HEBEI GREEN NONGHUA CROP TECHNOLOGY CO.,LTD. Co-patentee after: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Address before: 101109 Tongzhou District County, Beijing, Ma Town Village 1000 meters West Co-patentee before: BEIJING GREEN AGROSINO CROP TECHNOLOGY CO.,LTD. Patentee before: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Co-patentee before: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Effective date of registration: 20180713 Address after: 101109 Tongzhou District County, Beijing, Ma Town Village 1000 meters West Co-patentee after: BEIJING GREEN AGROSINO CROP TECHNOLOGY CO.,LTD. Patentee after: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Co-patentee after: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Address before: 101109 Tongzhou District County, Beijing, Ma Town Village 1000 meters West Co-patentee before: BEIJING GREEN AGROSINO CROP TECHNOLOGY CO.,LTD. Patentee before: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Co-patentee before: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Co-patentee before: Beijing Agrosino Import and Export Co.,Ltd. |
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