CN109392942A - A kind of Pesticidal combination containing indoxacarb and bistrifluron - Google Patents
A kind of Pesticidal combination containing indoxacarb and bistrifluron Download PDFInfo
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- CN109392942A CN109392942A CN201710700343.2A CN201710700343A CN109392942A CN 109392942 A CN109392942 A CN 109392942A CN 201710700343 A CN201710700343 A CN 201710700343A CN 109392942 A CN109392942 A CN 109392942A
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- Prior art keywords
- bistrifluron
- indoxacarb
- pesticidal combination
- agent
- effective component
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/38—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< where at least one nitrogen atom is part of a heterocyclic ring; Thio analogues thereof
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of Pesticidal combination containing indoxacarb and bistrifluron, effective component are indoxacarb and bistrifluron binary built.Wherein the mass ratio of indoxacarb and bistrifluron is 1~40: 40~1, effective component indoxacarb and bistrifluron total quality in preparation account for the 1%~80% of the entire quality of the pharmaceutical preparations in preparation, remaining is the auxiliary element for allowing to use and receive in pesticide, and the dosage form of the Pesticidal combination is missible oil, suspending agent, wettable powder, water dispersible granules, aqueous emulsion, microemulsion, granule, microcapsule formulations.Most of lepidoptera pests of the various plants such as vegetables, tealeaves, cotton can be effectively prevented.
Description
Technical field
The present invention relates to technical field of pesticide compounding, more particularly to a kind of desinsection containing indoxacarb and bistrifluron
Composition.
Background technique
Indoxacarb is the one of DuPont Corporation (E.I.du Pont de Nemours and Company) development and production
Kind insecticide, homerun make nerve cell loss function, can effectively prevent by blocking the sodium-ion channel in insect nerve cell
Control the various pests on the crops such as grain, cotton, fruit and vegetable.
Bistrifluron is the high activity that Dong Bao chemical company, South Korea filters out from the more a benzoyl urea derivatives of 2OOO
Insect growth regulator, IGR, belongs to bis- (trifluoromethyl) the Phenylbenzoyl urea derivatives of chloro- 3, the 5- of novel 2-, and mechanism of action is unique
And bioactivity is high.Bistrifluron has significant Growth inhibition to insect, has special efficacy to trialeurodes vaporariorum, the chemical combination
Object inhibit insect chitin formed, influence endepidermis generation, keep insect dead from smoothly casting off a skin, can effectively prevent vegetables,
Most of lepidoptera pests of the various plants such as tealeaves, cotton, antagonism pest is generally effective, and to crop natural enemy, Ren Xuhe
Environment high safety.
In the real process of agricultural production, application chemical agent is prevention and treatment plant pest the most effective means, but
The problem of being most easily produced by chemical prevention pest is the generation of pest resistance to insecticide.And apply list to continuous high dose for a long time
One chemical insecticide, a series of problems, such as be easy to causeing residual, the environmental pollution of medicament.Reasonable chemical insecticide compounding or
Mixture, which has, expands insecticidal spectrum, improves control efficiency, extends the optimum period for applying fertilizer, reduce dosage, reduce phytotoxicity, reduce residual, prolong
The positive features such as the generation and development of slow pest resistance and drug resistance, pesticide compositional or mixture are to solve the above problems most
For one of effective method.We filter out indoxacarb and bistrifluron are multiple based on the indoor screening and field trials
Match, there is apparent synergistic effect, and the Pesticidal combination that is compounded with bistrifluron about indoxacarb and applying at present there is no
People reported.
Summary of the invention
Based on the above circumstances, it is an object of that present invention to provide a kind of new and effective agricultural insecticide compositions.Can effectively it prevent
Control most of lepidoptera pests of the various plants such as vegetables, tealeaves, cotton.
The technical solution of the present invention is achieved by the following measures:
A kind of Pesticidal combination containing indoxacarb and bistrifluron, in the Pesticidal combination effective component indoxacarb with
The mass ratio of bistrifluron is 1~50: 50~1, and the Pesticidal combination of the present invention is through toxicity test experimental verification, indenes worm
For the mass ratio of prestige and bistrifluron at 1~40: 40~1, synergistic effect is preferable.
The formulations of pesticide that the Pesticidal combination of the present invention can be prepared are missible oil, suspending agent, wettable powder, moisture
Shot agent, aqueous emulsion, microemulsion, granule, microcapsule formulations.Indoxacarb and bistrifluron total quality in preparation account for entirely
The 1%~80% of the quality of the pharmaceutical preparations, wherein toxicity and residues achieve a better balance when accounting for 5%~50%, cost is relatively low.
The specific embodiment for the formulations of pesticide that Pesticidal combination of the present invention is configured to is as follows:
The Pesticidal combination is cream preparation, the mass fraction of component are as follows: 1~50 part of indoxacarb；Bistrifluron 1
~50 parts；10~30 parts of conventional emulsifier；20~50 parts of Conventional solvents；1~5 part of conventional synergist.The cream preparation it is specific
Production stage is to add emulsifier, synergy after being first completely dissolved in effective component indoxacarb and bistrifluron addition solvent
Agent is filling after mixing evenly at homogeneous and transparent oily liquids, can the missible oil preparation made into the composition of the present invention.
The Pesticidal combination is suspending agent, the mass fraction of component are as follows: 1~50 part of indoxacarb；Bistrifluron 1~
50 parts；5~20 parts of dispersing agent；1~5 part of antifreezing agent；0.1~2 part of thickener；0.1~0.8 part of defoaming agent；Penetrating agent 0~10
Part；0.1~5 part of pH adjusting agent；Water, surplus.The specific production stage of the suspending agent is first to mix other auxiliary agents, through high speed
Shear-mixed is uniform, and effective component indoxacarb and bistrifluron, abrading-ball 2~3 hours in ball crusher, which is added, keeps a diameter equal
In 5mm hereinafter, can be made into the aqueous suspension formulations of the present composition.
The Pesticidal combination is wettable powder, the mass fraction of component are as follows: 1~50 part of indoxacarb；Double trifluoro worms
1~50 part of urea；3~10 parts of dispersing agent；1~5 part of wetting agent；Filler, surplus.The specific production stage of the wettable powder are as follows:
Effective component indoxacarb is mixed with bistrifluron and dispersing agent, wetting agent and filler by above-mentioned formula, in a stirring kettle
Uniform stirring remixes uniformly after being smashed by air jet mill, that is, can be made into the wettable powder of the present composition.
The Pesticidal combination is water dispersible granules, the mass fraction of component are as follows: 1~50 part of indoxacarb；Double trifluoro worms
1~50 part of urea；3~10 parts of dispersing agent；1~10 part of wetting agent；1~5 part of disintegrating agent；Filler surplus.The tool of the water dispersible granules
Body production stage are as follows: by above-mentioned formula by effective component indoxacarb and bistrifluron and dispersing agent, wetting agent, disintegrating agent and
Filler is uniformly mixed, and is crushed with micro jet, through mediating, be then granulated in addition fluidized-bed granulation dryer,
Through sampling analysis after dry, screening, that is, it can be made into the water dispersible granules of the present composition.
The Pesticidal combination is aqueous emulsion, the mass fraction of component are as follows: 1~50 part of indoxacarb；Bistrifluron 1~
50 parts；3~30 parts of emulsifier；5~15 parts of solvent；2~15 parts of stabilizer；1~5 part of antifreezing agent；0.1~8 part of defoaming agent；Thickening
0.2~2 part of agent；Water, surplus.The specific production stage of the aqueous emulsion are as follows: first by indoxacarb and bistrifluron, solvent and cream
Agent, cosolvent are added together, and make to be dissolved into uniform oily phase；By part water, antifreeze, the others pesticide such as antimicrobial
Auxiliary agent mixes into uniform water phase；The oil phase is added to the aqueous phase while being stirred in the reactor at high speed, and slowly plus water is straight
It to phase inversion point is reached, opens cutter and carries out high speed shear, and remaining water is added, shearing about half an hour, form oil-in-water type
Aqueous emulsion, that is, can be made into the aqueous emulsion of the present composition.
The Pesticidal combination is microemulsion, the mass fraction of component are as follows: 1~50 part of indoxacarb；Bistrifluron 1~
50 parts；10~30 parts of emulsifier, 1~8 part of antifreezing agent, 0.5~10 part of stabilizer, 20~50 parts of Conventional solvents cosolvent.By indenes
Worm prestige and bistrifluron are completely dissolved with cosolvent, add the other compositions such as emulsifier, antifreezing agent, stabilizer, uniformly mixed
It closes, is eventually adding water, microemulsion can be made into after being sufficiently stirred.
The Pesticidal combination is granule, the mass fraction of component are as follows: 1~50 part of indoxacarb；Bistrifluron 1~
50 parts；1~10 part of wetting dispersing agent；0.1~5 part of thickener；0.1~5 part of defoaming agent；Castor oil, surplus are supplied.Will effectively at
Divide each components such as indoxacarb and bistrifluron, dispersing agent, stabilizer, defoaming agent and solvent to be mixed according to the formula, is put into
In sand milling kettle after grinding, it is sent into mixing in mixer for well-distribution and gets product.
The Pesticidal combination is microcapsule formulations, the mass fraction of component are as follows: 1~50 part of indoxacarb；Bistrifluron 1
~50 parts；5~20 parts of urea；5~20 parts of formaldehyde；5~20 parts of emulsifying dispersant；1~5 part of antifreezing agent；0.1~2 part of thickener；
0.1~0.8 part of defoaming agent；Water, surplus.Urea and formaldehyde (the mass ratio of the material are added in three-necked flask with a mixing device
About l:1.5~2.0), the pH value for adjusting solution with sodium hydroxide solution then heats to 70~80 DEG C, instead to 8~9 or so
It should obtain stable urea resin prepolymer.The raw medicine of a certain amount of indoxacarb and bistrifluron is taken to be dissolved in hexamethylene, and
Emulsifying dispersant is added in the solution, with being vigorously stirred, is made into steady using aqueous solution containing emulsified dispersant as the O/W type of water phase
Determine lotion.Above-mentioned urea resin prepolymer is added in lotion, pH value is adjusted, polymerization occurs under acid catalyzed conditions,
It is wrapped oil phase substance, forms microcapsule granule.Slowly heating, solidification, temperature control is at 40~50 DEG C, curing time
1h.Suitable auxiliary agent is added in selection, can obtain stable microcapsule suspending agent.
Wherein above-described emulsifier is selected from calcium dodecyl benzene sulfonate and aliphatic acid polyethenoxy ether, alkyl phenol polyoxy
Ethylene ether sulfosuccinates, styrylphenol polyoxyethylene ether, nonylphenol polyoxyethylene ether, castor oil polyoxyethylene ether,
Aliphatic acid polyethenoxy base ester, any one of polyoxyethylene aliphatic alcohol ether or more than one a mixture of arbitrary proportions.
The solvent is xylene or biodiesel, toluene, diesel oil, methanol, ethyl alcohol, n-butanol, isopropanol, rosin-based
Vegetable oil code name be ND-45, solvent naphtha, dimethylformamide, dimethyl sulfoxide, one of water equal solvent or more than one
It anticipates than the mixture of composition.
It is LG-3, GY-D1252, GY-D1256, SNWGF-01, lignin that the dispersing agent, which is selected from polycarboxylate code name,
Sulfonate code name is 201107,201108, alkylphenol polyoxyethylene ether methyl ether condensation sulfate, alkylsulfonate calcium salt, naphthalene
Sulfonic formaldehyde condensation compound sodium salt, alkyl phenol polyoxyethylene ether, polyoxyethylene carboxylate, aliphatic amine polyoxyethylene ether, glycerolipid
One or more of fat acid ester polyoxyethylene ether.
The wetting agent is selected from lauryl sodium sulfate, calcium dodecyl benzene sulfonate, and Nekal BX moistens bleeding agent F,
Alkylbenzene sulfonate polyoxyethylene triphen phosphenylic acid salt dimly, spaonin powder, silkworm excrement, one of spaonin powder or a variety of.
The disintegrating agent is selected from bentonite, urea, ammonium sulfate, aluminium chloride, citric acid, succinic acid, in sodium bicarbonate
It is one or more.
The thickener be selected from xanthan gum, carboxymethyl cellulose, carboxyethyl cellulose, methylcellulose, aluminum magnesium silicate,
It is one or more in polyvinyl alcohol.
The stabilizer is selected from sodium citrate, one of resorcinol.
The antifreezing agent is selected from ethylene glycol, propylene glycol, one of glycerine or a variety of.
The defoaming agent is selected from silicone oil, silicone compound, C10-20Saturated fat acids compound, C8-10Fatty alcohol
It is one or more.
The filler is selected from kaolin, diatomite, bentonite, attapulgite, white carbon black, starch, in precipitated calcium carbonate
It is one or more.
The present invention has apparent synergistic effect by the compounded pesticides of indoxacarb and bistrifluron of effective component, prolongs
The generation of slow key drug resistance, and production and application costs are reduced, it is a variety of that vegetables, tealeaves, cotton etc. can be effectively prevented
Most of lepidoptera pests of plant.
Specific embodiment
To make technical solution of the present invention, purpose and advantage are more clearly understood, present invention following specific embodiments
It is illustrated, but the present invention is not limited to these examples.Effect experiment of the invention uses indoor biometrics and field trial phase
In conjunction with mode, unless otherwise instructed, ratio mentioned below is all mass parts ratio.
Embodiment: indoxacarb and bistrifluron virulence experiment with different proportions.
1.1 reagent agent
96% former medicine of indoxacarb, 96% bistrifluron amine raw medicine, above-mentioned raw medicine are had by extra large Lear medicine company share
Research and development department, limit company provides.
1.2 test targets
Diamondback moth: 5 generations of indoor continuous raising and three ages of its Individual Size and the consistent responsive type diamondback moth of physiological status
Larva.Temperature (25 ± 2) DEG C.Relative humidity 65% ± 5%, periodicity of illumination 12/12h (L/D).
1.3 experimental procedure
1.3.1 medicament is prepared
Acetone solution raw medicine is first used, suitable two raw medicine is made by several different ratios according to the result of preliminary experiment,
It is diluted each of the treatment into several concentration gradients for use with acetone again.
It is measured using the drop method that NY/T1 154.1-2006 recommends.Micro intravenous drip device is cleaned with solvent, is adjusted
Dropper is to stand-by state.The test worm CO of neat and consistent is chosen with writing brush2Mild paralysis is placed in 9cm culture dish, then
Medicament is dripped to the abdomen of polypide, every point drops physic liquor 0.1L, corresponding third contained with drop 0.1L with micro intravenous drip device by head
The processing of ketone is control, and the test worm after drop is moved to (28 ± 2) DEG C, is normally cultivated in the culture dish of relative humidity 75%.Often
Handle 4 repetitions, 20 test worms of every repetition.
1.4 control time
It investigates test worm death condition (judging that test worm death standard is gently to pierce no autonomic response with needle), records for 24 hours after processing
Total borer population and dead borer population.
1.5 data statistics and analysis
According to investigation statistics, the corrected mortality of each processing is calculated.And Sun Yunpei is used referring to NY/T1 154.7-2006
The co-toxicity coefficient (CTC value) of method calculating mixture.If compareing the death rate < 5%, do not correct, compare the death rate between 5%-20%,
It is corrected by formula 2, compares the death rate > 20%, test need to reform.
Using the logarithm of drug concentration (mg/L) as independent variable X, using the probability value of corrected mortality as dependent variable y, respectively
Virulence regression equation is established, the LC of single dose and each proportion mixture is calculated using DPS software50Poison altogether is calculated according to Sun Yunpei method
Coefficient (CTC).Co-toxicity coefficient CTC, calculation formula are as follows: (using indoxacarb as standard agent, toxicity index 100):
Toxicity index (TI)=indoxacarb EC of bistrifluron50The EC of/bistrifluron50×100
True toxicity index (ATI)=indoxacarb EC of M50The EC of/M50×100
Theoretical toxicity index (TTI)=indoxacarb TI × P indoxacarb+bistrifluron TI × P bistrifluron of M
TTI × 100 of co-toxicity coefficient (CTC)=M ATI/M of M
In formula:
M is the mixture of indoxacarb and bistrifluron different ratio
P indoxacarb is indoxacarb ratio shared in mixture
P bistrifluron is bistrifluron ratio shared in mixture.
2.1 toxicity test results
The indoor measurement result of 1 indoxacarb of table and bistrifluron to diamondback moth
It as can be seen from the table, is that it is total when 1:50~50:1 dilutes in effective component indoxacarb and bistrifluron ratio
Malicious coefficient is all larger than 120, shows certain synergistic effect, the synergy that wherein indoxacarb and bistrifluron are 1:10~10:1
It acts on most obvious.Test result show in room conditions indoxacarb compounded with bistrifluron to diamondback moth have it is higher
Activity, it is proposed that further field control effectiveness test is carried out to suitable proportion 1:10~10:1 or so mixture preparation, to evaluate its field
Between practical application effect.
3, field trial prevents and treats the experimental result of diamondback moth, trialeurodes vaporariorum
3.1 field trials prevent and treat diamondback moth
3.1.1 test method
Test is carried out in Kaiping City, Guangdong Province suburb truck garden.It is carried out by each processing design concentration conventional to water spray
Mist.Spraying equipment is WF-16 type knapsack hand sprayer, and spray head is single fan nozzle, operating pressure 0.2-
0.4Mpa, spray amount 0.36-0.48L/min, carry out conventional spraying, and when spray makes every effort to uniformly thoughtful.Field pickles when application
Moth is 1~2 instar larvae peak period.
3.1.2 investigation method
There are Eggs of Diamondback Moth and 2~3 plants of the wild cabbage of larva by every selection of 5 points of diagonal line samplings in every cell before application
(depending on insect density).Diamondback moth larvae head number is in this, as insect population before being administered in probability demarcation strain.After application
The diamondback moth larvae number that survival is remained in fixed point singling is investigated respectively to correct Revision insect recluced rate as prevention and treatment within 1 day, 3 days, 7 days
Effect.
3.1.3 drug effect calculation method
Revision insect recluced rate (%)=(larva number after medicine prelarva number-medicine)/medicine prelarva number × 100
Preventive effect (%)=(treatment region Revision insect recluced rate-control Revision insect recluced rate)/(check plot 100- Revision insect recluced rate) ×
100。
3.1.4 phytotoxicity investigation method
7 days observation wild cabbage growing states after medicine estimate medicament to wild cabbage without phytotoxicity.
3.1.5 field control effectiveness test result
From table 2 it can be seen that the Mixed Pharmacy of different proportion, carries out field experiment by different dosages, it is to small after medicine
The control efficiency of diamond-back moth is better than comparison medicament, quick with 1:3 ratio compounding prevention and treatment diamondback moth with indoxacarb and bistrifluron,
Efficiency time is long, and control efficiency is good, and insecticidal effect is incremented by with the increase of dosage.This mixture, can effectively control small
Harm of the diamond-back moth to host is of great significance to the raising and volume increase of quality of vegetable, there is stronger popularizing value.
3.2 field trials prevent and treat trialeurodes vaporariorum
3.2.1 test method
Test is located at the village Li Lou, Luoyang City, the township Li Lou, Luolong District, and cucumber planting system is greenhouse, is cucumber, product for studying object
Kind is prosperous excellent No. 3.Cucumber variety is consistent, and growing way is uniform, and water and fertilizer management level is more consistent, and trialeurodes vaporariorum is moderate.
3.2.2 investigation method
Worm radix living to be investigated before application, takes 5 sampling point/canopies, each sampling point takes 5 plants, complete stool worm amount is looked into, 1d, 3d after application,
7d investigates worm storage living and calculates preventive effect.
3.2.3 drug effect calculation method
Revision insect recluced rate (%)=(larva number after medicine prelarva number-medicine)/medicine prelarva number × 100
Preventive effect (%)=(treatment region Revision insect recluced rate-control Revision insect recluced rate)/(check plot 100- Revision insect recluced rate) ×
100。
3.2.4 phytotoxicity investigation method
7 days observation cucumber growth situations after medicine estimate medicament to cucumber without phytotoxicity.
3.2.5 field control effectiveness test result
From table 3 it can be seen that the Mixed Pharmacy of different proportion, carries out field experiment, its dialogue after medicine by different dosages
The control efficiency of aleyrodid is quick with 1:3 ratio compounding prevention and treatment trialeurodes vaporariorum better than comparison medicament, indoxacarb and bistrifluron, holds
The effect time is long, and control efficiency is good, and insecticidal effect is incremented by with the increase of dosage.According to experimental observation, each medication processing is to cucumber
Do not generate phytotoxicity.It is of great significance to the raising and volume increase of cucumber quality, there is stronger popularizing value.
To sum up indoor biometrics and twice described in field experiment result, it is of the present invention to be with indoxacarb and bistrifluron
Effective component carries out the Pesticidal combination of two-spot compounding, shows good control efficiency to pests such as diamondback moth, trialeurodes vaporariorums, right
Target crops safety, compared with single dose, Pesticidal combination of the present invention has the mechanism of action unique, and unit dose is few, quick-acting is good,
Many advantages, such as lasting period is long, and effect field is more wide in range, can have preferable prevention and treatment to plant diseases, insect pest, so, in this hair
Bright research and development and promotion conference generate very big economic value, increasing both production and income to the peasant household of vast vegetables, fruit tree producing region and work as
The protection of ground ecological environment has a very important significance.
Claims (4)
1. a kind of Pesticidal combination containing indoxacarb and bistrifluron, it is characterised in that: the Pesticidal combination it is effective at
It is divided into indoxacarb and bistrifluron binary built, remaining is auxiliary element, wherein effective component indoxacarb and bistrifluron
Mass ratio be 1~50: 50~1.
2. Pesticidal combination according to claim 1, it is characterised in that: indoxacarb and bistrifluron in the formulation total
Quality accounts for the 1%~80% of the entire quality of the pharmaceutical preparations.
3. Pesticidal combination according to claim 2, it is characterised in that: indoxacarb and bistrifluron in the formulation total
Weight accounts for the 5%~50% of the entire quality of the pharmaceutical preparations.
4. Pesticidal combination according to claim 1 or 2 or 3, it is characterised in that: the dosage form of the Pesticidal combination is cream
Oil, suspending agent, wettable powder, water dispersible granules, aqueous emulsion, microemulsion, granule, microcapsule formulations.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111116507A (en) * | 2019-12-30 | 2020-05-08 | 江苏腾龙生物药业有限公司 | Synthetic process of indoxacarb |
| CN112956484A (en) * | 2021-02-23 | 2021-06-15 | 青岛奥迪斯生物科技有限公司 | Insecticidal composition containing flufenoxuron and indoxacarb and application thereof |
| CN116649358A (en) * | 2021-11-05 | 2023-08-29 | 青岛海利尔生物科技有限公司 | Insecticidal composition containing bistrifluron and application thereof |
-
2017
- 2017-08-16 CN CN201710700343.2A patent/CN109392942A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111116507A (en) * | 2019-12-30 | 2020-05-08 | 江苏腾龙生物药业有限公司 | Synthetic process of indoxacarb |
| CN112956484A (en) * | 2021-02-23 | 2021-06-15 | 青岛奥迪斯生物科技有限公司 | Insecticidal composition containing flufenoxuron and indoxacarb and application thereof |
| CN112956484B (en) * | 2021-02-23 | 2022-06-24 | 青岛奥迪斯生物科技有限公司 | Insecticidal composition containing flufenoxuron and indoxacarb and application thereof |
| CN116649358A (en) * | 2021-11-05 | 2023-08-29 | 青岛海利尔生物科技有限公司 | Insecticidal composition containing bistrifluron and application thereof |
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