CN101531848A - An environment-friendly digital ink-jet direct printing textile ink and method for preparing same - Google Patents
An environment-friendly digital ink-jet direct printing textile ink and method for preparing same Download PDFInfo
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- CN101531848A CN101531848A CN 200910301072 CN200910301072A CN101531848A CN 101531848 A CN101531848 A CN 101531848A CN 200910301072 CN200910301072 CN 200910301072 CN 200910301072 A CN200910301072 A CN 200910301072A CN 101531848 A CN101531848 A CN 101531848A
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- 239000004753 textile Substances 0.000 title claims abstract description 30
- 238000010017 direct printing Methods 0.000 title claims abstract description 24
- 238000000034 method Methods 0.000 title abstract description 6
- 239000000049 pigment Substances 0.000 claims abstract description 57
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 14
- 239000008367 deionised water Substances 0.000 claims abstract description 13
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000002270 dispersing agent Substances 0.000 claims abstract description 10
- 238000000227 grinding Methods 0.000 claims abstract description 10
- 239000000080 wetting agent Substances 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims abstract description 8
- 238000002360 preparation method Methods 0.000 claims abstract description 8
- 239000004902 Softening Agent Substances 0.000 claims abstract description 7
- 238000009775 high-speed stirring Methods 0.000 claims abstract description 7
- 239000002904 solvent Substances 0.000 claims abstract description 6
- 238000001914 filtration Methods 0.000 claims abstract description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 230000003750 conditioning effect Effects 0.000 claims description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- 239000013543 active substance Substances 0.000 claims description 4
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 4
- AXDJCCTWPBKUKL-UHFFFAOYSA-N 4-[(4-aminophenyl)-(4-imino-3-methylcyclohexa-2,5-dien-1-ylidene)methyl]aniline;hydron;chloride Chemical compound Cl.C1=CC(=N)C(C)=CC1=C(C=1C=CC(N)=CC=1)C1=CC=C(N)C=C1 AXDJCCTWPBKUKL-UHFFFAOYSA-N 0.000 claims description 3
- 239000004925 Acrylic resin Substances 0.000 claims description 3
- 229920000178 Acrylic resin Polymers 0.000 claims description 3
- 244000025254 Cannabis sativa Species 0.000 claims description 3
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims description 3
- NSOXQYCFHDMMGV-UHFFFAOYSA-N Tetrakis(2-hydroxypropyl)ethylenediamine Chemical compound CC(O)CN(CC(C)O)CCN(CC(C)O)CC(C)O NSOXQYCFHDMMGV-UHFFFAOYSA-N 0.000 claims description 3
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical group OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 3
- 239000003139 biocide Substances 0.000 claims description 3
- 238000004132 cross linking Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 claims description 3
- MGIYRDNGCNKGJU-UHFFFAOYSA-N isothiazolinone Chemical compound O=C1C=CSN1 MGIYRDNGCNKGJU-UHFFFAOYSA-N 0.000 claims description 3
- 229920000642 polymer Polymers 0.000 claims description 3
- 229960004418 trolamine Drugs 0.000 claims description 3
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 claims description 2
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims description 2
- UEEJHVSXFDXPFK-UHFFFAOYSA-N N-dimethylaminoethanol Chemical compound CN(C)CCO UEEJHVSXFDXPFK-UHFFFAOYSA-N 0.000 claims description 2
- 229960002887 deanol Drugs 0.000 claims description 2
- 239000012972 dimethylethanolamine Substances 0.000 claims description 2
- 239000000839 emulsion Substances 0.000 claims description 2
- 239000006260 foam Substances 0.000 claims description 2
- 235000011187 glycerol Nutrition 0.000 claims description 2
- 229920000831 ionic polymer Polymers 0.000 claims description 2
- 229920005749 polyurethane resin Polymers 0.000 claims description 2
- 229960001124 trientine Drugs 0.000 claims description 2
- JRSHMRFEWSBYLO-UHFFFAOYSA-N C[C-]1NC=CC1=O Chemical compound C[C-]1NC=CC1=O JRSHMRFEWSBYLO-UHFFFAOYSA-N 0.000 claims 1
- 238000007639 printing Methods 0.000 abstract description 11
- 230000007613 environmental effect Effects 0.000 abstract description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract 3
- 230000000844 anti-bacterial effect Effects 0.000 abstract 1
- 239000003899 bactericide agent Substances 0.000 abstract 1
- 239000003431 cross linking reagent Substances 0.000 abstract 1
- 238000007641 inkjet printing Methods 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- 239000000976 ink Substances 0.000 description 39
- 239000004744 fabric Substances 0.000 description 15
- 238000005516 engineering process Methods 0.000 description 7
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- 239000000975 dye Substances 0.000 description 6
- 238000002203 pretreatment Methods 0.000 description 5
- 230000000176 photostabilization Effects 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 229920000742 Cotton Polymers 0.000 description 3
- 229920004933 Terylene® Polymers 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 239000005020 polyethylene terephthalate Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000000859 sublimation Methods 0.000 description 3
- 230000008022 sublimation Effects 0.000 description 3
- 238000009941 weaving Methods 0.000 description 3
- -1 glycol ethers Chemical class 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- 238000003911 water pollution Methods 0.000 description 2
- 210000002268 wool Anatomy 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 238000012356 Product development Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000004144 decalcomania Methods 0.000 description 1
- 239000013530 defoamer Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000011819 refractory material Substances 0.000 description 1
- 238000007650 screen-printing Methods 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000010023 transfer printing Methods 0.000 description 1
Abstract
An environment-friendly digital ink-jet direct printing textile ink and method for preparing same, the digital ink-jet direct printing textile ink composed of components as follows: pigment paste, connection materials, cross-linking agent, softening agent, solvent, surfactant, bactericide, pH regulating agent, and deionized water. The pigment paste is a mixture of the following components: pigments, ultra-dispersing agent, wetting agent, and deionized water. The preparation method includes: a. mixing the pigments, ultra-dispersing agent, wetting agent, and deionized water into a pigment paste, mixing the pigment paste at high-speed and then grinding it in an ultra-fine nano-grinding machine, to obtain the nano stage ultrafine grain paste; b. mixing the proportioning mixture with the grinded nano stage ultrafine grain paste, high-speed stirring and then filtering to obtain a finished environment-friendly digital ink-jet direct printing textile ink. The inventive printing textile ink does not contain formaldehyde, can be direct digital printed wtihtout plate-making when in use, and has rich color, soft hand feeling, and capability of allowing the digital ink-jet printing textile materials to meet the high environmental and quality requirements.
Description
[technical field]
The present invention relates to the ink that digital ink-jet printed flat-panel printer is used, particularly relate to a kind of formaldehydeless environment-friendly digital ink-jet direct printing textile ink and preparation method thereof.
[background technology]
In traditional textile printing technology, stamp all needs to make a plate in advance on yarn fabric, and some printing technology needs pre-treatment and aftertreatment, and all can produce water pollution problems in the process of plate-making or pre-treatment, aftertreatment.In addition, traditional yarn fabric printing technology need carry out in batches, and feasible production technology and final product quality to stamp all has high requirement.
Digital ink-jet printed technology is a kind of new textile printing technology, and it is that dedicated dye ink or paint ink are passed through the direct spray printing of ink-jet printer on textiles.The digital ink-jet printed ink of dye-type is divided into reactive dyestuffs type, acidic dye type and dispersed dye type ink, all contain formaldehyde in these inks, chemical reaction takes place in dyestuff in its ink and yarn fabric (as wool, cotton, terylene etc.), thereby pattern is attached on the yarn fabric.At present, use the thermal sublimation digit printing of dispersed dye type ink to be used widely, but must printing to pattern on the special-purpose heat sublimation paper, this stamp mode carries out thermal dye sublimation transfer printing again, and be confined to resistant to elevated temperatures terylene cloth, and can not be used for the cloth that cotton textiles wait some non-refractories, and it is digital ink-jet printed no matter to be to use active ink or acid ink to carry out, and all must carry out pre-treatment and aftertreatment to yarn fabric, and light fastness and washing fastness are all poor.
[summary of the invention]
The present invention is intended to address the above problem, and provides a kind of formaldehydeless, makes digital ink-jet printed yarn fabric satisfy the environment-friendly digital ink-jet direct printing textile ink of high environmental protection, high quality requirement.
The present invention also aims to provide a kind of preparation method of this stamp textile ink.
For achieving the above object, the invention provides a kind of environment-friendly digital ink-jet direct printing textile ink, this ink is the mixture of following component by weight percentage:
Dispersible pigment color paste 12～55
Connect material 5～20
Linking agent 5～20
Softening agent 2～15
Solvent 5～20
Tensio-active agent 0.2～2
Sterilant 0.2～1
PH conditioning agent 0.2～2
Deionized water 20～40.
The preferred weight per distribution ratio of described dispersible pigment color paste is:
Pigment 15～30
Hyper-dispersant 15～30
Wetting agent 15～30
Deionized water 10～40.
Specifically, pigment is selected from one or more the combination in Pigment black (C.I.Pigment Black), pigment green grass or young crops (C.I.Pigment Cyan), pigment fuchsin (C.I.Pigment Magenta), Pigment blue (C.I.Pigment Blue), Pigment red (C.I.PigmentRed), Pigment Yellow 73 (C.I.Pigment Yellow), pigment orange (C.I.Pigment Orange), the Pigment green (C.I.Pigment Green); Described hyper-dispersant is a non-ionic polymer; Described wetting agent is selected from a kind of in propylene glycol, glycerine, the glycol ether.Described hyper-dispersant is used for the ground pigment mill base, improves the wettability and the glossiness of pigment, lowers to grind viscosity, makes to keep stable between the granules of pigments in the mill base mutually, and prevents that effectively pigment from the phenomenon of flocculation taking place; Wetting agent is used to prevent that ink is dried at the shower nozzle place of printer, guarantees that ink has outstanding stability when the printer closing condition, and does not stop up shower nozzle; Deionized water is in order to guarantee the purity of ink, to make ink can not produce the crystalline phenomenon and plug nozzle.
Described connection material is polyacrylic polymer or ACRYLIC EMULSION, and linking agent is self-crosslinking acrylic resin or waterborne polyurethane resin, and softening agent is selected from a kind of in quadrol, diethylenetriamine, the triethylene tetramine.Described connection material, linking agent, softening agent can make color pigments have good washing fastness, photostabilization on yarn fabric, and soft.
Solvent is selected from a kind of in N～methyl-2-pyrrolidone, 2 methyl-2-pyrrolidones, the diethylene glycol ether, and it is used to increase solvability and dispersiveness.
Tensio-active agent is the low foam surface activity agent of nonionic, and its surface tension that is used to control ink makes ink have the ideal diffustivity at 20-50, thereby guarantees the quality of printing.
Sterilant is the isothiazolinone biocide agent, and it is used to suppress growing of bacterium; Described PH conditioning agent is trolamine or dimethylethanolamine, and it is used to keep the scope of the pH value of ink at 7-9, guarantees the solvability of each composition in ink.
Deionized water in the ink is the carrier of ink, and the purity that it is used to guarantee ink makes ink can not produce the crystalline phenomenon and plug nozzle.
The present invention also provides the preparation method of this stamp textile ink, and this method comprises the steps:
A, be that 15～30% pigment, 15～30% hyper-dispersant, 15～30% wetting agent and 10～40% deionized water are mixed into dispersible pigment color paste with weight percent content, with dispersible pigment color paste high-speed stirring 30～60 minutes, nano level superfine grinding machine for grinding 8～16 hours, obtain nano level superfine particle mill base then;
B, the nano level superfine particle mill base after the mixture of 5～8 parts described proportionings and 2～4 parts the grinding is mixed the back high-speed stirring 30～60 minutes, then after filtration, obtain environment-friendly digital ink-jet direct printing textile ink finished product.
Contribution of the present invention is that it efficiently solves in the existing digital ink-jet printed ink and is easy to problems such as environment pollute because of containing formaldehyde, and it has the following advantages:
One, digital ink-jet printed ink of the present invention can directly carry out digit printing to yarn fabric, incalculability and restriction in batches, can select pattern that the single-piece clothes is carried out stamp flexibly, thereby demand that can very big satisfying personalized product, complied with the international propensity to consume by the trend of standardised prod toward the personalized product development.
Two, digital ink-jet printed ink of the present invention can directly carry out digit printing to yarn fabric, need not plate-making, need not yarn fabric is carried out pre-treatment and aftertreatment, therefore can not produce the water pollution problems of sewage discharge and traditional silk-screen, and formaldehydeless printed textile provides health reassurance for the mankind and the Nature.
Three, digital ink-jet printed ink of the present invention can pass through directly stamp on yarn fabric of digital ink-jet printed flat-panel printer, need not to carry out pre-process and post-process, the yarn fabric of having printed only needs to dry in the 150-180 degree, photostabilization reaches the 7-8 level, washing fastness reaches 45 grades, reaches children's direct cutaneous contact class rank.
Four, use the decalcomania of digital ink-jet printed ink of the present invention to compare with traditional silk-screen, pattern bright-coloured meticulous, the transition color abundant, soft.
[embodiment]
The following example is to further explanation of the present invention and explanation, and the present invention is not constituted any limitation.
One, the preparation of dispersible pigment color paste:
Get any two parts in Pigment black, pigment green grass or young crops, pigment fuchsin, Pigment Yellow 73, Pigment red, Pigment blue, pigment orange, the Pigment green by weight, two parts of hyper-dispersants, two parts of wetting agent glycol ethers, in four parts of adding reaction vessels of deionized water, under the high-speed stirring condition, mixed 50 minutes, form the mill base mixture, then with the mill base mixture nano level superfine grinding machine for grinding 12 hours, obtain nano level superfine particle mill base.
Two, the preparation of environment-friendly formaldehyde-free digital ink-jet direct printing weaving coating ink:
Get 30 parts of the nano level superfine particle mill bases that ground by weight, connect 8 parts of material polyacrylic polymers, 8 parts of linking agent self-crosslinking acrylic resins, 4 parts of quadrol softening agents, 10 parts of N～crassitude ketone solvent, 1 part of non-ionic type defoamer, 0.2 part of isothiazolinone biocide agent, 0.2 part of trolamine PH conditioning agent, in 30 parts of adding reaction vessels of deionized water, under the high-speed stirring condition, mixed 50 minutes, filter processing then, first pass filters with the filter membrane of aperture 1.0um, and second time the filter membrane with aperture 0.5um filters, the 3rd time the filter membrane with aperture 0.3um filters, and is not contained the environment-friendly digital ink-jet direct printing weaving coating ink finished product of formaldehyde at last.
Test shows that environment-friendly digital ink-jet direct printing textile ink of the present invention has following feature:
1. surface tension is 20-50dyn/cm
2. viscosity is 2-5mPa*sec
3.PH value is 7-9Ph
4. specific conductivity is 2000-8000Ms/cm
5. photostabilization is the 7-8 level
6. water-wash resistance is 45 grades
7. weathering resistance is 6 grades
Digital ink-jet direct printing weaving coating ink of the present invention, by digital ink-jet printed flat-panel printer, can directly carry out number on multiple yarn fabric (cotton, silk, terylene, wool etc.) prints, bright in luster, soft, have digital print meticulous advantage and transition color abundant effects, photostabilization reaches the 7-8 level, washing fastness reaches 45 grades, need not make a plate, need not pre-treatment and aftertreatment, printout only needs to solve the pollution problem that traditional screen printing brings in the oven dry of 150-180 degree.
Claims (10)
- [claim 1] a kind of environment-friendly digital ink-jet direct printing textile ink is characterized in that it is the mixture of following component by weight percentage:Dispersible pigment color paste 12～55Connect material 5～20Linking agent 5～20Softening agent 2～15Solvent 5～20Tensio-active agent 0.2～2Sterilant 0.2～1PH conditioning agent 0.2～2Deionized water 20～40.
- [claim 2] environment-friendly digital ink-jet as claimed in claim 1 direct printing textile ink is characterized in that, described dispersible pigment color paste is that the following component by the weight percent proportioning mixes:Pigment 15～30Hyper-dispersant 15～30Wetting agent 15～30Deionized water 10～40.
- [claim 3] environment-friendly digital ink-jet as claimed in claim 2 direct printing textile ink, it is characterized in that described pigment is selected from one or more the combination in Pigment black, pigment green grass or young crops, pigment fuchsin, Pigment blue, Pigment red, Pigment Yellow 73, pigment orange, the Pigment green; Described hyper-dispersant is a non-ionic polymer; Described wetting agent is selected from a kind of in propylene glycol, glycerine, the glycol ether.
- [claim 4] environment-friendly digital ink-jet as claimed in claim 1 direct printing textile ink is characterized in that described connection material is polyacrylic polymer or ACRYLIC EMULSION.
- [claim 5] environment-friendly digital ink-jet as claimed in claim 1 direct printing textile ink is characterized in that described linking agent is self-crosslinking acrylic resin or waterborne polyurethane resin.
- [claim 6] environment-friendly digital ink-jet as claimed in claim 1 direct printing textile ink is characterized in that, described softening agent is selected from a kind of in quadrol, diethylenetriamine, the triethylene tetramine.
- [claim 7] environment-friendly digital ink-jet as claimed in claim 1 direct printing textile ink is characterized in that, described solvent is selected from a kind of in N～methyl-2-pyrrolidone, 2-methyl-2-pyrrolidone, the diethylene glycol ether.
- [claim 8] environment-friendly digital ink-jet as claimed in claim 1 direct printing textile ink is characterized in that, described tensio-active agent is the low foam surface activity agent of nonionic.
- [claim 9] environment-friendly digital ink-jet as claimed in claim 1 direct printing textile ink is characterized in that described sterilant is the isothiazolinone biocide agent; Described PH conditioning agent is trolamine or dimethylethanolamine.
- The preparation method of the described environment-friendly digital ink-jet of [claim 10] claim 1 direct printing textile ink is characterized in that it comprises the steps:A, be that 15～30% pigment, 15～30% hyper-dispersant, 15～30% wetting agent and 10～40% deionized water are mixed into dispersible pigment color paste with weight percent content, with dispersible pigment color paste high-speed stirring 30～60 minutes, nano level superfine grinding machine for grinding 8～16 hours, obtain nano level superfine particle mill base then;B, the nano level superfine particle mill base after the mixture of 5～8 parts described proportionings and 2～4 parts the grinding is mixed the back high-speed stirring 30～60 minutes, then after filtration, obtain environment-friendly digital ink-jet direct printing textile ink finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910301072 CN101531848B (en) | 2009-03-24 | 2009-03-24 | An environment-friendly digital ink-jet direct printing textile ink and method for preparing same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910301072 CN101531848B (en) | 2009-03-24 | 2009-03-24 | An environment-friendly digital ink-jet direct printing textile ink and method for preparing same |
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| Publication Number | Publication Date |
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| CN101531848A true CN101531848A (en) | 2009-09-16 |
| CN101531848B CN101531848B (en) | 2011-10-05 |
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