CN110713753A - Textile ink for light-regulating nozzle and preparation method thereof - Google Patents
Textile ink for light-regulating nozzle and preparation method thereof Download PDFInfo
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- CN110713753A CN110713753A CN201910918855.5A CN201910918855A CN110713753A CN 110713753 A CN110713753 A CN 110713753A CN 201910918855 A CN201910918855 A CN 201910918855A CN 110713753 A CN110713753 A CN 110713753A
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- polymer emulsion
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/322—Pigment inks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/324—Inkjet printing inks characterised by colouring agents containing carbon black
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/36—Inkjet printing inks based on non-aqueous solvents
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- D06P1/525—Polymers of unsaturated carboxylic acids or functional derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/90—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dyes dissolved in organic solvents or aqueous emulsions thereof
- D06P1/92—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dyes dissolved in organic solvents or aqueous emulsions thereof in organic solvents
- D06P1/928—Solvents other than hydrocarbons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/30—Ink jet printing
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a textile ink for a light-management nozzle, which comprises the following components in parts by weight: the feed is prepared from the following raw materials in parts by weight: pigment color paste: 200-300 parts; aqueous acrylic polymer emulsion: 100-200 parts; solvent: 400-550 parts; surfactant (b): 10-20 parts; curing agent: 20-40 parts; and (3) bactericide: 1-10 parts; pH value regulator: 2-10 parts; deionized water: 10-200 parts; the average particle size of the water-based acrylic polymer emulsion is less than 200nm, and the glass transition temperature of the water-based acrylic polymer emulsion is less than-20 ℃; the solvent is one or more selected from diethylene glycol, propylene glycol, glycerol, polyethylene glycol, 1-5 pentanediol and hexanediol; the surfactant is an anionic surfactant. The invention also provides a preparation method of the textile ink for the light-management nozzle, which comprises the steps of adding the raw materials, mixing and stirring, and filtering twice by using a 1.0Um filter membrane to obtain the textile ink for the light-management nozzle. Because the average particle size of the resin is below 200nm, agglomeration and flocculation are avoided, the nozzle is prevented from being blocked, and the ink has good stability and printing fluency.
Description
Technical Field
The invention relates to the field of digital printing, in particular to textile ink for a light-management nozzle, and especially relates to textile ink for a light-management nozzle and a preparation method thereof.
Background
The digital direct-injection coating printing is mainly to directly spray and print patterns or images on textiles by adopting digital direct-injection textile coating ink through a wide-format printer. Digital direct-injection pigment printing has many advantages: the fiber has universality for different fibers; the process is simple, and the finished product is obtained by directly baking at high temperature after printing; no sewage discharge, and environmental protection is facilitated; the light fastness is good. Due to the advantages, the digital direct-injection pigment printing is favored by a plurality of printing manufacturers, and the development is faster in recent years. The Epson heads commonly used in the market have high printing precision, but have low printing speed, and cannot meet the requirements of printing piece cloth, curtains and the like on the printing speed, so that a plurality of industrial spray head printers are used for digital printing of cloth. Common industrial nozzles are rational light, starlight, Konika and the like, and because each type of printing head has different ink jet drops and different requirements on the viscosity of ink, common industrial nozzle printers are matched with special ink. In recent years, the light-regulating industrial spray head is very suitable for industrial digital printing, has accurate ink dots, strong spraying force, open ink system, wide printing scheme and quick development, is second to an Epson DX spray head and leaps second. The printer mainly comprises MIMAKI, color god, Dingshang, win, Xuanlang, Rui Nuo Si, etc.
However, in the prior art, because the scheme that the light-regulating nozzle is used for the pure cotton direct-injection printing machine is not long in the world, the matched printing ink is less, and most of the light-regulating nozzle inks on the market have the problems of poor printing smoothness and poor dry and wet rubbing fastness.
Disclosure of Invention
The invention provides textile ink for a light-management nozzle, which effectively improves the dry and wet rubbing fastness of the ink and the smoothness of printing.
In order to solve the technical problems, the technical scheme of the invention is as follows:
a textile ink for a light management nozzle: the feed is prepared from the following raw materials in parts by weight:
pigment color paste: 200-300 parts; aqueous acrylic polymer emulsion: 100-200 parts; solvent: 400-550 parts; surfactant (b): 10-20 parts; curing agent: 20-40 parts; and (3) bactericide: 1-10 parts; pH value regulator: 2-10 parts; deionized water: 10-200 parts; the average particle size of the water-based acrylic polymer emulsion is less than 200nm, and the glass transition temperature of the water-based acrylic polymer emulsion is less than-20 ℃; the solvent is one or more selected from diethylene glycol, propylene glycol, glycerol, polyethylene glycol, 1-5 pentanediol and hexanediol; the surfactant is an anionic surfactant.
The glass transition temperature (Tg) of the water-based acrylic polymer emulsion is below-20 ℃, so that the softness of a coating film is ensured; the aqueous acrylic polymer emulsion is preferred624,
One or two of HRC 1661.
The aqueous acrylic polymer emulsion imparts good adhesion of the ink to textiles.
The average particle size of the resin is below 200nm, and the resin can be stable for a long time in an ink system and cannot generate agglomeration and flocculation.
The solvent is selected from diethylene glycol, propylene glycol, glycerol, polyethylene glycol and 1-5 pentanediol, and the hexanediol endows the ink with proper viscosity and good moisturizing performance.
Preferably, the feed is prepared from the following raw materials in parts by weight:
pigment color paste: 200 portions and 250 portions; aqueous acrylic polymer emulsion: 100-150 parts; solvent: 400-480 parts; surfactant (b): 10-15 parts; curing agent: 20-30 parts of a solvent; and (3) bactericide: 2-3 parts of a solvent; pH value regulator: 2-6 parts; deionized water: 10-156 parts.
More preferably, the feed additive is prepared from the following raw materials in parts by weight:
pigment color paste: 250-300 parts; aqueous acrylic polymer emulsion: 150-200 parts; solvent: 480-550 parts; surfactant (b): 15-20 parts of a solvent; curing agent: 30-40 parts; and (3) bactericide: 3-10 parts; pH value regulator: 6-10 parts; deionized water: 156 portion and 200 portions.
More preferably, the feed additive is prepared from the following raw materials in parts by weight:
pigment color paste: 250 parts of (A); aqueous acrylic polymer emulsion: 150 parts; solvent: 480 parts of a mixture; surfactant (b): 15 parts of (1); curing agent: 30 parts of (1); and (3) bactericide: 3 parts of a mixture; pH value regulator: 6 parts of (1); deionized water: 74 parts. The pigment color paste comprises a black pigment, a blue pigment, a red pigment and a yellow pigment, wherein the black pigment is carbon black.
The blue pigment is pigment blue 15:3 and pigment blue 15: 4; the red pigment is pigment red 122 and pigment red 205; the yellow pigments are pigment yellow 155, pigment yellow 74.
More preferably, the curing agent is selected from blocked isocyanates; the bactericide is benzisothiazolinone; the pH value regulator is one of trihydroxymethyl aminomethane or triethanolamine.
In another aspect, the present invention provides a method for preparing textile ink, comprising the following steps:
s1) raw material preparation: adding a solvent, a surfactant, a bactericide and a pH value regulator into deionized water in sequence according to parts by weight;
s2) mixing: stirring the raw materials at a high speed for 5 minutes, adding the aqueous acrylic polymer emulsion, and stirring at a high speed for 30 minutes;
s3) stirring: adding pigment color paste and curing agent, and continuing to stir at high speed for 2 hours;
s4) filtering: and filtering twice through a 1.0-Um filter membrane to obtain the textile ink for the light-management nozzle.
By adopting the technical scheme, the glass transition temperature (Tg) of the aqueous acrylic polymer emulsion is below-20 ℃, so that the softness of a coating film is ensured, the coating film can not crack when printed on a textile, and the dry and wet rubbing fastness of a printed pattern is obviously improved by combining the good adhesion performance of the ink on the textile given by the aqueous acrylic polymer emulsion. In addition, the average resin particle size of the aqueous acrylic polymer emulsion is below 200nm, and the aqueous acrylic polymer emulsion can be stable for a long time in an ink system, cannot generate agglomeration and flocculation, prevents a spray head from being blocked, and endows the ink with good stability and printing fluency. In addition, the solvent is selected from diethylene glycol, propylene glycol, glycerol, polyethylene glycol, 1-5 pentanediol and hexanediol, so that the ink is endowed with proper viscosity and good moisture retention performance, and the ink can also have good printing fluency.
Detailed Description
The following further describes the embodiments of the present invention. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
A preparation method of textile ink comprises the following steps:
s1) raw material preparation: adding a solvent, a surfactant, a bactericide and a pH value regulator into deionized water in sequence according to parts by weight;
s2) mixing: stirring the raw materials at a high speed for 5 minutes, adding the aqueous acrylic polymer emulsion, and stirring at a high speed for 30 minutes;
s3) stirring: adding pigment color paste and curing agent, and continuing to stir at high speed for 2 hours;
s4) filtering: and filtering twice through a 1.0-Um filter membrane to obtain the textile ink for the light-management nozzle. Example 1, example 2, example 3 and comparative examples were prepared according to the procedure of example 1, the above preparation procedure and the formulation of table 1 below.
TABLE 1 ink formulations (in weight percent) of the examples
Blue ink, red ink and yellow ink of each example were prepared according to the formulation of table 1 and the above preparation method.
The physical and chemical parameters of the prepared ink are as follows:
pH value: 7-9;
surface tension: 25-40 dyn/cm;
viscosity: 8-12 mpa · s;
conductivity: ≦ 1 mS/cm;
and testing dry and wet rubbing fastness on a dry and wet rubbing fastness instrument according to the AATCC 8-2013 standard.
And (3) printing fluency testing, namely continuously printing by 4pass for 30m on a Caishen TX-3200DS direct-injection printing machine, and judging that the printing is qualified when the number of broken holes is less than 3.
The test results are shown in table 2:
TABLE 2 ink Dry and Wet rub fastness and printing Performance
| Fastness to dry rubbing | Fastness to wet rubbing | Fluency of printing | |
| Example 1 | 3.5 | 3.0 | Qualified |
| Example 2 | 4.0 | 3.0 | Qualified |
| Example 3 | 4.0 | 3.5 | Qualified |
| Comparative example | 3.0 | 2.5 | Fail to be qualified |
The finishing Gen5 nozzle textile coating ink can directly print patterns typeset by a computer on various fabrics through a digital printing printer, has bright and bright color, high dry and wet rubbing color fastness and good printing smoothness, does not crack when being stretched, does not need the processes of plate making, pretreatment and post-treatment of the traditional printing process, and only needs to be dried after printing finished products, thereby saving energy and protecting environment.
The embodiments of the present invention have been described in detail, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.
Claims (6)
1. A textile ink for a light management nozzle is characterized in that: the feed is prepared from the following raw materials in parts by weight:
pigment color paste: 200-300 parts; aqueous acrylic polymer emulsion: 100-200 parts; solvent: 400-550 parts; surfactant (b): 10-20 parts; curing agent: 20-40 parts; and (3) bactericide: 1-10 parts; pH value regulator: 2-10 parts; deionized water: 10-200 parts; the average particle size of the aqueous acrylic polymer emulsion is less than 200nm, and the glass transition temperature of the aqueous acrylic polymer emulsion is less than-20 ℃; the solvent is one or more selected from diethylene glycol, propylene glycol, glycerol, polyethylene glycol, 1-5 pentanediol and hexanediol; the surfactant is an anionic surfactant.
2. The textile ink of claim 1, wherein: the feed is prepared from the following raw materials in parts by weight:
pigment color paste: 200 portions and 250 portions; aqueous acrylic polymer emulsion: 100-150 parts; solvent: 400-480 parts; surfactant (b): 10-15 parts; curing agent: 20-30 parts of a solvent; and (3) bactericide: 2-3 parts of a solvent; pH value regulator: 2-6 parts; deionized water: 10-156 parts.
3. The textile ink of claim 1, wherein: the feed is prepared from the following raw materials in parts by weight:
pigment color paste: 250-300 parts; aqueous acrylic polymer emulsion: 150-200 parts; solvent: 480-550 parts; surfactant (b): 15-20 parts of a solvent; curing agent: 30-40 parts; and (3) bactericide: 3-10 parts; pH value regulator: 6-10 parts; deionized water: 156 portion and 200 portions.
4. The textile ink of claim 1, wherein: the feed is prepared from the following raw materials in parts by weight:
pigment color paste: 250 parts of (A); aqueous acrylic polymer emulsion: 150 parts; solvent: 480 parts of a mixture; surfactant (b): 15 parts of (1); curing agent: 30 parts of (1); and (3) bactericide: 3 parts of a mixture; pH value regulator: 6 parts of (1); deionized water: 74 parts of; the pigment color paste comprises a black pigment, a blue pigment, a red pigment and a yellow pigment, wherein the black pigment is carbon black.
5. The textile ink of claim 1, wherein: the curing agent is selected from blocked isocyanate; the bactericide is benzisothiazolinone; the pH value regulator is one of trihydroxymethyl aminomethane or triethanolamine.
6. A process for the preparation of a textile ink according to any one of claims 1 to 5, characterized in that: the method comprises the following steps:
s1) raw material preparation: adding a solvent, a surfactant, a bactericide and a pH value regulator into deionized water in sequence according to parts by weight;
s2) mixing: stirring the raw materials at a high speed for 5 minutes, adding the aqueous acrylic polymer emulsion, and stirring at a high speed for 30 minutes;
s3) stirring: adding pigment color paste and curing agent, and continuing to stir at high speed for 2 hours;
s4) filtering: and filtering twice through a 1.0-Um filter membrane to obtain the textile ink for the light-management nozzle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910918855.5A CN110713753A (en) | 2019-09-26 | 2019-09-26 | Textile ink for light-regulating nozzle and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910918855.5A CN110713753A (en) | 2019-09-26 | 2019-09-26 | Textile ink for light-regulating nozzle and preparation method thereof |
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| CN110713753A true CN110713753A (en) | 2020-01-21 |
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Application publication date: 20200121 |