CN106675092A - Environment-friendly type composite disperse dye and preparation method and application thereof - Google Patents
Environment-friendly type composite disperse dye and preparation method and application thereof Download PDFInfo
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- CN106675092A CN106675092A CN201611267658.4A CN201611267658A CN106675092A CN 106675092 A CN106675092 A CN 106675092A CN 201611267658 A CN201611267658 A CN 201611267658A CN 106675092 A CN106675092 A CN 106675092A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0041—Blends of pigments; Mixtured crystals; Solid solutions mixtures containing one azo dye
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0079—Azoic dyestuff preparations
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/18—Azo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
- D06P3/6033—Natural or regenerated cellulose using dispersed dyes
Abstract
The invention provides environment-friendly type composite disperse dye and a preparation method thereof. The environment-friendly type composite disperse dye is basically prepared from the following ingredients in parts by mass: 5 to 50 parts of dye monomer A which is as shown in a formula (I), 0 to 14 parts of dye monomer B which is as shown in a formula (II) and 2 to 25 parts of dye monomer C which is as shown in a formula (III). The environment-friendly type composite disperse dye provided by the invention is very suitable for dyeing and printing of polyester materials and acetate fiber materials, is good in light fastness, high in dyeing power, and bright in color light, has better covering property, better level-dyeing property, better lifting property and better absorption and purification property and is the main dye for dyeing medium to light color, and the environment-friendly type composite disperse dye not only can be used as monochrome, but also has better compatibility.
Description
(1) technical field
The present invention relates to a kind of environment-friendly type composite disperse dye and preparation method and application, compound point of described environment-friendly type
Scattered dyestuff is particularly well-suited to dyeing and the stamp of polyester material and vinegar fiber material.
(2) background technology
From the point of view of textile fabric present situation, there is the ratio shared by the fabric that multiple fiber combines to increase year by year, such as state
The medium-to-high grade fabric of some interior, including polyester blended fabric etc..The disperse dyes supplied in the market, can't expire well
The printing and dyeing of sufficient such textile need.The kind of the dyeing Yellow disperse dye of polyester material and vinegar fiber material is a lot, such as
C.I. the usage amount of disperse yellow 23 (strong yellow RGFL) is than larger, but due to dyestuff bisazo molecule knot under given conditions
Unstable can the cracking of structure and produce carcinogenic suspicious material or harmful aromatic amine, be classified as disabling by European Union member countries already
Disperse dyes.So the environment-friendly type composite disperse dye for substituting strong yellow RGFL just becomes the succedaneum is badly in need of by printing and dyeing producer, and
And the succedaneum should possess that coloured light is approximate therewith, tint applications performance is also approximate, can be with the low temperature such as Disperse Blue 2BLN, Disperse Red 3B
The characteristics of type dye has preferable compatibility, to meet needed for printed textile outlet.
Some for occurring in the market substitute the golden yellow disperse dyes of C.I. disperse yellows 23, the gradually reality of Jing printing and dyeing producer
Use rear discovery, with the colorant match such as Disperse Blue 2BLN, Disperse Red 3B during compatibility it is poor, there is poor end to end, overflow dyeing in dye gigging
Easily there is dyeing defect phenomenon, so the effective succedaneum for substituting strong yellow RGFL is badly in need of in printing and dyeing producer.
(3) content of the invention
To solve the environmental issue of C.I. disperse yellows 23 and asking with the compatibility of the low temperature dyestuff such as Disperse Blue 2BLN, Disperse Red 3B
Topic, the invention provides a kind of environment-friendly type composite disperse dye.
The present invention is adopted the following technical scheme that：
A kind of environment-friendly type composite disperse dye, is substantially made up of the component of following mass parts：
5~50 parts of dye monomer A shown in formula (I)；
0~14 part of dye monomer B shown in formula (II) (0 is meant that without dye monomer B, similarly hereinafter)；
2~25 parts of dye monomer C shown in formula (III).
Preferably, the environment-friendly type composite disperse dye is substantially made up of the component of following mass parts：
8~40 parts of dye monomer A shown in formula (I)；
0~5 part of dye monomer B shown in formula (II)；
15~25 parts of dye monomer C shown in formula (III).
The connotation of indication " substantially " of the present invention refers to that described environment-friendly type composite disperse dye can also be comprising auxiliary agent, institute
Any dyestuff usual auxiliaries that the auxiliary agent stated is known in the art, for example, may be selected from but be not limited to the one kind in following material or two
Plant the mixture of any of the above ratio：Naphthalene sulfonic acid-formaldehyde condensation product, alkyl naphthalene sulfonic acid formaldehyde condensation products, lignosulfonates, benzyl
Base naphthalenesulfonate formaldehyde condensation compound, Matrii Sulfas Exsiccatus.Described naphthalene sulfonic acid-formaldehyde condensation product such as dispersing agent NNO；Alkyl naphthalene sulfonic acid formaldehyde
Condensation substance such as Dispersant MF (condensation compound of methyl naphthalene sulfonic acid and formaldehyde)；Lignosulfonates such as sodium lignin sulfonate is (as sold on market
Dispersant Reax83A, Reax85A for selling)；Benzyl naphthalenesulfonate formaldehyde condensation compound such as dispersing agent CNF.But the present invention is not excluded for
Directly with the compositionss of dye monomer as intermediate products before adding assistant, added auxiliary agent again before dyeing is applied to.
The quality consumption of the auxiliary agent is usually dye monomer A, dye monomer B, dye monomer C three's quality sum
0.01~13.2 times, preferably 0.4~3.3 times.
Particularly preferred, environment-friendly type composite disperse dye of the present invention is made up of the component of following mass parts：
30 parts of dye monomer A shown in formula (I)；
10 parts of dye monomer B shown in formula (II)；
10 parts of dye monomer C shown in formula (III)；
50 parts of auxiliary agent；
Described auxiliary agent is condensation compound of methyl naphthalene sulfonic acid and formaldehyde, sodium lignin sulfonate, in Matrii Sulfas Exsiccatus one or two with
The mixture of upper arbitrary proportion.
Same particularly preferred, environment-friendly type composite disperse dye of the present invention is made up of the component of following mass parts：
20 parts of dye monomer A shown in formula (I)；
9 parts of dye monomer B shown in formula (II)；
7 parts of dye monomer C shown in formula (III)；
64 parts of auxiliary agent；
Described auxiliary agent is condensation compound of methyl naphthalene sulfonic acid and formaldehyde, sodium lignin sulfonate, in Matrii Sulfas Exsiccatus one or two with
The mixture of upper arbitrary proportion.
Present invention also offers the preparation method of the environment-friendly type composite disperse dye, described preparation method is：
The dye monomer A of formula metering ratio, dye monomer B, dye monomer C, auxiliary agent are added to the water, after mix homogeneously,
Dispersion is ground with grinder, then 120~135 DEG C, 3.5~5.0MPa of atomisation pressure, solid content 40%~45%
Under the conditions of be spray-dried, obtain final product product environment-friendly type composite disperse dye of the present invention；
The quality consumption of the water is usually all components raw material (i.e. described dye monomer A, dye monomer B, dyestuff list
Body C and auxiliary agent) 1~1.5 times of quality sum.
Environment-friendly type composite disperse dye of the present invention can also be prepared as follows：
First by dye monomer A and auxiliary agent finished product dyestuff C.I. dispersion yellow 64s, by dye monomer B and auxiliary agent finished product
Dyestuff C.I. disperse yellows 54, by dye monomer C and auxiliary agent finished product dyestuff C.I. disperse orange 25s, take according still further to formula metering ratio
Obtained three kinds of finished product dyestuffs (with the cubage of dye monomer A, dye monomer B, dye monomer C in three kinds of finished product dyestuffs),
(if necessary) after supplying the amount of auxiliary agent needed for formula, add water blending, grinding distribution, is then spray-dried (spray drying
Condition is same as described above), obtain final product product environment-friendly type composite disperse dye of the present invention.
Or, it is also possible to three kinds of finished product dyestuffs obtained above are taken (to contaminate in three kinds of finished product dyestuffs according to formula metering ratio
Material list body A, dye monomer B, the cubage of dye monomer C), after (if necessary) supplies the amount of the auxiliary agent needed for formula, directly
Row blending is tapped into, is ground to and is uniformly dispersed, obtain final product product environment-friendly type composite disperse dye of the present invention.
Equally, it is also possible to directly buy commercially available prod C.I. dispersion yellow 64 original dyestuffs, 54 former dyestuff of C.I. disperse yellows, C.I.
Disperse orange 25 original dyestuff carries out the preparation of product environment-friendly type composite disperse dye of the present invention.
Environment-friendly type composite disperse dye of the present invention can be applicable to dyeing and the stamp of polyester material and vinegar fiber material.
The beneficial effects of the present invention is：
(1) due to environment-friendly type composite disperse dye of the present invention with low temperature type dye (such as Disperse Blue 2BLN, dispersion
Red 3B) match when the compatibility compatibility it is more satisfactory, can effectively substitute strong yellow RGFL, not only solve environmental issue but also solved
The phenomenons such as the aberration dyeing defect occurred in some succedaneum such as decentralized decoupling uses；
(2) environment-friendly type composite disperse dye of the present invention be highly suitable for polyester material, the dyeing of vinegar fiber material and
Stamp, and light fastness is excellent, tinting power is high, bright in color light, with preferable opacifying property, level-dyeing property, enhancing and exhaustion property
Can, be the primary dye of light color in dye, not only can as it is monochromatic using but also can with Disperse Red 3B (or FB), Disperse Blue 2BLN have compared with
Good compatibility.
(4) specific embodiment
With reference to specific embodiment, the invention will be further described, but protection scope of the present invention is not limited in
This.
The commercial dye C.I. dispersion yellow 64s (monomer A contents be 56%, remaining is auxiliary agent) used in following examples,
C.I. disperse yellow 54 (monomer B content is 55%, and remaining is auxiliary agent), (monomer C content is 42% to C.I. disperse orange 25s, and remaining is
Auxiliary agent), provided by the production of Zhejiang Bo Ao dye industries company limited.
Embodiment 1~8
According to continuous data shown in table 1, by dye monomer A, dye monomer B, auxiliary agent【Dispersant MF (methyl naphthalene sulfonic acid first
Aldehyde condensate), it is dispersing agent CNF (benzyl naphthalenesulfonate formaldehyde condensation compound), dispersing agent NNO (naphthalene sulfonic acid-formaldehyde condensation product), wooden
Plain sodium sulfonate, Matrii Sulfas Exsiccatus】After the blending that adds water, with SB250 sand mills according to 0.5~1.0m of flow3/ h is ground dispersion,
120~135 DEG C, 3.5~5.0MPa of atomisation pressure, be spray-dried under conditions of solid content 40%~45%.
Table 1
Embodiment 9~11
According to continuous data shown in table 2, by C.I. dispersion yellow 64s, C.I. disperse yellows 54, C.I. disperse orange 25s, auxiliary agent【Point
Powder MF (condensation compound of methyl naphthalene sulfonic acid and formaldehyde), dispersing agent CNF (benzyl naphthalenesulfonate formaldehyde condensation compound), dispersing agent NNO (naphthalene sulphur
Sour formaldehyde condensation products), sodium lignin sulfonate, Matrii Sulfas Exsiccatus】After the blending that adds water, with SB250 grinders according to 0.5~1.0m3/ of flow
H is ground dispersion, the spray dried under conditions of 120~135 DEG C, 3.5~5.0MPa of atomisation pressure, solid content 40%~45%
It is dry.
Table 2
Embodiment 12~15
According to data shown in table 3, C.I. dispersion yellow 64s, C.I. disperse yellows 54, C.I. disperse orange 25s, auxiliary agent【Dispersant MF
(condensation compound of methyl naphthalene sulfonic acid and formaldehyde), dispersing agent NNO (naphthalene sulfonic acid-formaldehyde condensation product), sodium lignin sulfonate, Matrii Sulfas Exsiccatus】Directly enter
Row blending, is ground to and is uniformly dispersed.
Table 3
Embodiment 16
Disperse dyes obtained in respectively taking 0.5 gram of embodiment 1-15 are dispersed in 500 milliliters of water, with 60 after drawing 20 milliliters
Milliliter water mixing.Dye bath pH=5 is adjusted with acetic acid, 70 DEG C is warming up to and is dyeed while being put into 2 grams of polyester fibers, in 30 minutes
Temperature rises to 130 DEG C by 70 DEG C, is incubated 30 minutes, starts sampling, watch its color when being cooled to 90 DEG C；With Disperse Blue 2BLN and
Disperse Red 3B colorant match, observes its compatibility with low temperature disperse dyes；Using GB GB/T3921-1997, GB/T3920-
1997th, GB/T8427-1998, GB/T5718-1997, test its fastness respectively.Test result is shown in Table 4.
Comparative example 1
Take 0.5 gram of 23 dyestuff of C.I. disperse yellows and repeat embodiment 16.
Table 4
Claims (8)
1. a kind of environment-friendly type composite disperse dye, it is characterised in that described environment-friendly type composite disperse dye is substantially by following matter
The component composition of amount part：
5~50 parts of dye monomer A shown in formula (I)；
0~14 part of dye monomer B shown in formula (II)；
2~25 parts of dye monomer C shown in formula (III)；
2. environment-friendly type composite disperse dye as claimed in claim 1, it is characterised in that described environment-friendly type composite disperse dye
Substantially it is made up of the component of following mass parts：
8~40 parts of dye monomer A shown in formula (I)；
0~5 part of dye monomer B shown in formula (II)；
15~25 parts of dye monomer C shown in formula (III).
3. environment-friendly type composite disperse dye as claimed in claim 1, it is characterised in that described environment-friendly type composite disperse dye
It is made up of the component of following mass parts：
5~50 parts of dye monomer A shown in formula (I)；
0~14 part of dye monomer B shown in formula (II)；
2~25 parts of dye monomer C shown in formula (III).
4. environment-friendly type composite disperse dye as claimed in claim 1, it is characterised in that described environment-friendly type composite disperse dye
It is made up of the component of following mass parts：
5~50 parts of dye monomer A shown in formula (I)；
0~14 part of dye monomer B shown in formula (II)；
2~25 parts of dye monomer C shown in formula (III)；
And auxiliary agent, the quality consumption of the auxiliary agent is dye monomer A, dye monomer B, dye monomer C three's quality sum
0.01~13.2 times.
5. environment-friendly type composite disperse dye as claimed in claim 4, it is characterised in that the quality consumption of the auxiliary agent is dyestuff
Monomer A, dye monomer B, 0.4~3.3 times of dye monomer C three's quality sum.
6. environment-friendly type composite disperse dye as claimed in claim 4, it is characterised in that described auxiliary agent is in following material
One or more arbitrary proportions mixture：Naphthalene sulfonic acid-formaldehyde condensation product, alkyl naphthalene sulfonic acid formaldehyde condensation products, lignin
Sulfonate, benzyl naphthalenesulfonate formaldehyde condensation compound, Matrii Sulfas Exsiccatus.
7. the preparation method of environment-friendly type composite disperse dye as claimed in claim 4, it is characterised in that described preparation method
For：
The dye monomer A of formula metering ratio, dye monomer B, dye monomer C, auxiliary agent are added to the water, after mix homogeneously, with grinding
Grinding machine is ground dispersion, then 120~135 DEG C, 3.5~5.0MPa of atomisation pressure, solid content 40%~45% condition
Under be spray-dried, obtain final product described environment-friendly type composite disperse dye.
8. dyeing of the environment-friendly type composite disperse dye as described in any one of claim 1~6 in polyester material and vinegar fiber material
With the application in stamp.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611267658.4A CN106675092A (en) | 2016-12-31 | 2016-12-31 | Environment-friendly type composite disperse dye and preparation method and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611267658.4A CN106675092A (en) | 2016-12-31 | 2016-12-31 | Environment-friendly type composite disperse dye and preparation method and application thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107298875A (en) * | 2017-01-23 | 2017-10-27 | 浙江博澳染料工业有限公司 | A kind of economic and environment-friendly type disperse dyes |
| CN107868488A (en) * | 2017-12-04 | 2018-04-03 | 浙江龙盛化工研究有限公司 | A kind of yellow disperse dye composition and dye preparations |
| CN110982300A (en) * | 2020-01-15 | 2020-04-10 | 浙江博澳染料工业有限公司 | Environment-friendly disperse golden dye and application thereof |
| CN112920620A (en) * | 2019-12-06 | 2021-06-08 | 嘉兴市创色化工原料有限公司 | Composition for gray disperse dye and gray disperse dye |
| WO2021149703A1 (en) * | 2020-01-20 | 2021-07-29 | 日本化薬株式会社 | Colored dispersion, recording medium, and textile printing method for hydrophobic fibers |
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| CN107298875A (en) * | 2017-01-23 | 2017-10-27 | 浙江博澳染料工业有限公司 | A kind of economic and environment-friendly type disperse dyes |
| CN107868488A (en) * | 2017-12-04 | 2018-04-03 | 浙江龙盛化工研究有限公司 | A kind of yellow disperse dye composition and dye preparations |
| CN107868488B (en) * | 2017-12-04 | 2019-11-29 | 浙江龙盛化工研究有限公司 | A kind of yellow disperse dye composition and dye preparations |
| CN112920620A (en) * | 2019-12-06 | 2021-06-08 | 嘉兴市创色化工原料有限公司 | Composition for gray disperse dye and gray disperse dye |
| CN110982300A (en) * | 2020-01-15 | 2020-04-10 | 浙江博澳染料工业有限公司 | Environment-friendly disperse golden dye and application thereof |
| WO2021149703A1 (en) * | 2020-01-20 | 2021-07-29 | 日本化薬株式会社 | Colored dispersion, recording medium, and textile printing method for hydrophobic fibers |
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Application publication date: 20170517 |