CN101461771A - Nonalcoholic Chinese medicine cologne water and method for producing the same - Google Patents
Nonalcoholic Chinese medicine cologne water and method for producing the same Download PDFInfo
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Abstract
The invention discloses an alcohol-free traditional Chinese medicine toilet water and a production method thereof. The invention aims at providing the toilet water which adopts an alcohol-free solubilizer and sanitizer and is capable of avoiding the impact of the alcohol contained in the toilet water on the human body health and production and use and improving the use and production safety of the toilet water. The toilet water comprises the following components according to the weight percentage: 0.3 to 1 percent of sanitizer, 1 to 3 percent of oil soluble toilet water essence, the solubilizer which is 1-2 times of the weight of the oil soluble toilet water essence, 1 to 5 percent of traditional Chinese medicine extraction solution, and the balance being deionized water. The sanitizer is prepared through the compounding of chlorhexidine acetate and 20 percent water soluble triclocarban; the solubilizer is the mixture of PEG-40 hydrogenated castor oil and PPG-26-butanol polyether-26; and a traditional Chinese medicine extracting solution is the extracting solution taking the mixture of honeysuckle, chrysanthemum indicum, ageratum, liquorice, rheum and snake gall as the traditional Chinese medicine components and taking water as the solvent. As the toilet water does not contain ethanol, the toilet water is favor of guaranteeing the human body health.
Description
Technical field
The present invention relates to a kind of floral water, in particular, relate to a kind of no pure Chinese medicine floral water and production method thereof.
Background technology
Floral water is the traditional summertime hygienic article of China.Mainly be to use the liquid distilled from honeysuckle flowers or lotus leaves quintessence oil, be equipped with a kind of perfume series products that ethanol is made as main body spice.The main effect of floral water is decontamination, sterilization, anti-miliaria, antipruritic, simultaneously, also is a kind of good summertime hygienic article of dispeling fetid sweat.
In the production of floral water, because soluble perfume does not have fragrance retention substantially, can't satisfy the requirement of floral water, therefore, many in the production of traditional floral water is main body with the Oleum lavandula angustifolia of water-fast delicate fragrance or the essence of rosemusk type.In order to dissolve essence, satisfy floral water sterilization, germ-resistant requirement again, need to add 65%～75% ethanol.In floral water, use ethanol mainly to have following problems:
1. ethanol has certain zest to skin, and anaphylaxis appears in easy chafe during use, increases the weight of the dermatitis symptom.
2. ethanol belongs to inflammable thing, breaking out of fire easily in production and the use.For this reason, mostly floral water all indicates the caution term, for example: use after the child should dilute 5 times, keep fire away and use and store, be sure not to be exposed to the sun, try not to allow child's floral water or the like that uses separately and play.
3. in process of production, the easy contaminated environment of ethanol can not satisfy environmental requirement.
Therefore, it is harmful to health to contain ethanol in floral water, and production and safety in utilization are poor.
Summary of the invention
The present invention is in order to overcome weak point of the prior art, a kind of solubilizing agent and disinfectant that does not have alcohol that adopt is provided, avoid the influence of the ethanol that contains in the floral water, improve that floral water uses and the pure Chinese medicine floral water of the nothing of production security health and production and use.
The present invention is achieved through the following technical solutions:
A kind of no pure Chinese medicine floral water is characterized in that, comprises following component in the described floral water by weight percentage: disinfectant 0.3-1%, oil-soluble toilet water essence 1～3%, the solubilizing agent of 1-2 times of oil-soluble toilet water essence weight, Chinese medicine extraction liquid 1～5%, balance of deionized water; Described disinfectant is 20% composite the forming of water solublity triclocarban by chlorhexidine acetate and working substance content by weight percentage, and described chlorhexidine acetate and working substance content by weight percentage are that the weight ratio of 20% water solublity triclocarban is 1:20-30; Described solubilizing agent is that PEG-40 castor oil hydrogenated and PPG-26-butylol polyether-26 are the mixture of the mixed of 1:1-1.5 according to weight ratio; Described Chinese medicine extraction liquid is that mixture with Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis is as Chinese medicine ingredients, with the extracting solution of water as solvent, wherein, the weight ratio of Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis is 1:1:0.5:0.5:0.1:0.1, and the 4kg Chinese medicine extraction liquid is equivalent to the 1kg crude drug.The English full name of triclocarban is Trichlocarban, is called for short: TCC.
In addition, in above-mentioned floral water, can also add some conventional floral water adjuvants with content according to a conventional method, as freshener, anti-allergic agent etc.Freshener can adopt the water-soluble lactic acid menthyl ester, and anti-allergic agent can adopt α-bisabolol.
Described Chinese medicine extraction liquid is the extracting solution that adopts ultrasonic extraction to obtain as Chinese medicine ingredients, with water as solvent with the mixture of Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis.
A kind of production method of not having pure Chinese medicine floral water is characterized in that, comprises the steps:
(1) get the raw materials ready:
The preparation disinfectant: be that 20% water solublity triclocarban is composite by weight the ratio for 1:20-30 with chlorhexidine acetate and working substance content by weight percentage, antibacterial is sterilized;
With solubilizing agent and essence mixing for standby use: with PEG-40 castor oil hydrogenated and PPG-26-butylol polyether-26 is that the mixed of 1:1-1.5 obtains solubilizing agent with the weight ratio, be the mixed of 1:0.5-1 by weight with solubilizing agent and oil-soluble toilet water essence then, speed with 400-500 rev/min stirs, obtain the mixture of solubilizing agent and essence, standby.
The preparation Chinese medicine extraction liquid:
Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis are obtained the Chinese medicine mixture for the mixed of 1:1:0.5:0.5:0.1:0.1 by weight, above-mentioned Chinese medicine mixture is soaked in the water, place ultrasound wave Chinese medicine extractor, under 40-50 ℃ temperature, use ultrasound wave effect 20-30 minute of 20-30KHz, be concentrated to the 4kg extracting solution after the filtration and be equivalent to the 1kg crude drug and obtain Chinese medicine extraction liquid.
(2) mixture, Chinese medicine extraction liquid and the deionized water with the above-mentioned disinfectant that obtains, solubilizing agent and essence fully stirs, mix homogeneously, obtain no pure Chinese medicine floral water of the present invention, wherein, percentage by weight according to the total amount that accounts for no pure Chinese medicine floral water: disinfectant is 0.3-1%, oil-soluble toilet water essence 1～3%, the solubilizing agent of 1-2 times of oil-soluble toilet water essence weight, Chinese medicine extraction liquid 1～5%, balance of deionized water.
In order to obtain best Chinese medicine extraction liquid concentration, Chinese medicine mixture in the step (1) and water are the ratio immersion of 1:7 according to weight ratio.
The present invention has following technique effect:
The present invention by to do not have alcohol solubilizing agent and the choose reasonable of disinfectant, can well be dissolved in essence in the water, be deionized water in the floral water of being produced more than 85%, do not contain ethanol, and, contain the plurality of Chinese composition, dispel except having traditional floral water that miliaria is antipruritic, refreshment, mosquito proof are bitten, fragrant, joyful, go the olfactory function, also have certain heat-clearing and toxic substances removing, reducing swelling and alleviating pain function, and degerming, bactericidal action are arranged.Owing to do not contain ethanol, help ensureing health, improved the safety of using and producing, simultaneously, can satisfy environmental requirement.
2. production method of the present invention can well be dissolved essence.And, by adopting the intensified by ultrasonic wave extraction, do not destroy the Chinese crude drug active ingredient, the extraction time only be decocting in water, alcohol deposition method 1/3rd or still less, improved production efficiency, and improved the drug effect of Chinese medicine.
The specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.
Embodiment 1
The preparation disinfectant: be 20% water solublity triclocarban antibacterial with chlorhexidine acetate powder and working substance content by weight percentage according to weight ratio be that the ratio of 1:20 is composite, antibacterial is sterilized.
The mixture of preparation solubilizing agent and essence: with PEG-40 castor oil hydrogenated and PPG-26-butylol polyether-26 is that the mixed of 1:1 obtains solubilizing agent with the weight ratio, then solubilizing agent 2.2kg is mixed with oil-soluble toilet water essence 1.1kg, speed with 500 rev/mins stirs, and obtains the mixture of solubilizing agent and essence.
The preparation Chinese medicine extraction liquid:
Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis are obtained the Chinese medicine mixture according to the 1:1:0.5:0.5:0.1:0.1 mixed, and be that the ratio of 1:7 is soaked in the water according to weight ratio with Chinese medicine mixture and water, frequency of utilization is the ultrasound wave effect 30 minutes of 20KHz under 40-50 ℃ temperature afterwards, is concentrated to the 4kg extracting solution after the filtration and is equivalent to the 1kg crude drug and obtains Chinese medicine extraction liquid.
Disinfectant 0.3kg, the solubilizing agent of above-mentioned preparation are mixed with mixture, Chinese medicine extraction liquid 3.0kg, water-soluble lactic acid menthyl ester 1.2kg, the α-bisabolol 0.1kg of essence, and add deionized water to 100kg, stir, obtain no pure Chinese medicine floral water of the present invention.
Embodiment 2
The preparation disinfectant: be 20% water solublity triclocarban antibacterial with chlorhexidine acetate powder and working substance content by weight percentage according to weight ratio be that the ratio of 1:30 is composite, antibacterial is sterilized.
The mixture of preparation solubilizing agent and essence: with PEG-40 castor oil hydrogenated and PPG-26-butylol polyether-26 is that the mixed of 1:1.5 obtains solubilizing agent with the weight ratio, solubilizing agent 3.0kg is mixed with oil-soluble toilet water essence 2.8kg, speed with 400 rev/mins stirs, and obtains the mixture of solubilizing agent and essence.
Preparation Chinese medicine extraction liquid: Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis are obtained the Chinese medicine mixture according to the mixing of 1:1:0.5:0.5:0.1:0.1 ratio proportioning, and be that the ratio of 1:7 is soaked in the water according to weight ratio with Chinese medicine mixture and water, frequency of utilization is the ultrasound wave effect 30 minutes of 30KHz under 40-50 ℃ temperature afterwards, is concentrated to the 4kg extracting solution after the filtration and is equivalent to the 1kg crude drug and obtains Chinese medicine extraction liquid.
With the disinfectant of above-mentioned preparation is that 0.4kg, solubilizing agent mix with mixture, Chinese medicine extraction liquid 2.0kg, water-soluble lactic acid menthyl ester 0.8kg, the α-bisabolol 0.1kg of oil-soluble toilet water essence, and add deionized water to 100kg, stir, obtain no pure Chinese medicine floral water of the present invention.
Embodiment 3
The preparation disinfectant: be 20% water solublity triclocarban antibacterial with chlorhexidine acetate powder and working substance content by weight percentage according to weight ratio be that the ratio of 1:25 is composite, antibacterial is sterilized.
The mixture of preparation solubilizing agent and essence: with PEG-40 castor oil hydrogenated and PPG-26-butylol polyether-26 is that the mixed of 1:1.2 obtains solubilizing agent with the weight ratio, then solubilizing agent 3.0kg, oil-soluble toilet water essence 2.0kg are mixed, speed with 400 rev/mins stirs, and obtains the mixture of solubilizing agent and essence.
Preparation Chinese medicine extraction liquid: with Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis, obtain the Chinese medicine mixture according to the 1:1:0.5:0.5:0.1:0.1 mixed, and be that the ratio of 1:7 is soaked in the water according to weight ratio with Chinese medicine mixture and water, frequency of utilization is the ultrasound wave effect 20 minutes of 20KHz under 40-50 ℃ temperature afterwards, is concentrated to the 4kg extracting solution after the filtration and is equivalent to the 1kg crude drug and obtains Chinese medicine extraction liquid.
Disinfectant 0.6kg, the solubilizing agent of above-mentioned preparation are mixed with mixture, Chinese medicine extraction liquid 1.0kg, water-soluble lactic acid menthyl ester 0.8kg, the α-bisabolol 0.1kg of oil-soluble toilet water essence, and add deionized water to 100kg, stir, obtain no pure Chinese medicine floral water of the present invention.
Embodiment 4
The preparation disinfectant: be 20% water solublity triclocarban antibacterial with chlorhexidine acetate powder and working substance content by weight percentage according to weight ratio be that the ratio of 1:28 is composite, antibacterial is sterilized.
The mixture of preparation solubilizing agent and essence: with PEG-40 castor oil hydrogenated and PPG-26-butylol polyether-26 is that the mixed of 1:1.5 obtains solubilizing agent with the weight ratio, then solubilizing agent 3.6kg, oil-soluble toilet water essence 2.2kg are mixed, speed with 400 rev/mins stirs, and obtains the mixture of solubilizing agent and essence.
Preparation Chinese medicine extraction liquid: Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis are obtained the Chinese medicine mixture according to the mixing of 1:1:0.5:0.5:0.1:0.1 ratio proportioning, and be that the ratio of 1:7 is soaked in the water according to weight ratio with Chinese medicine mixture and water, frequency of utilization is 25KHz ultrasound wave effect 20 minutes under 40-50 ℃ temperature afterwards, is concentrated to the 4kg extracting solution after the filtration and is equivalent to the 1kg crude drug and obtains Chinese medicine extraction liquid.
Disinfectant 1.0kg, the solubilizing agent of above-mentioned preparation are mixed with mixture, Chinese medicine extraction liquid 5.0kg, water-soluble lactic acid menthyl ester 1.2kg, the α-bisabolol 0.1kg of oil-soluble toilet water essence, and add deionized water to 100kg, stir, obtain no pure Chinese medicine floral water of the present invention.
No pure Chinese medicine floral water of the present invention detects by national floral water standard (QB/T1858.1), and its outward appearance, index such as cold-resistant, heat-resisting are all up to specification, have good stability.
No pure Chinese medicine floral water of the present invention experimentizes according to " 2002 disinfection technology standard " sterilization method of Ministry of Public Health promulgation, and the result is as shown in table 1.As known from Table 1, the bactericidal property of the disinfectant that is contained among the present invention is good.
Table 1
| Sequence number | The concentration % of disinfectant | The effect microorganism | Action time min | Killing rate % |
| 1 | 0.25％ | Staphylococcus aureus ATCC6538 | 3 | ≥99.999 |
| 2 | 0.25％ | Escherichia coli 8099 | 3 | ≥99.999 |
| 3 | 0.65％ | Candida albicans ATCC10231 | 3 | ≥99.99 |
Claims (4)
1, a kind of no pure Chinese medicine floral water is characterized in that, comprises following component in the described floral water by weight percentage: disinfectant 0.3-1%, oil-soluble toilet water essence 1～3%, the solubilizing agent of 1-2 times of oil-soluble toilet water essence weight, Chinese medicine extraction liquid 1～5%, balance of deionized water; Described disinfectant is 20% composite the forming of water solublity triclocarban by chlorhexidine acetate and working substance content by weight percentage, and described chlorhexidine acetate and working substance content by weight percentage are that the weight ratio of 20% water solublity triclocarban is 1:20-30; Described solubilizing agent is that PEG-40 castor oil hydrogenated and PPG-26-butylol polyether-26 are the mixture of the mixed of 1:1-1.5 according to weight ratio; Described Chinese medicine extraction liquid is that mixture with Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis is as Chinese medicine ingredients, with the extracting solution of water as solvent, wherein, the weight ratio of Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis is 1:1:0.5:0.5:0.1:0.1, and the 4kg Chinese medicine extraction liquid is equivalent to the 1kg crude drug.
2, no pure Chinese medicine floral water according to claim 1, it is characterized in that described Chinese medicine extraction liquid is the extracting solution that adopts ultrasonic extraction to obtain as Chinese medicine ingredients, with water as solvent with the mixture of Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis.
3, the production method of the described no pure Chinese medicine floral water of a kind of claim 1 is characterized in that, comprises the steps:
(1) get the raw materials ready:
The preparation disinfectant: be that 20% water solublity triclocarban is composite by weight the ratio for 1:20-30 with chlorhexidine acetate and working substance content by weight percentage, antibacterial is sterilized;
With solubilizing agent and essence mixing for standby use: with PEG-40 castor oil hydrogenated and PPG-26-butylol polyether-26 is that the mixed of 1:1-1.5 obtains solubilizing agent with the weight ratio, be the mixed of 1:0.5-1 by weight with solubilizing agent and oil-soluble toilet water essence then, speed with 400-500 rev/min stirs, obtain the mixture of solubilizing agent and essence, standby;
The preparation Chinese medicine extraction liquid:
Flos Lonicerae, Flos Chrysanthemi Indici, Herba Pogostemonis, Radix Glycyrrhizae, Radix Et Rhizoma Rhei, Fel Serpentis are obtained the Chinese medicine mixture for the mixed of 1:1:0.5:0.5:0.1:0.1 by weight, above-mentioned Chinese medicine mixture is soaked in the water, place ultrasound wave Chinese medicine extractor, under 40-50 ℃ temperature, use ultrasound wave effect 20-30 minute of 20-30KHz, be concentrated to the 4kg extracting solution after the filtration and be equivalent to the 1kg crude drug and obtain Chinese medicine extraction liquid;
(2) mixture, Chinese medicine extraction liquid and the deionized water with the above-mentioned disinfectant that obtains, solubilizing agent and essence fully stirs, mix homogeneously, obtain no pure Chinese medicine floral water of the present invention, wherein, percentage by weight disinfectant according to the total amount that accounts for no pure Chinese medicine floral water is 0.3-1%, and the oil-soluble toilet water essence is 1～3%, the solubilizing agent of 1-2 times of oil-soluble toilet water essence weight, Chinese medicine extraction liquid is 1～5%, balance of deionized water.
4, the production method of no pure Chinese medicine floral water according to claim 3 is characterized in that, Chinese medicine mixture in the step (1) and water are the ratio immersion of 1:7 according to weight ratio.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102366389A (en) * | 2011-11-01 | 2012-03-07 | 重庆泰尔森制药有限公司 | Preparation method for compound mosquito repelling and itching relieving floral water |
| CN103238638A (en) * | 2013-05-10 | 2013-08-14 | 路维玲 | Preparation method of disinfectant |
| CN103735464A (en) * | 2014-01-15 | 2014-04-23 | 张一文 | Floral water for preventing mosquito bite |
| CN106466278A (en) * | 2015-08-20 | 2017-03-01 | 金玛瑙香水（明光）有限公司 | A kind of Flos micheliae Albae refreshment perfume |
| CN108685774A (en) * | 2018-07-09 | 2018-10-23 | 福建省海乐威生物工程有限公司 | A kind of mosquito-repellent water of the jasmin containing thermal water |
| WO2020042095A1 (en) * | 2018-08-30 | 2020-03-05 | 江苏奇力康皮肤药业有限公司 | Alcohol-free bacteriostatic florida water and preparation method therefor |
| CN111388338A (en) * | 2020-03-20 | 2020-07-10 | 广州乐宠宠物用品有限公司 | Pet perfume with lasting fragrance retaining effect and preparation method thereof |
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| CN114533928A (en) * | 2021-12-30 | 2022-05-27 | 上海芬尚生物科技有限公司 | Formula of oily essence dissolved in water-based fragrance product and preparation method thereof |
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2009
- 2009-01-06 CN CN2009100676282A patent/CN101461771B/en active Active
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102366389A (en) * | 2011-11-01 | 2012-03-07 | 重庆泰尔森制药有限公司 | Preparation method for compound mosquito repelling and itching relieving floral water |
| CN102366389B (en) * | 2011-11-01 | 2013-03-20 | 重庆泰尔森制药有限公司 | Preparation method for compound mosquito repelling and itching relieving floral water |
| CN103238638A (en) * | 2013-05-10 | 2013-08-14 | 路维玲 | Preparation method of disinfectant |
| CN103735464A (en) * | 2014-01-15 | 2014-04-23 | 张一文 | Floral water for preventing mosquito bite |
| CN106466278A (en) * | 2015-08-20 | 2017-03-01 | 金玛瑙香水（明光）有限公司 | A kind of Flos micheliae Albae refreshment perfume |
| CN108685774A (en) * | 2018-07-09 | 2018-10-23 | 福建省海乐威生物工程有限公司 | A kind of mosquito-repellent water of the jasmin containing thermal water |
| WO2020042095A1 (en) * | 2018-08-30 | 2020-03-05 | 江苏奇力康皮肤药业有限公司 | Alcohol-free bacteriostatic florida water and preparation method therefor |
| CN113039259A (en) * | 2018-11-09 | 2021-06-25 | 株式会社资生堂 | Transparent liquid composition |
| CN113039259B (en) * | 2018-11-09 | 2024-04-26 | 株式会社资生堂 | Transparent liquid composition |
| CN111388338A (en) * | 2020-03-20 | 2020-07-10 | 广州乐宠宠物用品有限公司 | Pet perfume with lasting fragrance retaining effect and preparation method thereof |
| CN114533928A (en) * | 2021-12-30 | 2022-05-27 | 上海芬尚生物科技有限公司 | Formula of oily essence dissolved in water-based fragrance product and preparation method thereof |
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