CN101448408B - 一步喷雾干燥法 - Google Patents

一步喷雾干燥法 Download PDF

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Publication number
CN101448408B
CN101448408B CN2007800180977A CN200780018097A CN101448408B CN 101448408 B CN101448408 B CN 101448408B CN 2007800180977 A CN2007800180977 A CN 2007800180977A CN 200780018097 A CN200780018097 A CN 200780018097A CN 101448408 B CN101448408 B CN 101448408B
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China
Prior art keywords
capsules
feed
spray
starch
powdering agent
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CN2007800180977A
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English (en)
Chinese (zh)
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CN101448408A (zh
Inventor
吉尔·特洛法尔迪
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Firmenich SA
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Firmenich SA
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/70—Fixation, conservation, or encapsulation of flavouring agents
    • A23L27/72—Encapsulation
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00—Shaping or working of foodstuffs characterised by the products
    • A23P10/30—Encapsulation of particles, e.g. foodstuff additives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
    • A61K9/1605—Excipients; Inactive ingredients
    • A61K9/1629—Organic macromolecular compounds
    • A61K9/1652—Polysaccharides, e.g. alginate, cellulose derivatives; Cyclodextrin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
    • A61K9/1682—Processes
    • A61K9/1694—Processes resulting in granules or microspheres of the matrix type containing more than 5% of excipient
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00—Formulations or additives for perfume preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
    • B01J13/043—Drying and spraying
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns

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  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Organic Chemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Epidemiology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medicinal Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Food Science & Technology (AREA)
  • Nutrition Science (AREA)
  • Dermatology (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • General Preparation And Processing Of Foods (AREA)
  • Medicinal Preparation (AREA)
  • Cosmetics (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Seasonings (AREA)
  • Glanulating (AREA)
CN2007800180977A 2006-05-19 2007-05-03 一步喷雾干燥法 Active CN101448408B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IB2006051606 2006-05-19
WOPCT/IB2006/051606 2006-05-19
PCT/IB2007/051655 WO2007135583A2 (en) 2006-05-19 2007-05-03 One step spray-drying process

Publications (2)

Publication Number Publication Date
CN101448408A CN101448408A (zh) 2009-06-03
CN101448408B true CN101448408B (zh) 2013-02-13

Family

ID=38565524

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2007800180977A Active CN101448408B (zh) 2006-05-19 2007-05-03 一步喷雾干燥法

Country Status (6)

Country Link
US (1) US20090252789A1 (enExample)
EP (1) EP2026664B1 (enExample)
JP (1) JP5254216B2 (enExample)
CN (1) CN101448408B (enExample)
BR (1) BRPI0711486B8 (enExample)
WO (1) WO2007135583A2 (enExample)

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WO2009012131A2 (en) * 2007-07-13 2009-01-22 Wm. Wrigley Jr. Company Flavor bead compositions
US20170137703A1 (en) 2007-12-11 2017-05-18 Superior Silica Sands, LLC Hydraulic fracture composition and method
US9856415B1 (en) * 2007-12-11 2018-01-02 Superior Silica Sands, LLC Hydraulic fracture composition and method
US10920494B2 (en) 2007-12-11 2021-02-16 Aquasmart Enterprises, Llc Hydraulic fracture composition and method
US9057014B2 (en) 2007-12-11 2015-06-16 Aquasmart Enterprises, Llc Hydraulic fracture composition and method
EP2100521A1 (en) * 2008-02-06 2009-09-16 Fortitech Europe ApS Use of a pulverulent composition to prepare a power or a food product
WO2010015580A1 (en) * 2008-08-04 2010-02-11 Dsm Ip Assets B.V. Production of beadlets comprising probiotic compounds
US20120196007A1 (en) * 2009-10-14 2012-08-02 Firmenich Sa Solid capsules comprising ethanol, a carbohydrate, a salt and a coating provided by a powdering agent, process for preparing said capsules by spray-drying
CN102883798B (zh) * 2010-03-22 2016-02-24 英斯迪罗有限公司 用于制备微粒和纳米粒的方法和设备
WO2011121515A1 (en) * 2010-03-29 2011-10-06 Firmenich Sa Spray-dried crystalline active ingredient
US9993793B2 (en) 2010-04-28 2018-06-12 The Procter & Gamble Company Delivery particles
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US8939388B1 (en) 2010-09-27 2015-01-27 ZoomEssence, Inc. Methods and apparatus for low heat spray drying
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WO2012138696A2 (en) 2011-04-07 2012-10-11 The Procter & Gamble Company Shampoo compositions with increased deposition of polyacrylate microcapsules
WO2012138710A2 (en) 2011-04-07 2012-10-11 The Procter & Gamble Company Personal cleansing compositions with increased deposition of polyacrylate microcapsules
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EP2768582B1 (en) 2011-10-21 2018-12-12 Firmenich SA Granules comprising an active substance
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EP2638811A1 (en) * 2012-03-15 2013-09-18 N.V. Nutricia Process for preparing infant formula
WO2014047496A2 (en) * 2012-09-20 2014-03-27 The Procter & Gamble Company Spray drying microcapsules
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US9993787B1 (en) 2017-08-04 2018-06-12 ZoomEssence, Inc. Ultrahigh efficiency spray drying apparatus and process
AU2018312095B2 (en) 2017-08-04 2021-10-28 ZoomEssence, Inc. Ultrahigh efficiency spray drying apparatus and process
US10486173B2 (en) 2017-08-04 2019-11-26 ZoomEssence, Inc. Ultrahigh efficiency spray drying apparatus and process
US9861945B1 (en) 2017-08-04 2018-01-09 ZoomEssence, Inc. Ultrahigh efficiency spray drying apparatus and process
WO2019115666A1 (en) 2017-12-14 2019-06-20 Firmenich Sa Process for releasing an active ingredient
US11260001B2 (en) 2017-12-14 2022-03-01 Firmenich Sa Process for preparing a powdered composition
CN111526729A (zh) 2018-02-23 2020-08-11 弗门尼舍有限公司 贮存稳定的粉末状组合物
WO2019173062A1 (en) 2018-03-07 2019-09-12 Trucapsol, Llc Reduced permeability microcapsules
US11344502B1 (en) 2018-03-29 2022-05-31 Trucapsol Llc Vitamin delivery particle
US10569244B2 (en) 2018-04-28 2020-02-25 ZoomEssence, Inc. Low temperature spray drying of carrier-free compositions
US11794161B1 (en) 2018-11-21 2023-10-24 Trucapsol, Llc Reduced permeability microcapsules
US11571674B1 (en) 2019-03-28 2023-02-07 Trucapsol Llc Environmentally biodegradable microcapsules
US11542392B1 (en) 2019-04-18 2023-01-03 Trucapsol Llc Multifunctional particle additive for enhancement of toughness and degradation in biodegradable polymers
EP3735840A1 (en) 2019-05-07 2020-11-11 DNA Catcher, S.L. Process for preparing high density, thermostable polysaccharide beads as food additives
KR102088136B1 (ko) * 2019-08-21 2020-03-11 구태훈 단미약재 또는 복합약재 추출물을 고농도로 포함하는 펠렛 제제 및 이의 제조방법
EP3945838A1 (en) 2019-11-29 2022-02-09 Firmenich SA Powdered composition comprising a solid plant-based fat
US11484857B2 (en) 2020-01-30 2022-11-01 Trucapsol Llc Environmentally biodegradable microcapsules
WO2021156892A1 (en) * 2020-02-04 2021-08-12 Fine Organic Industries Limited A polymer additive powder composition
EP4106552A1 (en) 2020-02-18 2022-12-28 Firmenich SA Flavored particles delivery system
BR112022013385A2 (pt) 2020-02-20 2022-09-13 Firmenich & Cie Composição em pó
JP2023527890A (ja) * 2020-06-02 2023-06-30 フイルメニツヒ ソシエテ アノニム フレーバー粒子
JP2022064439A (ja) * 2020-10-14 2022-04-26 株式会社アルバック 凍結乾燥装置
MX2023004232A (es) 2020-10-16 2023-04-21 Procter & Gamble Composiciones de productos de consumo con al menos dos poblaciones de encapsulados.
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CN120152625A (zh) * 2022-11-09 2025-06-13 西姆莱斯有限公司 用于碳酸饮料的香味组合物
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US5607708A (en) * 1992-12-14 1997-03-04 Hunt-Wesson, Inc. Encapsulated volatile flavoring materials
FR2758055A1 (fr) * 1997-01-06 1998-07-10 Sea Oil Poudre formee de microcapsules a base d'huile de poisson riche en acides gras polyinsatures
CN1194827A (zh) * 1997-02-28 1998-10-07 弗·哈夫曼-拉罗切有限公司 自由流动的干燥颗粒
US6482433B1 (en) * 1999-06-30 2002-11-19 Givaudan Sa Encapsulation of active ingredients
CN1735350A (zh) * 2003-01-10 2006-02-15 帝斯曼知识产权资产管理有限公司 制造脂溶性物质的粉状制剂的方法

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US4634598A (en) * 1978-08-07 1987-01-06 Nestec S. A. Flavorant capsules
US5607708A (en) * 1992-12-14 1997-03-04 Hunt-Wesson, Inc. Encapsulated volatile flavoring materials
FR2758055A1 (fr) * 1997-01-06 1998-07-10 Sea Oil Poudre formee de microcapsules a base d'huile de poisson riche en acides gras polyinsatures
CN1194827A (zh) * 1997-02-28 1998-10-07 弗·哈夫曼-拉罗切有限公司 自由流动的干燥颗粒
US6482433B1 (en) * 1999-06-30 2002-11-19 Givaudan Sa Encapsulation of active ingredients
CN1735350A (zh) * 2003-01-10 2006-02-15 帝斯曼知识产权资产管理有限公司 制造脂溶性物质的粉状制剂的方法

Also Published As

Publication number Publication date
US20090252789A1 (en) 2009-10-08
CN101448408A (zh) 2009-06-03
BRPI0711486B1 (pt) 2020-09-24
EP2026664B1 (en) 2014-09-10
WO2007135583A2 (en) 2007-11-29
EP2026664A2 (en) 2009-02-25
JP2009537322A (ja) 2009-10-29
BRPI0711486B8 (pt) 2021-05-25
BRPI0711486A2 (pt) 2012-02-14
JP5254216B2 (ja) 2013-08-07
WO2007135583A3 (en) 2008-01-24

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