CN101406504B - 菊米中黄酮类物质的提取方法 - Google Patents
菊米中黄酮类物质的提取方法 Download PDFInfo
- Publication number
- CN101406504B CN101406504B CN2008101624238A CN200810162423A CN101406504B CN 101406504 B CN101406504 B CN 101406504B CN 2008101624238 A CN2008101624238 A CN 2008101624238A CN 200810162423 A CN200810162423 A CN 200810162423A CN 101406504 B CN101406504 B CN 101406504B
- Authority
- CN
- China
- Prior art keywords
- cellulase
- chrysanthemum indicum
- buffer
- flavonoid substances
- suspension
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 239000000126 substance Substances 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 title claims abstract description 24
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 title description 4
- 229930003944 flavone Natural products 0.000 title description 4
- 235000011949 flavones Nutrition 0.000 title description 4
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 title description 4
- 150000002212 flavone derivatives Chemical class 0.000 title description 2
- 229930003935 flavonoid Natural products 0.000 claims abstract description 26
- 150000002215 flavonoids Chemical class 0.000 claims abstract description 26
- 235000017173 flavonoids Nutrition 0.000 claims abstract description 26
- 108010059892 Cellulase Proteins 0.000 claims abstract description 25
- 229940106157 cellulase Drugs 0.000 claims abstract description 25
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000000725 suspension Substances 0.000 claims abstract description 17
- 239000006228 supernatant Substances 0.000 claims abstract description 12
- 230000000694 effects Effects 0.000 claims abstract description 10
- 238000009210 therapy by ultrasound Methods 0.000 claims abstract description 6
- 239000007853 buffer solution Substances 0.000 claims abstract description 4
- 240000005250 Chrysanthemum indicum Species 0.000 claims description 28
- 235000018959 Chrysanthemum indicum Nutrition 0.000 claims description 28
- 239000000872 buffer Substances 0.000 claims description 10
- 235000013305 food Nutrition 0.000 claims description 7
- 108090000790 Enzymes Proteins 0.000 claims description 6
- 102000004190 Enzymes Human genes 0.000 claims description 6
- 229940088598 enzyme Drugs 0.000 claims description 6
- 229960004756 ethanol Drugs 0.000 claims description 6
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- 239000007974 sodium acetate buffer Substances 0.000 claims description 4
- BHZOKUMUHVTPBX-UHFFFAOYSA-M sodium acetic acid acetate Chemical compound [Na+].CC(O)=O.CC([O-])=O BHZOKUMUHVTPBX-UHFFFAOYSA-M 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 230000007935 neutral effect Effects 0.000 claims description 3
- CSVGEMRSDNSWRF-UHFFFAOYSA-L disodium;dihydrogen phosphate Chemical group [Na+].[Na+].OP(O)([O-])=O.OP(O)([O-])=O CSVGEMRSDNSWRF-UHFFFAOYSA-L 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000000605 extraction Methods 0.000 abstract description 11
- 238000001914 filtration Methods 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 8
- 238000005516 engineering process Methods 0.000 description 5
- 210000002421 cell wall Anatomy 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 238000002604 ultrasonography Methods 0.000 description 3
- 238000001291 vacuum drying Methods 0.000 description 3
- 206010020772 Hypertension Diseases 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- -1 flavone compound Chemical class 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 206010002383 Angina Pectoris Diseases 0.000 description 1
- 241000050051 Chelone glabra Species 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 241000723353 Chrysanthemum Species 0.000 description 1
- 241000201295 Euphrasia Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 208000019695 Migraine disease Diseases 0.000 description 1
- 208000005392 Spasm Diseases 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 208000029078 coronary artery disease Diseases 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 206010027599 migraine Diseases 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000008363 phosphate buffer Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
- 239000001509 sodium citrate Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2008101624238A CN101406504B (zh) | 2008-11-24 | 2008-11-24 | 菊米中黄酮类物质的提取方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2008101624238A CN101406504B (zh) | 2008-11-24 | 2008-11-24 | 菊米中黄酮类物质的提取方法 |
Publications (2)
Publication Number | Publication Date |
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CN101406504A CN101406504A (zh) | 2009-04-15 |
CN101406504B true CN101406504B (zh) | 2011-06-22 |
Family
ID=40569849
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN2008101624238A Active CN101406504B (zh) | 2008-11-24 | 2008-11-24 | 菊米中黄酮类物质的提取方法 |
Country Status (1)
Country | Link |
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CN (1) | CN101406504B (zh) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101993902A (zh) * | 2010-10-27 | 2011-03-30 | 漳州职业技术学院 | 一种芦笋及其下脚料中黄酮类化合物的提取方法 |
CN102191131A (zh) * | 2011-03-08 | 2011-09-21 | 浙江农林大学 | 菊米精油、菊米多糖、菊总黄酮提取物和菊米粉的系统制备方法 |
CN102246895B (zh) * | 2011-04-28 | 2014-04-16 | 浙江农林大学 | 一种白术花饲料添加剂及其制备和应用 |
CN102489038B (zh) * | 2011-11-29 | 2014-09-24 | 华东理工大学 | 表面活性剂协同超声波-酶解提取中草药中黄酮的方法 |
CN102631446B (zh) * | 2012-04-20 | 2013-11-06 | 浙江省中医院 | 一种葡萄柚皮黄酮类提取物及制备与应用 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101095711A (zh) * | 2006-06-29 | 2008-01-02 | 上海祥鹤药业有限公司 | 一种菊米提取物的提取及其制剂的制备方法 |
-
2008
- 2008-11-24 CN CN2008101624238A patent/CN101406504B/zh active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101095711A (zh) * | 2006-06-29 | 2008-01-02 | 上海祥鹤药业有限公司 | 一种菊米提取物的提取及其制剂的制备方法 |
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Publication number | Publication date |
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CN101406504A (zh) | 2009-04-15 |
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C06 | Publication | ||
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C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: PROYA COSMETICS CO., LTD. Free format text: FORMER OWNER: ZHEJIANG UNIVERSITY Effective date: 20130105 |
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C41 | Transfer of patent application or patent right or utility model | ||
COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 310027 HANGZHOU, ZHEJIANG PROVINCE TO: 310012 HANGZHOU, ZHEJIANG PROVINCE |
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TR01 | Transfer of patent right |
Effective date of registration: 20130105 Address after: 1605, room 1, building D, Europe and America Center, Xihu District World Trade Center, Hangzhou, Zhejiang, 310012, China Patentee after: Proya Cosmetics Co., Ltd. Address before: 310027 Hangzhou, Zhejiang Province, Xihu District, Zhejiang Road, No. 38, No. Patentee before: Zhejiang University |