CN101402137A - 采用真空熔铸法制备CuCr40触头材料的方法 - Google Patents

采用真空熔铸法制备CuCr40触头材料的方法 Download PDF

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CN101402137A
CN101402137A CNA2008102320348A CN200810232034A CN101402137A CN 101402137 A CN101402137 A CN 101402137A CN A2008102320348 A CNA2008102320348 A CN A2008102320348A CN 200810232034 A CN200810232034 A CN 200810232034A CN 101402137 A CN101402137 A CN 101402137A
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cucr40
powder
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contact material
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CN101402137B (zh
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王文斌
王小军
师晓云
张红军
李刚
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Shaanxi Sirui Advanced Materials Co Ltd
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Abstract

本发明公开的采用真空熔铸法制备CuCr40电触头,属于金属材料制备技术领域。按重量百分比其组成为:40%的Cr,其余为Cu。通过以下方法制备得到:将Cr块在低温液体保护下,通过研磨破碎机加工制成Cr粉,将Cr粉经压制后烧结成Cr粉坯,然后将Cu块与Cr粉坯放入真空炉中加热,熔化后进行浇铸,冷却后即制得CuCr40电触头材料。本发明的优点在于:将Cr块破碎成Cr粉,再经压制、烧结制成Cr粉坯,降低了熔化温度,缩短了熔化时间。本发明的制备方法,工艺简单、成本低,制得的CuCr40复合材料与熔渗的CuCr40复合材料相比具有更优越的性能。

Description

采用真空熔铸法制备CuCr40触头材料的方法
技术领域
本发明属于金属材料制备技术领域,具体涉及真空熔铸法制备CuCr 40电触头的方法。
背景技术
CuCr40主要用于12kv和40.5kv的真空灭弧室中。CuCr合金触头材料的制造工艺,国内外有四种制造工艺:(1)混粉压制烧结法;(2)真空熔渗法;(3)真空熔铸法;(4)真空电弧自耗法。这四种制造工艺中,混粉烧结的CuCr40材料中Cr颗粒与基体Cu的界面结合不良,韧性差。熔渗法制备的CuCr40颗粒度较大,耐电压强度不理想,开断容量已达到极限。真空电弧自耗法,能制造出较为理想的CuCr40触头材料,但它的成本高、工艺稳定性很难掌握。真空熔铸工艺具有诸多的优点和优势,但在此之前,真空熔铸法只能制造出CuCr25和CuCr30触头材料。熔铸CuCr40合金触头材料的试制是在熔铸CuCr25和熔铸CuCr30合金触头材料的基础上进行的。即将Cu、Cr两种组元放入到中频真空感应炉中,通过感应加热方法,在高温下将两种材料熔化,搅拌均匀,快速浇铸,并辅以快速冷却过程。实现快速形核并且抑制核长大,从而实现CuCr合金触头材料的Cr颗粒细化、均匀弥散分布。
发明内容
本发明的目的在于提供一种采用真空熔铸法制备CuCr40触头材料的方法。不仅细化了Cr颗粒,而且提高了触头材料的各项电性能指标。
本发明所提出的采用真空熔铸法制备CuCr40触头材料的方法,其特征在于:它包括以下步骤:
a.制粉
先将金属Cr在低温液体保护下,通过研磨破碎机加工制成Cr粉,制粉温度控制在-100℃以下
b.烧结
将制得的Cr粉经压制后进行烧结,烧结温度为1300~1400℃时间为1~3小时。
c.熔铸
将Cu块与烧结后的Cr粉坯一起装入真空炉中,真空度达到P≤8×10-2Pa时进行加热。升温速率为80℃/min左右,浇铸温度为1800~2000℃,快速浇铸。制得CuCr40电触头材料。
按以上工艺生产的CuCr40电触头材料,开断能力、耐电压强度、抗熔焊性能和机械强度得到了显著提高。
附图说明
附图1是本发明制备方法的流程图。
具体实施方式
下面结合附图和具体实施案例对本发明进行详细说明。
本发明的复合材料通过附图1所示的步骤来实现,包括以下步骤:
a.制粉
先将金属Cr在低温液体保护下,通过研磨破碎机加工制成Cr粉,制粉温度控制在-100℃以下
b.烧结
将制得的Cr粉经压制后进行烧结,烧结温度为1300~1400℃时间为1~3小时。
c.熔铸
将Cu块与烧结后的Cr粉坯一起装入真空炉中,真空度达到P≤8×10-2Pa时进行加热。升温速率为80℃/min,浇铸温度为1800~2000℃,快速浇铸。制得CuCr40电触头材料。
实施例1
称取Cr块2.24kg在低温液体保护下,通过研磨破碎机加工制成Cr粉,制粉温度控制在-100℃以下,将Cr粉经压制后,在1300℃烧结1小时制成Cr粉坯,然后称取Cu块3.36Kg与Cr粉坯放入真空炉中,在P≤8×10-2Pa的真空度下以80℃/min的速度进行加热,当温度上升到1800℃保温5min,快速浇铸。冷却后即制得CuCr40电触头材料。
实施例2
称取Cr块2.24kg在低温液体保护下,通过研磨破碎机加工制成Cr粉,制粉温度控制在-100℃,将Cr粉经压制后,在1350℃烧结2小时制成Cr粉坯,然后称取Cu块3.36kg,与Cr粉坯放入真空炉中,在P≤8×10-2Pa的真空度下以80℃/min的速度进行加热,当温度上升到1900℃保温5min,快速浇铸。冷却后即制得CuCr40电触头材料。
实施例3
称取Cr块2.24kg在低温液体保护下,通过研磨破碎机加工制成Cr粉,制粉温度控制在-100℃,将Cr粉经压制后,在1400℃烧结3小时制成Cr粉坯,然后称取Cu块3.36kg,与Cr粉坯放入真空炉中,在P≤8×10-2Pa的真空度下以80℃/min的速度进行加热,当温度上升到2000℃保温5min,快速浇铸。冷却后即制得CuCr40电触头材料。
本发明所制备的复合材料具有优良的综合性能。所制备的CuCr40复合材料与熔渗法CuCr40复合材料的性能对比见表1所示。
表1CuCr40复合材料的性能对比
Figure A20081023203400061

Claims (4)

1.一种采用熔铸法制备CuCr40电触头的方法,其特征在于,该方法按以下步骤进行:
a.制粉
先将金属Cr在低温液体保护下,通过研磨破碎机加工制成Cr粉,制粉温度控制在-100℃以下;
b.烧结
将制得的Cr粉经压制后进行烧结,烧结温度为1300~1400℃时间为1~3小时;
c.熔铸
将Cu块与Cr粉坯一起装入真空炉中,升温速率为80℃/min,浇铸温度为1800~2000℃,快速浇铸;制得CuCr40电触头材料。
2.按照权利要求1所述的制备方法,其特征在于,Cr的含量为40%。
3.按照权利要求1所述的制备方法,其特征在于,熔铸工艺是在真空条件下进行。
4.按照权利要求1所述的制备方法,其特征在于,所制备CuCr40电触头材料的各项电性能得到了提高。
CN2008102320348A 2008-10-30 2008-10-30 采用真空熔铸法制备CuCr 40触头材料的方法 Active CN101402137B (zh)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101786164A (zh) * 2010-03-05 2010-07-28 陕西斯瑞工业有限责任公司 采用CrMo合金粉制备CuCrMo触头材料的方法
CN102938337A (zh) * 2012-10-22 2013-02-20 西安建筑科技大学 一种梯度触头材料的生产工艺
CN104120245A (zh) * 2014-08-06 2014-10-29 陕西斯瑞工业有限责任公司 一种真空灭弧室用CuCr触头材料表面处理方法
CN110202159A (zh) * 2019-06-21 2019-09-06 西安斯瑞先进铜合金科技有限公司 一种高性能CuCr电触头专用金属铬粉的制备方法
CN116574937A (zh) * 2023-05-08 2023-08-11 江苏爱斯凯电气有限公司 一种用作真空开关的触头材料及其制备方法

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CN1186318A (zh) * 1996-12-27 1998-07-01 辽宁工学院 电渣熔铸生产铜铬合金真空开关触头材料的方法
CN1264143A (zh) * 2000-02-24 2000-08-23 周武平 真空开关铜铬系触头材料的制造方法
CN1260382C (zh) * 2002-04-10 2006-06-21 贵研铂业股份有限公司 铜基合金电真空触头材料及其制备方法
CN1489162A (zh) * 2002-10-08 2004-04-14 中国科学院金属研究所 一种真空开关用低偏析铜铬触头的制备方法
CN100497685C (zh) * 2007-06-08 2009-06-10 东北大学 自蔓延熔铸-电渣重熔制备CuCr合金触头材料的方法

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101786164A (zh) * 2010-03-05 2010-07-28 陕西斯瑞工业有限责任公司 采用CrMo合金粉制备CuCrMo触头材料的方法
CN102938337A (zh) * 2012-10-22 2013-02-20 西安建筑科技大学 一种梯度触头材料的生产工艺
CN102938337B (zh) * 2012-10-22 2015-06-10 西安建筑科技大学 一种梯度触头材料的生产工艺
CN104120245A (zh) * 2014-08-06 2014-10-29 陕西斯瑞工业有限责任公司 一种真空灭弧室用CuCr触头材料表面处理方法
CN110202159A (zh) * 2019-06-21 2019-09-06 西安斯瑞先进铜合金科技有限公司 一种高性能CuCr电触头专用金属铬粉的制备方法
CN116574937A (zh) * 2023-05-08 2023-08-11 江苏爱斯凯电气有限公司 一种用作真空开关的触头材料及其制备方法
CN116574937B (zh) * 2023-05-08 2023-10-03 江苏爱斯凯电气有限公司 一种用作真空开关的触头材料及其制备方法

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