CN101190957B - 一种制备交联聚合物的方法 - Google Patents
一种制备交联聚合物的方法 Download PDFInfo
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- CN101190957B CN101190957B CN2007101900731A CN200710190073A CN101190957B CN 101190957 B CN101190957 B CN 101190957B CN 2007101900731 A CN2007101900731 A CN 2007101900731A CN 200710190073 A CN200710190073 A CN 200710190073A CN 101190957 B CN101190957 B CN 101190957B
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- 239000008367 deionised water Substances 0.000 claims abstract description 52
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 52
- JKNCOURZONDCGV-UHFFFAOYSA-N 2-(dimethylamino)ethyl 2-methylprop-2-enoate Chemical compound CN(C)CCOC(=O)C(C)=C JKNCOURZONDCGV-UHFFFAOYSA-N 0.000 claims abstract description 26
- UKODFQOELJFMII-UHFFFAOYSA-N pentamethyldiethylenetriamine Chemical compound CN(C)CCN(C)CCN(C)C UKODFQOELJFMII-UHFFFAOYSA-N 0.000 claims abstract description 23
- 238000006116 polymerization reaction Methods 0.000 claims abstract description 3
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- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 6
- -1 tetrahydrofuran compound Chemical class 0.000 claims description 6
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- 239000000203 mixture Substances 0.000 claims description 4
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- QATBRNFTOCXULG-UHFFFAOYSA-N n'-[2-(methylamino)ethyl]ethane-1,2-diamine Chemical compound CNCCNCCN QATBRNFTOCXULG-UHFFFAOYSA-N 0.000 claims description 2
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- 229910021591 Copper(I) chloride Inorganic materials 0.000 description 15
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- 239000000463 material Substances 0.000 description 4
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- 239000005864 Sulphur Substances 0.000 description 2
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- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
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- 229920002246 poly[2-(dimethylamino)ethyl methacrylate] polymer Polymers 0.000 description 2
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- 229910021589 Copper(I) bromide Inorganic materials 0.000 description 1
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- 244000043261 Hevea brasiliensis Species 0.000 description 1
- VHOQXEIFYTTXJU-UHFFFAOYSA-N Isobutylene-isoprene copolymer Chemical group CC(C)=C.CC(=C)C=C VHOQXEIFYTTXJU-UHFFFAOYSA-N 0.000 description 1
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- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- YPHQUSNPXDGUHL-UHFFFAOYSA-N n-methylprop-2-enamide Chemical compound CNC(=O)C=C YPHQUSNPXDGUHL-UHFFFAOYSA-N 0.000 description 1
- XXQBGBUZLWZPKT-UHFFFAOYSA-N n-prop-2-enoylbuta-2,3-dienamide Chemical compound C=CC(=O)NC(=O)C=C=C XXQBGBUZLWZPKT-UHFFFAOYSA-N 0.000 description 1
- 229920003052 natural elastomer Polymers 0.000 description 1
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- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
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- 229920002223 polystyrene Polymers 0.000 description 1
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- 229920003987 resole Polymers 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- AGGKEGLBGGJEBZ-UHFFFAOYSA-N tetramethylenedisulfotetramine Chemical compound C1N(S2(=O)=O)CN3S(=O)(=O)N1CN2C3 AGGKEGLBGGJEBZ-UHFFFAOYSA-N 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
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CN2007101900731A CN101190957B (zh) | 2007-11-20 | 2007-11-20 | 一种制备交联聚合物的方法 |
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CN101190957B true CN101190957B (zh) | 2010-09-29 |
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Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101787095B (zh) * | 2010-03-12 | 2012-01-18 | 江苏工业学院 | 一种通过氧化聚合制备超支化聚合物的方法 |
CN101787093B (zh) * | 2010-03-12 | 2012-01-18 | 江苏工业学院 | 甲基丙烯酸二甲氨基乙酯的自引发原子转移自由基聚合方法 |
CN102295418B (zh) * | 2011-06-10 | 2013-06-19 | 常州大学 | 一种在玻璃表面接枝聚合物的方法 |
CN102690469B (zh) * | 2011-11-26 | 2014-07-16 | 河南科技大学 | 吸油树脂材料及其制备方法 |
CN109161045B (zh) * | 2018-08-30 | 2020-12-15 | 江南大学 | 一种温度、pH双重响应型智能高分子膜及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6541580B1 (en) * | 1995-03-31 | 2003-04-01 | Carnegie Mellon University | Atom or group transfer radical polymerization |
CN1806901A (zh) * | 2005-12-27 | 2006-07-26 | 天津工业大学 | 一种复合纳滤膜及其制备方法 |
CN1869081A (zh) * | 2005-05-23 | 2006-11-29 | 中国科学院化学研究所 | 自由基聚合一步合成星形聚合物的方法 |
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2007
- 2007-11-20 CN CN2007101900731A patent/CN101190957B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6541580B1 (en) * | 1995-03-31 | 2003-04-01 | Carnegie Mellon University | Atom or group transfer radical polymerization |
CN1869081A (zh) * | 2005-05-23 | 2006-11-29 | 中国科学院化学研究所 | 自由基聚合一步合成星形聚合物的方法 |
CN1806901A (zh) * | 2005-12-27 | 2006-07-26 | 天津工业大学 | 一种复合纳滤膜及其制备方法 |
Non-Patent Citations (4)
Title |
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SOLOMON M. KIMANI,ET AL.Ambient-Temperature Copper-Catalyzed Atom TransferRadical Polymerization of Methacrylates in Ethylene GlycolSolvents.Journal of Polymer Science Part A: Polymer Chemistry43 8.2005,43(8),1588-1598. |
SOLOMON M. KIMANI,ET AL.Ambient-Temperature Copper-Catalyzed Atom TransferRadical Polymerization of Methacrylates in Ethylene GlycolSolvents.Journal of Polymer Science Part A: Polymer Chemistry43 8.2005,43(8),1588-1598. * |
ZHENG FANG,ET AL.Novel Block Ionomers ii. Synthesis and Characterization ofPolyisobutylene-Based Block Cationomers.Journal of Polymer Science Part A: Polymer Chemistry40 21.2002,40(21),3679-3691. |
ZHENG FANG,ET AL.Novel Block Ionomers ii. Synthesis and Characterization ofPolyisobutylene-Based Block Cationomers.Journal of Polymer Science Part A: Polymer Chemistry40 21.2002,40(21),3679-3691. * |
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