CN101185616A - Face pack and preparation method thereof - Google Patents

Face pack and preparation method thereof Download PDF

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CN101185616A
CN101185616A CNA2006101146114A CN200610114611A CN101185616A CN 101185616 A CN101185616 A CN 101185616A CN A2006101146114 A CNA2006101146114 A CN A2006101146114A CN 200610114611 A CN200610114611 A CN 200610114611A CN 101185616 A CN101185616 A CN 101185616A
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extract
facial film
semen litchi
radix
semen
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程宇镳
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Abstract

The invention pertains to the field of household chemical products, which more particularly discloses a mask which is made by taking the extract of plants as the raw materials. The mask has the function of epiphyte and acarid killing, thus having good market prospect.

Description

A kind of facial film and preparation method thereof
[technical field]
The invention belongs to the cosmetics of everyday use technical field, be specifically related to a kind of facial film that contains Semen Litchi extract and preparation method thereof.
[background technology]
Semen Litchi is the mature seed of Sapindaceae aiphyllium plant Fructus Litchi (Litchi chinsis Sonn.).Main product in Fujian, ground such as Guangdong, Guangxi.Pluck mature fruit summer, remove peel and meat aril, clean, dry.Give birth to or saline process usefulness.Time spent smashes.Semen Litchi acrid in the mouth, little hardship, temperature.Return liver, stomach through being mainly used in colicky, painful and swollen testis.This product catharsis of working hard has the merit of depressed liver-energy dispersing and QI regulating, promoting QI to circulate and dispersing the agglomeration of the pathogens, dispersing cold for relieving pain.Semen Litchi is controlled colic of cold type pain, can be equal to usefulness with Fructus Foeniculi, Fructus Evodiae, Semen Citri Reticulatae, as the hernia internal diabetes ball of " Beijing's Chinese traditional patent formulation selected works ".Control painful and swollen testis, many and Semen Citri Reticulatae, Fructus Toosendan are equal to usefulness.Semen Litchi also can be used for gastral cavilty pain of a specified duration, dysmenorrhea, puerperal abdonimal pain.It is logical that the hot row of this product hardship is let out temperature, and dispersing the stagnated liver-QI for regulating the stomach, regulating QI to relieve pain effect are arranged.The gastral cavilty pain of a specified duration of Semen Litchi treating the liver stagnation of QI knot, incoordination between the liver and stomach can be ground clothes into powder with the Radix Aucklandiae, looses as the Jing-Yue Complete Works litchi is fragrant, the dysmenorrhea and the puerperal abdonimal pain of the strongly fragrant qi depression to blood stasis for the treatment of the liver, can grind clothes into powder with perfume (or spice) limit, diffusing bitterly as " married woman's good recipe " stannum, or be equal to usefulness with Rhizoma Chuanxiong, Radix Angelicae Sinensis, Radix Bupleuri.
Semen Litchi is Long Circle or oval, and is slightly flat, long 1.5~2.2cm, diameter 0.6~1.5cm.Surface brownish red or purple brown, glossy, slightly cave in and insertion waves.One end has the hilum of similar round or oval yellowish-brown, diameter 5~7mm.Matter is hard, cuts 2 of the visible plump cotyledons in back open with water infiltration, and orange-yellow or pale brown color is combined closely with kind of a skin.Feeble QI, it is little sweet, bitter, puckery to distinguish the flavor of.Big, full, bright person is good with grain.Its microscopical identification is: Semen Litchi (middle part) cross section: all plant the chrotoplast wall and be pale brown color.Plant the exocuticle cell extend radially of skin.About 10~15 row of parenchyma cell are arranged in it, and cell tangentially prolongs, the visible sparse Kong Wen that has.Brown oil cell similar round or Long Circle.The interrupted annular arrangement of vascular bundle.Decadent near the several layers of parenchyma cell of planting the skin epidermis, cell shrinkage, the gap is big.The endepidermis of planting skin is 1 row parenchyma cell, and is flat, different in size.Be full of starch grain in the parenchyma cell of cotyledon, and as seen have brown oil cell to be dispersed in.
Fungus-caused disease is divided into shallow and infects and deep infection.The shallow fungal infection in the world many areas very general, belong to propagated common frdquently encountered disease; Mainly cause, can invade the keratoprotein tissue of skin, hair follicle and fingernail, account for about 90% of fungal infection incidence rate by Epidermophyton, the mould Pseudomonas of little spore and trichophyton.Well-known have tinea capitis, tinea corporis, tinea cruris, tinea manus and pedis, tinea versicolor and a tinea unguium, and mining area operator and the crowd who lives in the warm environment have generation more, though easily ignored by people, also are the persistent ailments of making us very worried.
Acarid less than 0.5 millimeter, belongs to Acarina usually, and is distributed more widely, and kind is more, and more common have a gamasid, trombiculid, and the type of wriggling demodicid mite, the dirt demodicid mite, acaricide, flour mite etc., table 1 is listed in common acarid and hazardness thereof.As shown in Table 1, acarid can colonize in human body skin, lives in the object that contacts with the people, exists in dust and the grain, its hazardness is also very big, they not only self cause the human body skin disease, diseases such as allergic rhinitis and asthma to being destroyed by parasitic body (host), but also propagate other disease. along with urban industryization, environmental pollution, koniology increases, and causes the factor of disease more important by acarid. so the acaricide series products obtains consumers in general's approval and acceptance in recent years.
Table 1 acarid and feature thereof and hazardness
Figure A20061011461100041
Available in the market health acaricide raw material is few, and the use amount of the indivedual effectively raw materials of minority is but very high.Because raw material and technology limitation, many products are often just done a conception of species, do not add effective composition, do not reach the target of driving the acarid that goes out at all. therefore good raw material and technology seems extremely important for preventing and treating acarid.
American documentation literature US2004/0101508A1 discloses the purposes of extract aspect cosmetics and medicine of Fructus Litchi.Chinese patent literature (200410022559) provides Fructus Litchi extract and preparation method thereof, and this invention also provides the application of this Fructus Litchi extract in medicine, health food and cosmetics.But to the deep development of Semen Litchi extract, especially Semen Litchi extract does not have document to mention in the application of facial film, does not have product open yet.Zheng Linying etc. reported Semen Litchi have suppress hbs antigen, effect (Chinese medicine journal, 1998 (5): 51-53) such as blood sugar lowering, enhancing mouse liver albumen and RNA be synthetic; (Chinese Journal of New Drugs, 2000 (1): 14-16) reported that also Semen Litchi has blood lipid regulation and antioxidation such as Pan Jing clanging or clanking sound except above effect.
[summary of the invention]
The Semen Litchi that the objective of the invention is to annual about 500,000 tons is turned waste into wealth, and development and use are used to prepare facial film, and this facial film has fungus and and the effect of acarid killed.
Another object of the present invention is to provide the facial film preparation method.
Facial film of the present invention contains Semen Litchi extract.
Facial film of the present invention contains Semen Litchi extract and facial film adjuvant.
Above-mentioned facial film, the Semen Litchi extract weight ratio in facial film is 0.1-25%, preferred 0.1-20%, more preferably 1-10%, most preferably 1-5%.
Above-mentioned facial film can be used to kill fungus and and acarid.
The preparation method of above-mentioned Semen Litchi extract is: water and alcoholic acid mixed solvent extraction were 2-3 time after Semen Litchi was pulverized, and each 1-2 hour, concentrated after drying promptly got Semen Litchi extract, with the Semen Litchi extract irradiation sterilization after, the dressing that adds facial film, stirring and evenly mixing, packing is promptly.Wherein the water content of Semen Litchi extract is controlled at 2.5-3.5%.Above-mentioned facial film can also add Herba Leonuri extract, Radix Salviae Miltiorrhizae extract, Radix Angelicae Sinensis extract, Rhizoma Chuanxiong extract, Semen Tritici aestivi extract, Radix Polygoni Multiflori extract, Radix Ginseng extract, Margarita, Margarita micropowder, Rhizoma Atractylodis Macrocephalae extract, Fructus Lycii extract, Radix Saposhnikoviae extract, Radix Angelicae Dahuricae extract, Radix Astragali extract, Rhizoma Dioscoreae extract, Semen Cuscutae extract, Radix Rehmanniae extract, alfalfa extract, Sargassum extract liquid, Aloe extract, Radix Arnebiae extract, the XINGTAO extract, the arnica montana extract, Laurel extract extract, the Fructus Citri Sarcodactylis extract, the sprout of birch extract, the Fructus Arctii extract, Flos Inulae extract, Camellia extract, camomile extract, green algal extract, Radix Glycyrrhizae extract, Caulis Hederae Sinensis extract, Herba Euphrasiae Regelii extract, Radix Oenotherae erythrosepalae oil, Fructus Foeniculi extract, Rhizoma Zingiberis Recens extract, in Semen Ginkgo extrac and the root of Gentiana lutea root extract one or more.
Can adopt vacuum packaging during above-mentioned facial film packing, also can be above-mentioned charge in nitrogen, helium, the carbon dioxide one or more during the facial film packing.
Semen Litchi extract among the present invention also can adopt commercially available product (existing at present Semen Litchi extract is sold), can also obtain by other organic solvents or water extraction.
Because Guangdong and Guangxi Provinces, Fujian and Taiwan Fructus Litchi output are huge, many mountain areas, the Fructus Litchi place of production and hills, have inconvenient traffic, and Fructus Litchi requires very harsh to storage and traffic condition, often occur going mouldy owing to Fructus Litchi can not be caused by place of production outward transport in time, at this moment pulp and Fructus Litchi kind skin have not all had value, Semen Litchi can also add in the facial film by drying, sterilization and pulverizing back or processing extraction only, turn waste into wealth, produce bigger economic worth, also can increase farmers' income for the Fructus Litchi grower retrieves a loss.
China's Fructus Litchi output is huge, and Fructus Litchi output was about 1,500,000 tons in 2005, and resource is very abundant, because the difference of Fructus Litchi kind accounts for Fructus Litchi gross weight 1/3 with Semen Litchi and calculates, annual China just has 500,000 tons of Semen Litchi resources to develop.From the raw material as facial film, Semen Litchi has than the better advantage of Fructus Litchi, says that from content of effective difference of them is little, but because Fructus Litchi is in the fruit outside, contacts with air, and active component is oxidized easily; And Fructus Litchi is as a kind of fruit, by people edible after, peel is difficult to collect, the gross weight ratio that Fructus Litchi accounts for litchi fruits is little; And Semen Litchi weight is big, is easy to collect after eating; Directly Semen Litchi is taken out when also having businessman to produce canned litchi, be more convenient for the collection of Semen Litchi like this.
Fructus Litchi fires one's imagination owing to the well-known phrase of " rides the human society imperial concubine laughs at, and nobody knows Fructus Litchi " since ancient times, becomes a kind of and beautiful fruit of becoming attached to, and Semen Litchi really is used to beautify people's life but also have no talent at present, also is not used in the preparation facial film.
The present invention verifies by experiment, the performance of facial film among the present invention kill fungus and and the acarid effect be that various compositions comprehensively play a role in the Semen Litchi extract, rather than a certain or a certain compounds plays a role, therefore Semen Litchi extract has the incomparable effect of other facial film as a kind of raw material of cosmetics.In addition, Semen Litchi extract also has favorable compatibility, also can make facial film by compatibility with other plant or plant extract, also have kill fungus and and the effect of the effect of acarid, wherein the effect of Semen Litchi extract is indispensable.
[specific embodiment]
Following embodiment further describes the present invention, but described embodiment only is used to illustrate the present invention rather than restriction the present invention.
The preparation of embodiment 1-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 2.5 ascending of pulverizing the two weight ratio of back water and acetone and being 1: 2 are got 1-2 hour at every turn 2-3 time, the temperature of extracting is 55-65 ℃, concentrates the back under 70 ℃ of conditions, vacuum drying oven 6 hours, promptly get Semen Litchi extract, water content is 2.8%.
The preparation of embodiment 2-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and ethanol and being 1: 3 are got 2-3 time, and each 1-2 hour, under 80 ℃ of conditions, vacuum drying oven 5 hours promptly got Semen Litchi extract after concentrating, and water content is 2.9%.
The preparation of embodiment 3-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 2.5 ascending of pulverizing the two weight ratio of back water and acetone and being 1: 2 are got 2-3 time, and each 1-2 hour, concentrated, spray drying promptly got Semen Litchi extract, and water content is 3.1%.
The preparation of embodiment 4-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and acetone and being 1: 3 are got 1-2 hour at every turn 2-3 time, concentrate, after the spray drying under 75 ℃ of conditions, vacuum drying oven 5 hours promptly gets Semen Litchi extract, and water content is 3.0%.
The preparation of embodiment 5-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and ethyl acetate and being 1: 3 are got 1-2 hour at every turn 2-3 time, concentrate, after the spray drying under 50 ℃ of conditions, vacuum drying oven 8 hours promptly gets Semen Litchi extract, and water content is 2.5%.
The preparation of embodiment 6-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 2.5 ascending of pulverizing the two weight ratio of back water and acetone and being 1: 20 are got 2-3 time, and each 1-2 hour, concentrated, spray drying promptly got Semen Litchi extract, and water content is 3.5%.
Table 1-contains the preparation of Semen Litchi extract facial film
Figure A20061011461100071
Figure A20061011461100081
Semen Litchi extract and adjuvant in above each Example formulations are fully mixed, stir even matter emulsifying, curing molding, packing, promptly.
Experimental example 1-human safety (skin irritation) test
1 test objective
Detection is tried the probability that thing causes the human body skin untoward reaction, and the effect of being tried thing is carried out preliminary assessment.
2 test basic principles
2.1 select qualified volunteer object on probation.
2.2 according to the type and the character of cosmetics, allow the actual use of experimenter be subjected to test product, tried the safety (skin irritation) of thing to human body with evaluation.
3 experimenters' selection
3.1 select volunteer that the Pass Test of 18-60 year requires as study subject.
3.2 can not select following situation person as the experimenter: a nearly week uses antihistaminic or uses immunosuppressant person in nearly one month; Tried the position in nearly two months and used any anti-inflammatory drug person; The experimenter suffers from the sick clinical person of not healing of inflammatory skin; The insulin-dependent diabetes patient; The asthma of receiving treatment or other chronic respiratory system diseases patient; The person that in nearly 6 months, accepts the anticancer chemotherapy; Immunodeficiency or autoimmune disease patient; Age of sucking or gravid woman; Bilateral mastectomy and bilateral axillary lymph knot excision person; Wait to try the position influences result of the test owing to cicatrix, pigment, atrophy, nevus flammeus or other flaw judgement person at skin; Participate in other clinical trial person; The extremely sensitive person of body constitution; Non-aspiration participant maybe can not finish specified content person by test requirements document.
4 dermoreaction grade scales: see Table 1.
Table 1 human body proof test skin adverse reaction grade scale
Figure A20061011461100091
5 test methods
Press subject enrollment experimenter 50 examples (male's 25 examples, women's 25 examples), the time on probation is 1 month.On the skin that embodiment 7-16 was affixed in 3 days 0.5 * 0.5 centimetre of experimenter's forearm inboard respectively, labelling, be coated with same position at every turn.Observe 1 experimenter's dermoreaction every 1 day, press table 1 skin adverse reaction grade scale record result.
6 result safety evaluations:
Nothing 1 example has the skin adverse reaction more than 1 grade or 1 grade among the of the present invention 50 routine experimenters, judges that soap of the present invention has without any untoward reaction human body.
Experimental example 2-facial film is to antifungic action
1. the experimenter must select
Use group: choose caused hand skin the infected 18 examples of fungus, male's 10 examples wherein, women's 8 examples.
Blank group: choose caused skin infection person 9 examples of fungus, male's 3 examples wherein, women's 6 examples.
1. Therapeutic Method
Use group: after washing one's face, embodiment 10 is spread on face, throw off after 25 minutes, every day 2 times, adhered to using 14 days.
Blank group: after washing one's face, common facial film is spread on face, throw off after 25 minutes, every day 2 times, adhered to using 14 days.
3. therapeutic evaluation standard:
Adopt " TCM Dermatology disease diagnosis criterion of therapeutical effect ".Cure: skin lesion disappears fully, and wound surface heals fully, no longer includes new rash and occurs.Take a turn for the better: skin lesion heals more than 50%.Do not heal: skin lesion seemingly has new rash constantly to occur or healing skin lesion deficiency as before.
4. therapeutic outcome:
The present invention has the broad-spectrum antifungal effect, and deep fungal and part superficial fungi are had good killing and inhibitory action, and the present invention is used for the skin affected part, suppresses antibacterial, fungi growth and breeding, and antipruritic, anti-allergic effects is played on the cleaning skin surface simultaneously.Data see Table 1
The caused skin infection curative effect statistics of 11 pairs of funguses of table 1 embodiment
Figure A20061011461100092
5 conclusions
The present invention has the broad-spectrum antifungal effect, and deep fungal and part superficial fungi are had good killing and inhibitory action, and the present invention is used for the skin affected part, suppresses antibacterial, fungi growth and breeding, and antipruritic, anti-allergic effects is played on the cleaning skin surface simultaneously.
Experimental example 3-facial film is to the removal effect of acarid
Prepared facial film is on probation 48 University Female Students, and being divided into is 6 groups, every group 8 people, and promptly A group (blank group), B group (embodiment 9), C group (embodiment 10), D group (embodiment 13), E group (embodiment 15), F organize (common facial film).Ginseng survey personnel and experimenter do not know the kind (double-blind method) of employed facial film.
Experimental technique: before 6 groups of University Female Students are used, after rising morning, put on the skin gently one time at face, then wet paper towel is detected acarid quantity, record respectively under 100 power microscopes with wet paper towel.6 groups of University Female Students are used the corresponding facial film of each group, every day 3 times.Continue after 15 days, with wet paper towel at face gently put one time after rising the 16th day morning, then wet paper towel detected acarid quantity respectively under 100 power microscopes, is recorded in microscopically and detects acarid quantity, record, the situation that detects of observing acarid.Effect is divided into 4 grades: 1 grade: wet paper towel does not have acarid and detects, 2 grades: wet paper towel has 1 acarid to detect 3 grades: wet paper towel has 2 acarids to detect 4 grades: wet paper towel has 3 or 3 above acarids to detect.Concrete data see Table 3
Table 3 is respectively organized experimenter's acarid situation
Figure A20061011461100101
Above data declaration facial film of the present invention has remarkable result to removing acarid.

Claims (10)

1. a facial film is characterized in that described facial film contains Semen Litchi extract.
2. a facial film is characterized in that described facial film contains Semen Litchi extract and facial film adjuvant.
3. according to the arbitrary described facial film of claim 1-2, it is characterized in that the weight ratio of described Semen Litchi extract in facial film is 0.1-25%.
4. according to the described facial film of claim 3, it is characterized in that the weight ratio of described Semen Litchi extract in facial film is 0.1-20%.
5. according to the described facial film of claim 4, it is characterized in that the weight ratio of described Semen Litchi extract in facial film is 1-10%.
6. according to the described facial film of claim 5, it is characterized in that the weight ratio of described Semen Litchi extract in facial film is 1-5%.
7. according to the arbitrary described facial film of claim 3-6, it is characterized in that described facial film can also add Herba Leonuri extract, Radix Salviae Miltiorrhizae extract, Radix Angelicae Sinensis extract, Rhizoma Chuanxiong extract, Semen Tritici aestivi extract, Radix Polygoni Multiflori extract, Radix Ginseng extract, Margarita, Margarita micropowder, Rhizoma Atractylodis Macrocephalae extract, Fructus Lycii extract, Radix Saposhnikoviae extract, Radix Angelicae Dahuricae extract, Radix Astragali extract, Rhizoma Dioscoreae extract, Semen Cuscutae extract, Radix Rehmanniae extract, alfalfa extract, Sargassum extract liquid, Aloe extract, Radix Arnebiae extract, the XINGTAO extract, the arnica montana extract, Laurel extract extract, the Fructus Citri Sarcodactylis extract, the sprout of birch extract, the Fructus Arctii extract, Flos Inulae extract, Camellia extract, camomile extract, green algal extract, Radix Glycyrrhizae extract, Caulis Hederae Sinensis extract, Herba Euphrasiae Regelii extract, Radix Oenotherae erythrosepalae oil, Fructus Foeniculi extract, Rhizoma Zingiberis Recens extract, in Semen Ginkgo extrac and the root of Gentiana lutea root extract one or more.
8. the preparation method of the arbitrary described facial film of claim 1-7, it is characterized in that water and alcoholic acid mixed solvent extraction after Semen Litchi pulverizing 2-3 time, each 1-2 hour, concentrated after drying promptly gets Semen Litchi extract, with the Semen Litchi extract irradiation sterilization after, the dressing that adds facial film, stirring and evenly mixing, packing is promptly.
9. the preparation method of described facial film according to Claim 8 is characterized in that the water content of wherein said Semen Litchi extract is controlled at 2.5-3.5%.
10. according to the arbitrary described facial film of claim 3-6, it is characterized in that to be used to kill fungus and and acarid.
CNA2006101146114A 2006-11-17 2006-11-17 Face pack and preparation method thereof Pending CN101185616A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103142452A (en) * 2011-12-06 2013-06-12 李伟业 Medicinal liquor beauty mask and manufacturing method thereof
CN104248610A (en) * 2014-09-09 2014-12-31 秋实草业有限公司 Medicago-sativa anti-aging mask and preparation method
CN104983643A (en) * 2015-07-24 2015-10-21 哈尔滨商业大学 Blueberry residue sleep nourishing mask and preparation method thereof
CN108578314A (en) * 2018-05-28 2018-09-28 浙江艾卡医学科技有限公司 A kind of composition containing plant extracts and its application in except mite nursing product

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103142452A (en) * 2011-12-06 2013-06-12 李伟业 Medicinal liquor beauty mask and manufacturing method thereof
CN104248610A (en) * 2014-09-09 2014-12-31 秋实草业有限公司 Medicago-sativa anti-aging mask and preparation method
CN104983643A (en) * 2015-07-24 2015-10-21 哈尔滨商业大学 Blueberry residue sleep nourishing mask and preparation method thereof
CN108578314A (en) * 2018-05-28 2018-09-28 浙江艾卡医学科技有限公司 A kind of composition containing plant extracts and its application in except mite nursing product

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