CN101180112B - 弱挥发性流体的蒸馏提纯方法 - Google Patents

弱挥发性流体的蒸馏提纯方法 Download PDF

Info

Publication number
CN101180112B
CN101180112B CN2006800178366A CN200680017836A CN101180112B CN 101180112 B CN101180112 B CN 101180112B CN 2006800178366 A CN2006800178366 A CN 2006800178366A CN 200680017836 A CN200680017836 A CN 200680017836A CN 101180112 B CN101180112 B CN 101180112B
Authority
CN
China
Prior art keywords
auxiliary agent
ethyl
methyl
volatile fluid
butyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2006800178366A
Other languages
English (en)
Chinese (zh)
Other versions
CN101180112A (zh
Inventor
G·鲁弗特
O·普福尔
M·格伦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer Technology Services GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Technology Services GmbH filed Critical Bayer Technology Services GmbH
Publication of CN101180112A publication Critical patent/CN101180112A/zh
Application granted granted Critical
Publication of CN101180112B publication Critical patent/CN101180112B/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/56—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/146—Multiple effect distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C07C7/05—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds
    • C07C7/08—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds by extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/54—Quaternary phosphonium compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
CN2006800178366A 2005-03-22 2006-03-21 弱挥发性流体的蒸馏提纯方法 Expired - Fee Related CN101180112B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102005013030A DE102005013030A1 (de) 2005-03-22 2005-03-22 Verfahren zur destillativen Reinigung schwerflüchtiger Fluide
DE102005013030.5 2005-03-22
PCT/EP2006/002553 WO2006100023A1 (de) 2005-03-22 2006-03-21 Verfahren zur destillativen reinigung schwerflüchtiger fluide

Publications (2)

Publication Number Publication Date
CN101180112A CN101180112A (zh) 2008-05-14
CN101180112B true CN101180112B (zh) 2011-02-02

Family

ID=36579102

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2006800178366A Expired - Fee Related CN101180112B (zh) 2005-03-22 2006-03-21 弱挥发性流体的蒸馏提纯方法

Country Status (7)

Country Link
US (1) US8277615B2 (https=)
EP (1) EP1866045B1 (https=)
JP (1) JP2008538722A (https=)
CN (1) CN101180112B (https=)
AT (1) ATE530237T1 (https=)
DE (1) DE102005013030A1 (https=)
WO (1) WO2006100023A1 (https=)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005028451B4 (de) 2005-06-17 2017-02-16 Evonik Degussa Gmbh Verfahren zum Transport von Wärme
DE102006024397B3 (de) * 2006-05-24 2007-10-11 Universität Rostock Mehrphasen-Membran
DE102007041416A1 (de) * 2007-08-31 2009-03-05 Basf Se Destillation ionischer Flüssigkeiten
EP2088389B1 (de) * 2008-02-05 2017-05-10 Evonik Degussa GmbH Absorptionskältemaschine
EP2087930A1 (de) 2008-02-05 2009-08-12 Evonik Degussa GmbH Verfahren zur Absorption eines flüchtigen Stoffes in einem flüssigen Absorptionsmittel
RU2400469C2 (ru) * 2008-12-09 2010-09-27 Общество с ограниченной ответственностью "Новые технологии" Способ очистки ацетона-сырца
DE102009000543A1 (de) 2009-02-02 2010-08-12 Evonik Degussa Gmbh Verfahren, Absorptionsmedien und Vorrichtung zur Absorption von CO2 aus Gasmischungen
WO2010094640A1 (de) * 2009-02-23 2010-08-26 Basf Se Destillation ionischer flüssigkeiten unter verwendung eines destillationshilfsmittels
EP2243530A1 (de) * 2009-04-21 2010-10-27 LANXESS Deutschland GmbH Verfahren zur Trennung aromatischer Verbindungen
DE102009047564A1 (de) 2009-12-07 2011-06-09 Evonik Degussa Gmbh Arbeitsmedium für eine Absorptionskältemaschine
DE102011077377A1 (de) 2010-11-12 2012-05-16 Evonik Degussa Gmbh Verfahren zur Absorption von sauren Gasen aus Gasmischungen
WO2013072147A1 (de) 2011-11-14 2013-05-23 Evonik Degussa Gmbh Verfahren und vorrichtung zur abtrennung von sauren gasen aus einer gasmischung
US9024079B2 (en) * 2012-01-11 2015-05-05 Lanxess Deutschland Gmbh Separation of isomeric menthol compounds
JP5888993B2 (ja) * 2012-01-12 2016-03-22 ランクセス・ドイチュランド・ゲーエムベーハー メントール化合物異性体の分離
DE102012200907A1 (de) 2012-01-23 2013-07-25 Evonik Industries Ag Verfahren und Absorptionsmedium zur Absorption von CO2 aus einer Gasmischung
DE102012207509A1 (de) 2012-05-07 2013-11-07 Evonik Degussa Gmbh Verfahren zur Absorption von CO2 aus einer Gasmischung
DE102015212749A1 (de) 2015-07-08 2017-01-12 Evonik Degussa Gmbh Verfahren zur Entfeuchtung von feuchten Gasgemischen
NO20151452A1 (en) * 2015-10-26 2017-04-27 Norwegian Tech As Method for separation of non-polar organic compounds from a material
EP3257568B1 (de) 2016-06-14 2019-09-18 Evonik Degussa GmbH Verfahren zur entfeuchtung von feuchten gasgemischen mit ionischen flüssigkeiten
DE102016210483A1 (de) 2016-06-14 2017-12-14 Evonik Degussa Gmbh Verfahren und Absorptionsmittel zur Entfeuchtung von feuchten Gasgemischen
DE102016210478A1 (de) 2016-06-14 2017-12-14 Evonik Degussa Gmbh Verfahren zur Entfeuchtung von feuchten Gasgemischen
DE102016210481B3 (de) 2016-06-14 2017-06-08 Evonik Degussa Gmbh Verfahren zum Reinigen einer ionischen Flüssigkeit
EP3257843A1 (en) 2016-06-14 2017-12-20 Evonik Degussa GmbH Method of preparing a high purity imidazolium salt
DE102016210484A1 (de) 2016-06-14 2017-12-14 Evonik Degussa Gmbh Verfahren zur Entfeuchtung von feuchten Gasgemischen
CN111631986B (zh) * 2020-06-23 2021-09-17 赫禧(广州)生物科技有限公司 一种植物活性成分提纯方法及其在化妆品的应用

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3689375A (en) * 1969-06-06 1972-09-05 Daicel Ltd Separating close boiling,two component mixture by distilling in presence of selective third component
DE3613975A1 (de) * 1986-04-25 1987-10-29 Bayer Ag Trennung von diastereomeren
US4726894A (en) * 1985-12-27 1988-02-23 The Foxboro Company Distillation cut point control
CN1064224A (zh) * 1992-04-17 1992-09-09 天津大学 吸附蒸馏分离方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2080064A (en) * 1935-10-25 1937-05-11 Shell Dev Distillation process for the purification of alcohols
US2357028A (en) * 1943-08-04 1944-08-29 Shell Dev Solvent extraction process
JPH09165348A (ja) * 1995-12-15 1997-06-24 Mitsubishi Chem Corp シクロヘキセンの分離方法
US5731453A (en) * 1996-03-12 1998-03-24 Ube Industries, Ltd. Process for producing a diaryl carbonate
US6616831B1 (en) * 1997-09-03 2003-09-09 Gtc Technology Inc. Aromatics separation process and method of retrofitting existing equipment for same
AU2002304855A1 (en) * 2001-03-20 2002-10-03 Basf Aktiengesellschaft Ionic liquids as selective additives for the separation of close-boiling or azeotropic mixtures
DE10336555A1 (de) * 2003-08-05 2005-02-24 Basf Ag Recycling von lonischen Flüssigkeiten bei der Extraktiv-Destillation
US8002953B2 (en) * 2007-07-13 2011-08-23 Amt International Inc. Low-energy extractive distillation process for dehydration of aqueous ethanol

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3689375A (en) * 1969-06-06 1972-09-05 Daicel Ltd Separating close boiling,two component mixture by distilling in presence of selective third component
US4726894A (en) * 1985-12-27 1988-02-23 The Foxboro Company Distillation cut point control
DE3613975A1 (de) * 1986-04-25 1987-10-29 Bayer Ag Trennung von diastereomeren
CN1064224A (zh) * 1992-04-17 1992-09-09 天津大学 吸附蒸馏分离方法

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
GARCIA VILLALUENGA J P ET AL.A review on the separation of benzene/cyclohexane mixturesby pervaporation process.Journal of Membrane Science,Elsevier Science,Amsterdam,NL169 2.2000,169(2),159-174.
GARCIA VILLALUENGA J P ET AL.A review on the separation of benzene/cyclohexane mixturesby pervaporation process.Journal of Membrane Science,Elsevier Science,Amsterdam,NL169 2.2000,169(2),159-174. *
THEODOR GREWER.Trennung von Chlorwasserstoff und Wasser durch extraktiveDestillation mit Schwefelsaure.CHEMIE INGENIEUR TECHNIK-CIT43 11.1971,43(11),655-658.
THEODOR GREWER.Trennung von Chlorwasserstoff und Wasser durch extraktiveDestillation mit Schwefelsaure.CHEMIE INGENIEUR TECHNIK-CIT43 11.1971,43(11),655-658. *

Also Published As

Publication number Publication date
WO2006100023A1 (de) 2006-09-28
DE102005013030A1 (de) 2006-09-28
EP1866045B1 (de) 2011-10-26
CN101180112A (zh) 2008-05-14
US8277615B2 (en) 2012-10-02
ATE530237T1 (de) 2011-11-15
JP2008538722A (ja) 2008-11-06
EP1866045A1 (de) 2007-12-19
WO2006100023A9 (de) 2007-12-13
US20080283383A1 (en) 2008-11-20

Similar Documents

Publication Publication Date Title
CN101180112B (zh) 弱挥发性流体的蒸馏提纯方法
US7435318B2 (en) Ionic liquids as selective additives for separation of close-boiling or azeotropic mixtures
Bart Reactive extraction
US3367749A (en) Purifying phosphoric acid using an amine extractant
EP1824575B1 (de) Reinigung von ionischen flüssigkeiten
JP2012502889A (ja) １つまたはそれより多くのアルカノールアミンを含有する混合物を連続的に蒸留分離するための装置および方法
WO2006029788A1 (de) Verfahren zur trennung von chlorwasserstoff und phosgen
DE102004053167A1 (de) Polymere Absorptionsmittel für die Gasabsorption und Absorptionsprozess
HRP960601A2 (en) Process for separating medium boiling substances from a mixture of low, medium and high boiling substances
DE102010004779A1 (de) Verfahren zur Trocknung von Gasen
Blahušiak et al. Simulation of a new regeneration process of solvents with ionic liquid by short-path distillation
DE102008013738A1 (de) Neuartige Waschmittel zur Sauergaswäsche und Verfahren zu ihrer Verwendung
Martínez-Galmiche et al. Design of energy-efficient ionic liquid-based extractive distillation systems for ethanol dehydration including alternatives for ionic liquid recovery
Schuur Selection and design of ionic liquids as solvents in extractive distillation and extraction processes
JP6065138B1 (ja) 芳香族化合物抽出溶剤中の腐食性イオン低減方法
Gonfa et al. COSMO-RS based screening ionic liquids for separation of benzene and cyclohexane
Tabakci et al. Synthesis and application of an efficient calix [4] arene-based anion receptor bearing imidazole groups for Cr (VI) anionic species
SA516371525B1 (ar) طرق وأنظمة لإزالة الهيدروكربونات الثقيلة
JP2014040389A (ja) 酢酸の製造方法
EP1817090B1 (de) Verfahren zur chemischen umsetzung und auftrennung eines gemisches in einer kolonne
Khamizov et al. Self-Sustaining Water Softening–Desalination Processes: Chloride–Sulfate Systems
DE19536941A1 (de) Verfahren zur Entsalzung von glykolstämmigen Lösemitteln für Gaswäschen
EP2432757A1 (de) Verfahren zur reinigung von halogenverbindungen enthaltenden carbonsäuren
KR101402523B1 (ko) 수용액 중에서 테트라플루오로보레이트 음이온을 제거하고 테트라플루오로보레이트 음이온을 포함하는 이온성 액체를 얻는 방법
RU2596624C1 (ru) Экстрагент для извлечения азотной кислоты из водных растворов

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110202

Termination date: 20120321