CN101178348A - 用于确定一种聚合物中分子量分布的方法 - Google Patents
用于确定一种聚合物中分子量分布的方法 Download PDFInfo
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- CN101178348A CN101178348A CNA2007101881571A CN200710188157A CN101178348A CN 101178348 A CN101178348 A CN 101178348A CN A2007101881571 A CNA2007101881571 A CN A2007101881571A CN 200710188157 A CN200710188157 A CN 200710188157A CN 101178348 A CN101178348 A CN 101178348A
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- 238000000034 method Methods 0.000 title claims abstract description 60
- 238000009826 distribution Methods 0.000 title claims abstract description 53
- 229920000642 polymer Polymers 0.000 title abstract description 25
- 238000001228 spectrum Methods 0.000 claims abstract description 27
- 238000005259 measurement Methods 0.000 claims description 32
- 239000000126 substance Substances 0.000 claims description 31
- 230000008569 process Effects 0.000 claims description 19
- 239000011521 glass Substances 0.000 claims description 5
- 229920000459 Nitrile rubber Polymers 0.000 description 48
- 229920006168 hydrated nitrile rubber Polymers 0.000 description 34
- 238000005984 hydrogenation reaction Methods 0.000 description 15
- 241001441571 Hiodontidae Species 0.000 description 13
- 238000010008 shearing Methods 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 7
- 238000012360 testing method Methods 0.000 description 5
- 239000004793 Polystyrene Substances 0.000 description 4
- 238000004146 energy storage Methods 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 229920002223 polystyrene Polymers 0.000 description 4
- 238000004513 sizing Methods 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 238000004364 calculation method Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 238000004845 hydriding Methods 0.000 description 3
- 230000007246 mechanism Effects 0.000 description 3
- 229920001195 polyisoprene Polymers 0.000 description 3
- 230000003595 spectral effect Effects 0.000 description 3
- 230000007704 transition Effects 0.000 description 3
- 244000043261 Hevea brasiliensis Species 0.000 description 2
- 230000002902 bimodal effect Effects 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011326 mechanical measurement Methods 0.000 description 2
- 229920003052 natural elastomer Polymers 0.000 description 2
- 229920001194 natural rubber Polymers 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 238000010408 sweeping Methods 0.000 description 2
- 241001589086 Bellapiscis medius Species 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
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- 238000012790 confirmation Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
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- 238000005315 distribution function Methods 0.000 description 1
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- 230000009191 jumping Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
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- 230000002441 reversible effect Effects 0.000 description 1
- 238000000518 rheometry Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000001131 transforming effect Effects 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Images
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
- G01N11/10—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
- G01N11/14—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by using rotary bodies, e.g. vane
- G01N11/142—Sample held between two members substantially perpendicular to axis of rotation, e.g. parallel plate viscometer
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
- G01N11/10—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
- G01N11/14—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by using rotary bodies, e.g. vane
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
- G01N11/10—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
- G01N11/14—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by using rotary bodies, e.g. vane
- G01N11/142—Sample held between two members substantially perpendicular to axis of rotation, e.g. parallel plate viscometer
- G01N2011/145—Sample held between two members substantially perpendicular to axis of rotation, e.g. parallel plate viscometer both members rotating
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0014—Type of force applied
- G01N2203/0025—Shearing
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0058—Kind of property studied
- G01N2203/0092—Visco-elasticity, solidification, curing, cross-linking degree, vulcanisation or strength properties of semi-solid materials
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0058—Kind of property studied
- G01N2203/0092—Visco-elasticity, solidification, curing, cross-linking degree, vulcanisation or strength properties of semi-solid materials
- G01N2203/0094—Visco-elasticity
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/0202—Control of the test
- G01N2203/0212—Theories, calculations
- G01N2203/0218—Calculations based on experimental data
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/44—Resins; Plastics; Rubber; Leather
- G01N33/445—Rubber
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Molecular Biology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102006053390.9 | 2006-11-10 | ||
| DE102006053390A DE102006053390A1 (de) | 2006-11-10 | 2006-11-10 | Verfahren zur Bestimmung einer Molekulargewichtsverteilung in einem Polymer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101178348A true CN101178348A (zh) | 2008-05-14 |
Family
ID=39144287
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA2007101881571A Pending CN101178348A (zh) | 2006-11-10 | 2007-11-12 | 用于确定一种聚合物中分子量分布的方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7917308B2 (enExample) |
| EP (1) | EP1921436A3 (enExample) |
| JP (1) | JP2008157922A (enExample) |
| KR (1) | KR20080042742A (enExample) |
| CN (1) | CN101178348A (enExample) |
| DE (1) | DE102006053390A1 (enExample) |
| TW (1) | TWI386637B (enExample) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101458246B (zh) * | 2009-01-08 | 2012-01-11 | 浙江大学 | 测量线形聚合物分子量分布的方法 |
| CN102466604A (zh) * | 2010-11-04 | 2012-05-23 | 中国石油天然气股份有限公司 | 聚乙烯分子量的测定方法 |
| CN105675440A (zh) * | 2014-11-20 | 2016-06-15 | 中国石油天然气股份有限公司 | 快速确定纤维型聚丙烯专用料分子量分布的检测方法 |
| CN115931807A (zh) * | 2022-12-21 | 2023-04-07 | 南京大学 | 一种采用非辐射能量转移技术实时检测流场中接枝在表面的高分子链构象的方法 |
| CN119000428A (zh) * | 2024-08-23 | 2024-11-22 | 中国热带农业科学院农产品加工研究所 | 一种天然橡胶生胶固有分子量分布类型的测试方法 |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015055511A1 (en) * | 2013-10-16 | 2015-04-23 | Lanxess Deutschland Gmbh | Determination of the degree of branching |
| DE102014213850B4 (de) * | 2014-07-16 | 2018-01-18 | Bayerische Motoren Werke Aktiengesellschaft | Verfahren und Vorrichtung zum Bestimmen von Werkstoffeigenschaften |
| WO2017161292A1 (en) * | 2016-03-17 | 2017-09-21 | Mohseni Alaeddin | Unified performance test for viscoelastic materials |
| CN105928828A (zh) * | 2016-04-21 | 2016-09-07 | 陈盈洁 | 一种影响油液粘度的颗粒智能识别的方法 |
| CN113166280B (zh) | 2018-12-17 | 2023-07-11 | 阿朗新科德国有限责任公司 | 用于生产peg丙烯酸酯-hnbr共聚物的方法 |
| KR102246834B1 (ko) * | 2019-08-19 | 2021-04-30 | 에쓰대시오일 주식회사 | 고분자 결정화도의 측정 방법 및 장치 |
| ES2988262T3 (es) * | 2022-02-14 | 2024-11-19 | Borealis Ag | Método y aparato para adaptar ajustes operativos para una medición de barrido de frecuencia de un producto polimérico |
| EP4406634A1 (en) | 2023-01-30 | 2024-07-31 | Basf Se | A process for size exclusion chromatography of a not fully soluble polymeric substance, and a reference substance for size exclusion chromatography of a polymeric substance |
| WO2025212665A1 (en) * | 2024-04-03 | 2025-10-09 | Dow Global Techologies LLC | Rheology-based modeling to identify the molecular weight distribution of linear polymers |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02167563A (ja) * | 1988-09-20 | 1990-06-27 | Mitsubishi Kasei Corp | 電子写真トナー |
| JPH05240854A (ja) * | 1991-04-30 | 1993-09-21 | Tonen Corp | ポリプロピレン分子量分布の測定法 |
| US6313241B1 (en) * | 1997-10-01 | 2001-11-06 | Cryovac, Inc. | Narrow molecular weight distribution copolymers containing long chain branches and process to form same |
| JP3918267B2 (ja) * | 1997-12-19 | 2007-05-23 | 株式会社プライムポリマー | ポリオレフィン樹脂組成物、発泡用ポリオレフィン樹脂組成物および発泡体 |
| JPH11327209A (ja) * | 1998-05-18 | 1999-11-26 | Ricoh Co Ltd | 静電荷像現像用トナー |
| JP2001206994A (ja) * | 1999-09-02 | 2001-07-31 | Sumitomo Chem Co Ltd | 熱可塑性エラストマー組成物及び成形体 |
| JP2002178469A (ja) * | 2000-12-11 | 2002-06-26 | Kanegafuchi Chem Ind Co Ltd | 制振性多層フィルム |
| JP4819313B2 (ja) * | 2002-02-08 | 2011-11-24 | エクソンモービル・ケミカル・パテンツ・インク | マルチモーダルエチレン、α−オレフィン及びジエンポリマー、当該組成物を生成する方法及び当該組成物を含む装置 |
| US7427506B2 (en) * | 2004-04-13 | 2008-09-23 | Exxonmobil Chemical Patents Inc. | High throughput property testing of olefin copolymers using rheological determinations |
| GB0508255D0 (en) * | 2005-04-25 | 2005-06-01 | Lucite Int Uk Ltd | Acrylic blends |
| WO2007049802A1 (ja) * | 2005-10-26 | 2007-05-03 | Canon Kabushiki Kaisha | トナー |
-
2006
- 2006-11-10 DE DE102006053390A patent/DE102006053390A1/de not_active Withdrawn
-
2007
- 2007-11-05 EP EP07119997A patent/EP1921436A3/de not_active Withdrawn
- 2007-11-06 US US11/982,912 patent/US7917308B2/en not_active Expired - Fee Related
- 2007-11-09 KR KR1020070114238A patent/KR20080042742A/ko not_active Ceased
- 2007-11-09 TW TW096142304A patent/TWI386637B/zh not_active IP Right Cessation
- 2007-11-09 JP JP2007292264A patent/JP2008157922A/ja not_active Ceased
- 2007-11-12 CN CNA2007101881571A patent/CN101178348A/zh active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101458246B (zh) * | 2009-01-08 | 2012-01-11 | 浙江大学 | 测量线形聚合物分子量分布的方法 |
| CN102466604A (zh) * | 2010-11-04 | 2012-05-23 | 中国石油天然气股份有限公司 | 聚乙烯分子量的测定方法 |
| CN102466604B (zh) * | 2010-11-04 | 2013-07-31 | 中国石油天然气股份有限公司 | 聚乙烯分子量的测定方法 |
| CN105675440A (zh) * | 2014-11-20 | 2016-06-15 | 中国石油天然气股份有限公司 | 快速确定纤维型聚丙烯专用料分子量分布的检测方法 |
| CN115931807A (zh) * | 2022-12-21 | 2023-04-07 | 南京大学 | 一种采用非辐射能量转移技术实时检测流场中接枝在表面的高分子链构象的方法 |
| CN119000428A (zh) * | 2024-08-23 | 2024-11-22 | 中国热带农业科学院农产品加工研究所 | 一种天然橡胶生胶固有分子量分布类型的测试方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP1921436A3 (de) | 2011-05-25 |
| EP1921436A2 (de) | 2008-05-14 |
| TWI386637B (zh) | 2013-02-21 |
| US7917308B2 (en) | 2011-03-29 |
| KR20080042742A (ko) | 2008-05-15 |
| DE102006053390A1 (de) | 2008-05-15 |
| TW200839210A (en) | 2008-10-01 |
| JP2008157922A (ja) | 2008-07-10 |
| US20080162055A1 (en) | 2008-07-03 |
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| C06 | Publication | ||
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| AD01 | Patent right deemed abandoned |
Effective date of abandoning: 20080514 |
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| C20 | Patent right or utility model deemed to be abandoned or is abandoned |