CN101160381A - 聚α烯烃与费托衍生的润滑剂基础油的润滑剂调合物 - Google Patents
聚α烯烃与费托衍生的润滑剂基础油的润滑剂调合物 Download PDFInfo
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- CN101160381A CN101160381A CNA2006800124169A CN200680012416A CN101160381A CN 101160381 A CN101160381 A CN 101160381A CN A2006800124169 A CNA2006800124169 A CN A2006800124169A CN 200680012416 A CN200680012416 A CN 200680012416A CN 101160381 A CN101160381 A CN 101160381A
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- 229910052809 inorganic oxide Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052741 iridium Inorganic materials 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 229910052762 osmium Inorganic materials 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 230000010363 phase shift Effects 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000003870 refractory metal Substances 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
- 238000005382 thermal cycling Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000002211 ultraviolet spectrum Methods 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
- 230000004304 visual acuity Effects 0.000 description 1
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
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Abstract
Description
SAE粘度等级 | 最大低温起动粘度,cP | 无屈服应力的最大低温泵送粘度,cP | 在100℃的最小低剪切速率运动粘度,cSt | 在100℃的最大低剪切速率运动粘度,cSt | 在150℃的最小高剪切速率粘度,cP |
0W-_ | 6200,-35℃ | 60000,-40℃ | 3.8 | - | - |
5W-_ | 6600,-30℃ | 60000,-35℃ | 3.8 | - | - |
10W-_ | 7000,-25℃ | 60000,-30℃ | 4.1 | - | - |
15W-_ | 7000,-20℃ | 60000,-25℃ | 5.6 | - | - |
20W-_ | 9500,-15℃ | 60000,-20℃ | 5.6 | - | - |
25W-_ | 13000,-10℃ | 60000,-15℃ | 9.3 | - | - |
_W-20 | - | - | 5.6 | 9.3 | 2.6 |
_W-30 | - | - | 9.3 | 12.5 | 2.9 |
0W-40,5W-40,10W-40 | - | - | 12.5 | 16.3 | 2.9 |
15W-40,20W-40,25W-40 | - | - | 12.5 | 16.3 | 3.7 |
_W-50 | - | - | 16.3 | 21.9 | 3.7 |
_W-60 | - | 21.9 | 26.1 | 3.7 |
测试时间 | 24小时 |
温度 | 285℃ |
样品大小 | 10mL |
流动速率(样品) | 0.25g/min |
流动速率(干空气) | 12mL/min |
催化剂 | Fe+Pb+Sn |
FT-4A | FT-4B | FT-8B | |
100℃的粘度(cSt) | 3.94 | 4.415 | 7.953 |
粘度指数 | 143 | 147 | 165 |
倾点(℃) | -19 | -12 | -12 |
FIMS分析%烷烃%单环烷烃%多环烷烃总计 | 89.011.00.0100.0 | 89.110.90.0100.0 | 87.212.60.2100.0 |
费托催化剂 | 钴基 | 钴基 |
费托蜡 | FT蜡A | FT蜡B |
硫,ppm | <6 | 7,<2 |
氮,ppm | 6,5 | 12,19* |
通过NA测定的氧,wt% | 0.59 | 0.69 |
气相色谱正构烷烃分析总正构烷烃,wt%平均碳数平均分子量 | 84.4727.3384.9 | 83.7230.7432.5 |
D-6352 SIMDIST TBP(WT%),T0.5T5T10T20T30T40T50T60T70T80T90T95T99.5 | 515597639689714751774807839870911935978 | 12956862567471775679282787391496510051090 |
T90-T10,℃ | 133 | 171 |
Wt%C30+ | 34.69 | 40.86 |
Wt%C60+ | 0.00 | 0.00 |
C60+/C30+ | 0.00 | 0.00 |
性质 | FT-4A | FT-4B | FT-8B |
加氢异构化温度, | 672 | 700 | 694 |
加氢异构化脱蜡催化剂 | Pt/SAPO-11 | Pt/SAPO-11 | Pt/SAPO-11 |
反应器压力,psig | 1000 | 1000 | 1000 |
100℃的粘度,cSt | 3.94 | 4.415 | 7.953 |
粘度指数 | 143 | 147 | 165 |
芳族化合物,wt% | 0.004 | 0.008 | 0.006 |
FIMS,分子的wt%链烷烃单环烷烃多环烷烃总计 | 89.011.00.0100.0 | 89.110.90.0100.0 | 87.212.60.2100.0 |
API比重 | 42.0 | 41.6 | 39.62 |
倾点,℃ | -19 | -12 | -12 |
浊点,℃ | -9 | -8 | +13 |
单环/多环烷烃的比 | >100 | >100 | 61 |
倾点/100℃粘度的比(SMA考虑除去) | -4.82 | -2.72 | -1.51 |
基础油倾倒因子 | -7.92 | -7.09 | -2.76 |
氧化器BN,小时 | 无数据 | 41.35 | 无数据 |
Noack挥发度,wt% | 14.6 | 10.89 | 2.72 |
-35℃的CCS粘度,cP | 1611 | 2079 | 13627 |
描述 | 0W-20 | 10W-30 |
Wt%FT-4A | 73.36 | 0 |
Wt%FT-8B | 0 | 78.5 |
Wt%Mobil SHF-1003 PAO-100 | 0 | 10.85 |
Wt%Durasyn174 PAO-40 | 15.99 | 0 |
Wt%DI添加剂包 | 10.35 | 10.35 |
Wt%PPD | 0.3 | 0.3 |
CCS(cP) | 4100,在-35℃ | 6360,在-25℃ |
100℃粘度(cSt) | 7.093 | 12.54 |
粘度指数 | 170 | 172 |
Noack挥发度(Wt%) | 14.36 | 3.65 |
MRV(cP) | 8442,在-40℃ | 228879-YS,在-30℃ |
氧化器B,L-4催化剂(小时) | 未测 | 30.04 |
在150℃的HTHS(cP) | 2.22 | 3.93 |
TEOST MHT(mg) | 33.3 | 54.2 |
HFRR摩擦系数 | 0.111 | 0.104 |
HFRR平面下磨损体积(立方微米) | 148645 | 109779 |
HFRR净磨损体积(立方微米) | -1600 | 20086 |
描述 | 0W-20 | 0W-20 | 5W-30 |
Wt%FT-4A | 31.83 | 69.87 | 0 |
Wt%FT-4B | 0 | 0 | 66.15 |
Wt%Chevron Phillips PAO-8 | 57.52 | 0 | 0 |
Wt%Chevron Phillips PAO-25 | 0 | 19.47 | 0 |
Wt%Mobil SHF-1003 PAO-100 | 0 | 0 | 23.2 |
Wt%DI添加剂包 | 10.35 | 10.35 | 10.35 |
Wt%PPD | 0.3 | 0.3 | 0.3 |
CCS(cP) | 5534,在-35℃ | 3876,在-35℃ | 5993,在-30℃ |
100℃粘度(cSt) | 7.555 | 6.981 | 11.32 |
粘度指数 | 145 | 169 | 161 |
Noack挥发度(Wt%) | 7.19 | 13.77 | 9.6 |
MRV(cP) | 11768,在-40℃ | 9600,在-40℃ | 13207,在-35℃ |
氧化器B,L-4催化剂(小时) | 28.82 | 未测 | 23.29 |
在150℃的HTHS(cP) | 2.32 | 2.41 | 3.58 |
TEOST MHT(mg) | 28.7 | 25.9 | 28.5 |
HFRR摩擦系数 | 0.116 | 0.115 | 0.111 |
HFRR平面下磨损体积(立方微米) | 187885 | 182030 | 172120 |
HFRR净磨损体积(立方微米) | 55510 | 35960 | 29425 |
描述 | 全FTBO0W-20 | 全PAO0W-20 |
Wt%FT-4B | 53.74 | 0 |
Wt%FT-8B | 35.61 | 0 |
Wt%Chevron Phillips PAO-4 | 0 | 31.83 |
Wt%Chevron Phillips PAO-8 | 0 | 57.52 |
Wt%DI添加剂包 | 10.35 | 10.35 |
Wt%PPD | 0.3 | 0.3 |
CCS(cP) | 5660,在-35℃ | 5534,在-35℃ |
100℃粘度(cSt) | 7.09 | 7.555 |
粘度指数 | 167 | 145 |
Noack挥发度(Wt%) | 8.86 | 7.19 |
MRV(cP) | 失败(71156,在-40℃) | 11768,在-40℃ |
氧化器B,L-4催化剂(小时) | 28.7 | 28.82 |
在150℃的HTHS(cP) | 2.36 | 2.3 |
TEOST MHT(mg) | 40 | 28.7 |
HFRR摩擦系数 | 0.110 | 0.116 |
HFRR平面下磨损体积(立方微米) | 170340 | 180560 |
HFRR净磨损体积(立方微米) | 30190 | 38975 |
Claims (29)
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US11/069,979 | 2005-03-03 | ||
PCT/US2006/007836 WO2006094264A2 (en) | 2005-03-03 | 2006-03-01 | Polyalphaolefin & fischer-tropsch derived lubricant base oil lubricant blends |
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Also Published As
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NL1031298A1 (nl) | 2006-09-06 |
CN101160381B (zh) | 2011-03-23 |
GB0716575D0 (en) | 2007-10-10 |
ZA200707484B (en) | 2009-01-28 |
AU2006218432B2 (en) | 2011-06-09 |
BRPI0608263A2 (pt) | 2010-11-16 |
GB2438131A (en) | 2007-11-14 |
NL1031298C2 (nl) | 2007-06-06 |
WO2006094264A3 (en) | 2007-10-25 |
JP2008531834A (ja) | 2008-08-14 |
AU2006218432A1 (en) | 2006-09-08 |
GB2438131B (en) | 2010-01-13 |
US20060196807A1 (en) | 2006-09-07 |
WO2006094264A2 (en) | 2006-09-08 |
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