CN101156670A - A production process of nutrition health care roxburgh rose powder - Google Patents

A production process of nutrition health care roxburgh rose powder Download PDF

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CN101156670A
CN101156670A CNA2007100313275A CN200710031327A CN101156670A CN 101156670 A CN101156670 A CN 101156670A CN A2007100313275 A CNA2007100313275 A CN A2007100313275A CN 200710031327 A CN200710031327 A CN 200710031327A CN 101156670 A CN101156670 A CN 101156670A
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fruit
rosa roxburghii
juice
pulp
production method
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CN101156670B (en
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罗发兴
罗志刚
蓝建平
何小维
黄强
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South China University of Technology SCUT
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Abstract

The invention discloses a production method for nutritional health Rosa roxburghii powder. The method comprises the following steps: the fresh Rosa roxburghii fruit is washed to clear off dust and sundries on the surface; the fresh Rosa roxburghii fruit is enucleated to separate out the mashed fruit, and the mashed fruit is diluted with water, and pectinase is added, the mass ratio between the added water and the mashed fruit is 1 to 3: 1, the mass ratio between the pectinase and the added water is 1: 10000 to 40000, and under the temperature of 25 to 55 DEG C, pH 3.0 to 5.0 zymohydrolysis reacts 20 to 170 min; the Rosa roxburghii fruit juice can be obtained by adopting a screw rod extruder to separate the enzymolyed mashed fruit; the fruit juice is clarified by ultrafiltering; the clarified Rosa roxburghii fruit juice is concentrated till the solids content reaches 10 to 25 percent; and maltodextrin is added into the fruit juice, then the nutritional health Rosa roxburghii powder of the invention can be obtained through spray drying. The product has rich vitamin C and active ingredients, has the functions of potent antioxidant, free radical exception and anti aging, thereby being a nutritional health product suitable for all ages.

Description

A kind of production method of nourishing healthy Ribes burejense powder
Technical field
The present invention relates to a kind of production method of nourishing healthy Ribes burejense powder, specifically be meant Rosa roxburghii is converted into and be rich in potent anti-oxidant, the production method of removing the nourishing healthy Ribes burejense powder of free radical, anti-senescence function of having of vitamin C and various active composition.
Background technology
Rosa roxburghii (Rosa roxburghii Tratt) belongs to rosaceous plant, is perennial shrub, and the fruit body is all over giving birth to soft thorn, and the fruit type is like pears, and color was light green when fruit was fresh, and sweet and sour is little puckery, and special and strong fragrance is arranged.It is best with Guizhou that Rosa roxburghii originates in China southwest, is the very high health-care nutritive fruit treasure of new generation of a kind of nutritive value, and the fruit of Rosa roxburghii contains a large amount of vitamin C (V C), Superoxide Dismutase (SOD), it is 1800~2500 milligrams that per 100 gram fresh fruits on average contain vitamin C, and SOD is 54000U, and citrin is 3000 milligrams, fructose 4 grams and trace element etc., wherein V CAverage content is 10 times of Kiwi berry, 50 times of sweet orange, 455 times of apple, rich " fruit V CQueen " laudatory title, add SOD, V PHero is preced with all fruit, and the title of " three chloroazotic acid fruit " is arranged, and China produces the area of Rosa roxburghii mainly in Guizhou Province, and 86 counties of the whole province (city) are except that Rongjiang prestige Ning San county, the Congjiang distributes less, and all there is more distribution all the other counties and cities.
In recent years, prove through the science medical research, Rosa roxburghii to strong carcinogen N-N nitroso ureas or N-N nitroso proline in vivo synthesized inhibitory action, can effectively prevent the potential carcinogenic danger of such material.Superoxide dismutase claims SOD again, thereby is the active principle that a kind of superoxide radical that can effectively remove in the human body improves immunity of organisms and delays senility, and the U.S. is called " doing the factor that declines ", is widely used in the product such as medicines and health protection edible cosmetic product.At present, domestic SOD extracts from animal, plant, but owing to extract from animal blood, be difficult to eliminate various viruses, and external source is polluted, European countries have issued the order in 1999 and have forbidden that animal blood extracts SOD and is used for the mankind, and the SOD output of extracting in the plant is little, the difficult suitability for industrialized production that realizes.The experiment confirm Rosa roxburghii has functions such as good detoxifcation, toxin expelling, row's heavy metal lead, to the various chemical medicine toxin that accumulates for a long time in the human body etc., has stronger dissolving and scavenging action, and prevention colon carcinogenesis effect is especially outstanding.In addition, clinical confirmation Rosa roxburghii has good disease-resistant work usefulness, strengthens body hypoxia-bearing and fatigue effect, contains a large amount of V in the Rosa roxburghii CCan obviously strengthen immunity of organisms with function such as SOD battalion oxygen species.In recent years, Rosa roxburghii is widely used in health food and medicine, and reputation spreads far and wide.
The Rosa roxburghii product of selling on the market mostly is fruit juice class I liquid I product at present, and it is short to exist the shelf-life, and circulation is poor, and the situation that formulation is single is difficult to large-scale popularization, is restricting the plantation production of Rosa roxburghii.Rosa roxburghii is based on wild, and value is lower, and fruit price per ton is lower than 2000 yuan/ton, and peasant's enthusiasm is not high, and income is low, not the benefit of bringing for local peasant.
Vitamin C is a kind of water vitamin, is least stable in all vitamins, and is destroyed easily when preserving the processing and the cooking, also easily oxidized and decomposition.Fruit of Grossularia burejensis Berger is V in process CDecompose loss easily with SOD, final products V C, SOD content low, be difficult for being processed into powder, particularly high-load V CThe smart powder of Rosa roxburghii is not found in the market at present as yet.
High-load V is produced in the Rosa roxburghii deep processing CPowder, the several times of can rising in value be to tens of times, accelerates the hill farmer paces of shaking off poverty for the prosperity mountain area economy, building a New Socialist Countryside, and the deep processing that solves the Rosa roxburghii characteristic resources improves its value, all is significant.
Summary of the invention
The objective of the invention is to single, the high-load V of product at present Rosa roxburghii deep processing existence CThe weak point of product forms shortage provides a kind of Rosa roxburghii is processed into to be rich in V CProduction method with the nourishing healthy Ribes burejense powder of various active composition.
Purpose of the present invention is achieved through the following technical solutions:
A kind of production method of nourishing healthy Ribes burejense powder comprises the steps:
(1) the Rosa roxburghii fresh fruit is cleaned, remove dust, the foreign material on surface;
(2) pulp is isolated in the stoning of step (1) gained fruit of Grossularia burejensis Berger, the dilute with water pulp adds pectase, perhaps pectase is mixed with the water that adds earlier to be made into and dilutes enzyme liquid and add in the pulp again; The water yield of adding and the mass ratio of pulp are 1~3: 1, and pectase is 1: 10000~40000 with the mass ratio that adds water, at 25~55 ℃, pH3.0~5.0 enzyme digestion reactions, 20~170min;
(3) pulp behind the screw extruder separation enzymolysis of employing band mesh screen obtains Blackthorn pear fruit-juice; Utilize ultrafiltration that fruit juice is clarified;
(4) Blackthorn pear fruit-juice of clarifying being concentrated to solid content is 10%~25%;
(5) add maltodextrin carrier or microcrystalline cellulose carrier in fruit juice, the mass ratio of solid content is 1~3: 1 in carrier and the fruit juice, and drying obtains the health-care nutritive Ribes burejense powder.
For further realizing purpose of the present invention, described step (2) pectase is Ultra SP-L, AFPXXL or YieldMASH type pectase.Described Rosa roxburghii fresh fruit is no disease and pest, does not have breakage, does not have the medium well Rosa roxburghii fresh fruit that goes rotten.
The order number of described step (3) mesh screen is preferably 30~100 orders.
Described step (3) ultrafiltration is to use the filter membrane ultrafiltration, and the molecular weight that blocks of filter membrane is preferably 100000~300000.
The concentrated employing triple effect falling liquid film concentration evaporator of described step (4) concentrates, or adopts reverse osmosis membrane apparatus to concentrate.
The drying of described step (5) is freeze drying or spray-drying.
The present invention compared with prior art has following advantage and beneficial effect:
1, the present invention adopts and add pectase in the process of squeezing the juice, and has obtained good extraction effect, V CBe greatly improved with the utilization rate of other active ingredient, wherein V CUtilization rate reaches more than 45%.
2, the Ribes burejense powder of the present invention's production can provide high-load natural V C, V CContent is 5%~25%, have potent anti-oxidant, remove free radical, anti-senescence function.Ribes burejense powder can be made into oral formulations and directly takes and improve the health oxidation resistance, also can be made into tablet or adds in other functional product as nutrition fortifier.
3, compare with Blackthorn pear fruit-juice, the Ribes burejense powder storage that the present invention produces, easy to use is applied on market easily.
4, high-load V is produced in the Rosa roxburghii deep processing CPowder, the several times of can rising in value be to tens of times, accelerates the hill farmer paces of shaking off poverty for the prosperity mountain area economy, building a New Socialist Countryside, and the deep processing that solves the Rosa roxburghii characteristic resources improves its value, has important society and economic implications.
The specific embodiment
For understanding the present invention better; below in conjunction with embodiment the present invention is described further; the inventor is to passing through further investigation and test; many successful embodiment have been arranged; enumerate six specific embodiments below, but the scope of protection of present invention is not limited to the scope of embodiment statement.
Embodiment 1
The first step is selected no disease and pest, does not have breakage, is not had the Rosa roxburghii fresh fruit about go rotten medium well, cleans with running water, removes surperficial dust, foreign material;
Pulp is isolated in the second step fruit of Grossularia burejensis Berger stoning that previous step is fresh, the dilute with water pulp, the water yield of adding and the mass ratio of pulp are 1: 1, add the pectase Ultra SP-L that letter (China) Investment Co., Ltd of Novi produces simultaneously, pectase is 1: 40000 with the mass ratio that adds water, at 55 ℃, pH4.5 enzyme digestion reaction 20min;
The 3rd step adopted the pulp behind the screw extruder separation enzymolysis that has 100 order mesh screens to obtain Blackthorn pear fruit-juice; Utilize ultrafiltration that fruit juice is clarified, the molecular weight that blocks of filter membrane is 100000;
It is 20% that the Blackthorn pear fruit-juice of the 4th step clarification adopts triple effect falling liquid film concentration evaporator to be concentrated to solid content;
The 5th step was added the maltodextrin carrier in fruit juice, and the mass ratio of solid content is 1: 1 in carrier and the fruit juice, the spray-dried nourishing healthy Ribes burejense powder that promptly obtains.After testing, gained nourishing healthy Ribes burejense powder V CContent is 5.1%.
Embodiment 2
The first step is selected no disease and pest, does not have breakage, is not had the Rosa roxburghii fresh fruit about go rotten medium well, cleans with running water, removes surperficial dust, foreign material;
Second step was isolated pulp with fresh fruit of Grossularia burejensis Berger stoning, the dilute with water pulp, the water yield of adding and the mass ratio of pulp are 3: 1, add the pectase AFPXXL that letter (China) Investment Co., Ltd of Novi produces simultaneously, pectase is 1: 20000 with the mass ratio that adds water, at 35 ℃, pH3.0 enzyme digestion reaction 90min;
The 3rd step adopted the pulp behind the screw extruder separation enzymolysis that has 50 order mesh screens to obtain Blackthorn pear fruit-juice; Utilize ultrafiltration that fruit juice is clarified, the molecular weight that blocks of filter membrane is 200000;
It is 25% that the Blackthorn pear fruit-juice of the 4th step clarification adopts triple effect falling liquid film concentration evaporator to be concentrated to solid content;
The 5th step was added the maltodextrin carrier in fruit juice, and the mass ratio of solid content is 1.5: 1 in carrier and the fruit juice, the spray-dried nourishing healthy Ribes burejense powder that promptly obtains.After testing, gained nourishing healthy Ribes burejense powder V CContent is 24.5%.
Embodiment 3
The first step is selected no disease and pest, does not have breakage, is not had the Rosa roxburghii fresh fruit about go rotten medium well, cleans with running water, removes surperficial dust, foreign material;
Second step was isolated pulp with fresh fruit of Grossularia burejensis Berger stoning, the dilute with water pulp, the water yield of adding and the mass ratio of pulp are 2: 1, add the pectase Yield MASH that letter (China) Investment Co., Ltd of Novi produces simultaneously, pectase is 1: 10000 with the mass ratio that adds water, at 25 ℃, pH5.0 enzyme digestion reaction 170min;
The 3rd step adopted the pulp behind the screw extruder separation enzymolysis that has 30 order mesh screens to obtain Blackthorn pear fruit-juice; Utilize ultrafiltration that fruit juice is clarified, the molecular weight that blocks of filter membrane is 300000;
It is 10% that the Blackthorn pear fruit-juice of the 4th step clarification adopts triple effect falling liquid film concentration evaporator to be concentrated to solid content;
The 5th step was added the maltodextrin carrier in fruit juice, and the mass ratio of solid content is 3: 1 in carrier and the fruit juice, the spray-dried nourishing healthy Ribes burejense powder that promptly obtains.After testing, gained nourishing healthy Ribes burejense powder V CContent is 5.9%.
Embodiment 4
The first step is selected no disease and pest, does not have breakage, is not had the Rosa roxburghii fresh fruit about go rotten medium well, cleans with running water, removes surperficial dust, foreign material;
Second step was isolated pulp with fresh fruit of Grossularia burejensis Berger stoning, the pectase Yield MASH that Novi letter (China) Investment Co., Ltd is produced mixes with the water that adds earlier to be made into and dilutes enzyme liquid and add in the pulp again, the water yield of adding and the mass ratio of pulp are 2: 1, pectase is 1: 30000 with the mass ratio that adds water, at 45 ℃, pH4.8 enzyme digestion reaction 80min;
The 3rd step adopted the pulp behind the screw extruder separation enzymolysis that has 70 order mesh screens to obtain Blackthorn pear fruit-juice; Utilize ultrafiltration that fruit juice is clarified, the molecular weight that blocks of filter membrane is 200000;
It is 20% that the Blackthorn pear fruit-juice of the 4th step clarification adopts conventional reverse osmosis unit to be concentrated to solid content;
The 5th step was added the maltodextrin carrier in fruit juice, and the mass ratio of solid content is 2: 1 in carrier and the fruit juice, the spray-dried nourishing healthy Ribes burejense powder that promptly obtains.After testing, gained nourishing healthy Ribes burejense powder V CContent is 17.2%.
Embodiment 5
The first step is selected no disease and pest, does not have breakage, is not had the Rosa roxburghii fresh fruit about go rotten medium well, cleans with running water, removes surperficial dust, foreign material;
Second step was isolated pulp with fresh fruit of Grossularia burejensis Berger stoning, the dilute with water pulp, the water yield of adding and the mass ratio of pulp are 3: 1, add the pectase AFP XXL that letter (China) Investment Co., Ltd of Novi produces simultaneously, pectase is 1: 20000 with the mass ratio that adds water, at 55 ℃, pH3.5 enzyme digestion reaction 50min;
The 3rd step adopted the pulp behind the screw extruder separation enzymolysis that has 80 order mesh screens to obtain Blackthorn pear fruit-juice; Utilize ultrafiltration that fruit juice is clarified, the molecular weight that blocks of filter membrane is 200000;
It is 15% that the Blackthorn pear fruit-juice of the 4th step clarification adopts triple effect falling liquid film concentration evaporator to be concentrated to solid content;
The 5th step was added the microcrystalline cellulose carrier in fruit juice, and the mass ratio of solid content is 2.5: 1 in carrier and the fruit juice, the spray-dried nourishing healthy Ribes burejense powder that promptly obtains.After testing, gained nourishing healthy Ribes burejense powder V CContent is 9.6%.
Embodiment 6
The first step is selected no disease and pest, does not have breakage, is not had the Rosa roxburghii fresh fruit about go rotten medium well, cleans with running water, removes surperficial dust, foreign material;
Second step was isolated pulp with fresh fruit of Grossularia burejensis Berger stoning, the pectase Ultra SP-L that Novi letter (China) Investment Co., Ltd is produced mixes with the water that adds earlier to be made into and dilutes enzyme liquid and add in the pulp again, the water yield of adding and the mass ratio of pulp are 1.5: 1, pectase is 1: 25000 with the mass ratio that adds water, at 40 ℃, pH4.0 enzyme digestion reaction 110min;
The 3rd step adopted the pulp behind the screw extruder separation enzymolysis that has 100 order mesh screens to obtain Blackthorn pear fruit-juice; Utilize ultrafiltration that fruit juice is clarified, the molecular weight that blocks of filter membrane is 200000;
It is 25% that the Blackthorn pear fruit-juice of the 4th step clarification adopts triple effect falling liquid film concentration evaporator to be concentrated to solid content;
The 5th step was added the maltodextrin carrier in fruit juice, and the mass ratio of solid content is 1: 1 in carrier and the fruit juice, promptly obtains the nourishing healthy Ribes burejense powder through freeze drying.After testing, gained nourishing healthy Ribes burejense powder V CContent is 20.8%.

Claims (7)

1. the production method of a nourishing healthy Ribes burejense powder is characterized in that comprising the steps:
(1) the Rosa roxburghii fresh fruit is cleaned, remove dust, the foreign material on surface;
(2) pulp is isolated in the stoning of step (1) gained fruit of Grossularia burejensis Berger, the dilute with water pulp adds pectase, perhaps pectase is mixed with the water that adds earlier to be made into and dilutes enzyme liquid and add in the pulp again; The water yield of adding and the mass ratio of pulp are 1~3: 1, and pectase is 1: 10000~40000 with the mass ratio that adds water, at 25~55 ℃, pH3.0~5.0 enzyme digestion reactions, 20~170min;
(3) pulp behind the screw extruder separation enzymolysis of employing band mesh screen obtains Blackthorn pear fruit-juice; Utilize ultrafiltration that fruit juice is clarified;
(4) Blackthorn pear fruit-juice of clarifying being concentrated to solid content is 10%~25%;
(5) add maltodextrin carrier or microcrystalline cellulose carrier in fruit juice, the mass ratio of solid content is 1~3: 1 in carrier and the fruit juice, and drying obtains the health-care nutritive Ribes burejense powder.
2. the production method of a kind of nourishing healthy Ribes burejense powder according to claim 1 is characterized in that described step (2) pectase is Ultra SP-L, AFP XXL or Yield MASH type pectase.
3. the production method of a kind of nourishing healthy Ribes burejense powder according to claim 1 is characterized in that the order number of described step (3) mesh screen is 30~100 orders.
4. the production method of a kind of nourishing healthy Ribes burejense powder according to claim 1 is characterized in that described step (3) ultrafiltration is to use the filter membrane ultrafiltration, and the molecular weight that blocks of filter membrane is 100000~300000.
5. the production method of a kind of nourishing healthy Ribes burejense powder according to claim 1 is characterized in that the concentrated of described step (4) is to adopt triple effect falling liquid film concentration evaporator or reverse osmosis membrane apparatus.
6. the production method of a kind of nourishing healthy Ribes burejense powder according to claim 1, the drying that it is characterized in that described step (5) is freeze drying or spray-drying.
7. the production method of a kind of nourishing healthy Ribes burejense powder according to claim 1 is characterized in that the medium well Rosa roxburghii fresh fruit that described Rosa roxburghii fresh fruit goes rotten for no disease and pest, nothing breakage, nothing.
CN200710031327A 2007-11-09 2007-11-09 A production process of nutrition health care roxburgh rose powder Expired - Fee Related CN101156670B (en)

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CN102232586A (en) * 2010-04-20 2011-11-09 唐俊 Roxburgh rose red soup drink and preparation method thereof
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CN115637261A (en) * 2022-12-22 2023-01-24 中国农业大学 Rosa roxburghii SOD powder with high activity and stable quality and preparation method thereof
CN115956661A (en) * 2023-01-10 2023-04-14 春归保健科技有限公司 Rosa roxburghii freeze-dried powder rich in bioactive components and preparation method thereof
CN116076680A (en) * 2023-01-10 2023-05-09 华南理工大学 Rosa roxburghii spray powder rich in bioactive components and preparation method thereof

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