CN107397099A - A kind of preparation method of feature Chinese torreya nut flavor beverage and products thereof - Google Patents

A kind of preparation method of feature Chinese torreya nut flavor beverage and products thereof Download PDF

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Publication number
CN107397099A
CN107397099A CN201710697255.1A CN201710697255A CN107397099A CN 107397099 A CN107397099 A CN 107397099A CN 201710697255 A CN201710697255 A CN 201710697255A CN 107397099 A CN107397099 A CN 107397099A
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Prior art keywords
chinese torreya
torreya nut
feature
flavor beverage
preparation
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Inventor
陈洁
王建峰
于美
全威
田华
何志勇
周宇驰
曾茂茂
秦昉
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Lanxi Feiyisuosi Ecological Agriculture Development Co Ltd
Jiangnan University
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Lanxi Feiyisuosi Ecological Agriculture Development Co Ltd
Jiangnan University
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Priority to CN201710697255.1A priority Critical patent/CN107397099A/en
Publication of CN107397099A publication Critical patent/CN107397099A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • A23L2/60Sweeteners
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Botany (AREA)
  • Mycology (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention discloses a kind of preparation method of feature Chinese torreya nut flavor beverage and products thereof, wherein, method includes, and pretreatment, Chinese torreya nut shells, and by kernel cleaning, drying, oil expression, obtains Chinese torreya nut grouts, after crushing, obtains Chinese torreya nut grouts powder;Extract solution is prepared, takes the Chinese torreya nut grouts powder, adds water, is centrifuged after stirring, filters, obtains Chinese torreya nut extract solution;Feature Chinese torreya nut flavor beverage is prepared, Chinese torreya nut extract solution is mixed with other auxiliary materials, obtains feature Chinese torreya nut flavor beverage.The technological equipment investment that the present invention prepares feature Chinese torreya nut flavor beverage is few, with short production cycle, prepares efficiently, and simple to operate, safety, cost is low, is easy to industrialized production.

Description

A kind of preparation method of feature Chinese torreya nut flavor beverage and products thereof
Technical field
The invention belongs to Chinese torreya nut extractive technique field, and in particular to a kind of preparation side of feature Chinese torreya nut flavor beverage Method and products thereof.
Background technology
Chinese torreya nut is not only the rare precious nut in the world, and the distinctive economic kind in China, have it is very high it is edible, Medical value.There are some researches show Chinese torreya nut is per the about fatty 44.0g of hectogram, protein 10.0g, water 6.4g, carbohydrate 29.8g, crude fibre 6.8g, ash content 2.9g and a variety of to human body containing abundant amino acid, vitamin and mineral matter element etc. Beneficial nutriment, there is the effect of anti-inflammatory, antifungal activity, sterilization, antiviral and antitumor activity, be to be used to treat The broad-spectrum de-worming medicine of a variety of diseases such as cough, rheumatism and Enterozoa.《Sheng Nong's herbal classic》、《Chinese Pharmacopoeia》And《Name Doctor does not record》There is good drug effect etc. Chinese torreya nut is also described in a variety of books, its flat property and sweet taste, enter lung, stomach and large intestine channel.It is fragrant Chinese torreyanut fat content is 42.67~61.47%, and content of fatty acid is high and composition is various, and unrighted acid is mainly with linoleic acid Based on oleic acid etc.;Saturated fatty acid is based on behenic acid;And unsaturated fatty acid content accounts for 80% left side of total fatty acid content The right side, there is preferable functional characteristic, there is higher nutritive value.As Chinese torreya plants the expansion of industry, Chinese torreya oil resource Exploitation must turn into trend.
Abundant albumen, carbohydrate, terpene, mineral matter, polyphenol isoreactivity material can still be contained in its grouts, had anti-oxidant It is a kind of excellent exploitable resources with the multiple biological activities function such as antibacterial, but grouts is extracted, a large amount of technologies is present Problem, such as the loss of extraction process mineral is serious, extract dissolubility is poor, unstable, extract has bad color and luster, it is raw Thing active function etc..Therefore, it is badly in need of a kind of method for solving Chinese torreya nut grouts and extracting problem, and is introduced into industrial applications 's.
The content of the invention
The purpose of this part is to summarize some aspects of embodiments of the invention and briefly introduce some preferably to implement Example.It may do a little simplified or be omitted to avoid making our department in this part and the description of the present application summary and denomination of invention Point, the purpose of specification digest and denomination of invention obscure, and this simplification or omit and cannot be used for limiting the scope of the present invention.
In view of above-mentioned and/or existing capability Chinese torreya nut flavor beverage preparation method, extracts Chinese torreya nut activity in grouts The technological gap of material, it is proposed that the present invention.
It is therefore an object of the present invention to solves deficiency of the prior art, there is provided a kind of feature Chinese torreya nut flavor beverage Preparation method.
In order to solve the above technical problems, the invention provides following technical scheme:A kind of feature Chinese torreya nut flavor beverage Preparation method, including, pretreatment, Chinese torreya nut shells, and by kernel cleaning, drying, oil expression, obtains Chinese torreya nut grouts, after crushing, Obtain Chinese torreya nut grouts powder;Extract solution is prepared, takes the Chinese torreya nut grouts powder, adds water, is centrifuged after stirring, filters, obtains Chinese torreya Sub- extract solution;Feature Chinese torreya nut flavor beverage is prepared, Chinese torreya nut extract solution is mixed with other auxiliary materials, obtains feature Chinese torreya Sub- flavor beverage.
As a kind of preferred scheme of the preparation method of feature Chinese torreya nut flavor beverage of the present invention, wherein:It is described Other auxiliary materials include the one or more in sugar, flavoring essence, sodium citrate or xanthans.
As a kind of preferred scheme of the preparation method of feature Chinese torreya nut flavor beverage of the present invention, wherein:It is described Chinese torreya nut extract solution is mixed with other auxiliary materials, wherein, counted using the Chinese torreya nut extract solution quality as 100%, described other are auxiliary Material includes sugared 1.8~2.2%, flavoring essence 0.10~0.12%, sodium citrate 0.04~0.06%, and xanthans 0.01~ 0.03%.
As a kind of preferred scheme of the preparation method of feature Chinese torreya nut flavor beverage of the present invention, wherein:It is described Stirring, its mixing speed is 500~700r/min, and mixing time is 1~3h, during temperature remain 20~30 DEG C.
As a kind of preferred scheme of the preparation method of feature Chinese torreya nut flavor beverage of the present invention, wherein:It is described Add water, the addition of its reclaimed water adds 7~9mL water for every gram of Chinese torreya nut grouts powder.
As a kind of preferred scheme of the preparation method of feature Chinese torreya nut flavor beverage of the present invention, wherein:It is described Centrifugation, its centrifugal force is 8000~12000g, and the time is 15~25min.
As a kind of preferred scheme of the preparation method of feature Chinese torreya nut flavor beverage of the present invention, wherein:It is described Drying, its drying temperature are 30~40 DEG C.
As a kind of preferred scheme of the preparation method of feature Chinese torreya nut flavor beverage of the present invention, wherein:It is described Oil expression, including temperature remains 50~60 DEG C during oil expression.
As a kind of preferred scheme of the preparation method of feature Chinese torreya nut flavor beverage of the present invention, wherein:It is described Crush, it is to cross 35~45 mesh sieves after crushing.
It is a still further object of the present invention to provide a kind of feature Chinese torreya nut flavor beverage.
In order to solve the above technical problems, the invention provides following technical scheme:A kind of feature Chinese torreya nut flavor beverage, Including being counted using Chinese torreya nut extract solution quality as claimed in claim 1 as 100%, the feature Chinese torreya nut flavor beverage bag Include sugar 1.8~2.2%, flavoring essence 0.10~0.12%, sodium citrate 0.04~0.06%, xanthans 0.01~0.03%.
Beneficial effect possessed by the present invention:
(1) present invention prepare Chinese torreya seed extract technological equipment investment it is few, it is with short production cycle, prepare efficient, operation letter Single, safety, cost is low, is easy to industrialized production.
(2) the preferred specified quantitative white granulated sugar of Chinese torreya nut beverage prepared by the present invention is as sweetener, and its addition is low, not only not Chinese torreya nut and the intrinsic flavor of flavoring essence can be covered, may also provide energy, and causes Chinese torreya nut beverage vessel for good mouth Sense, and cooperateed with the albumen of Chinese torreya seed extract and can make the strong stabilization of beverage flavor.
(3) contain more aldehydes matter in Chinese torreya nut beverage prepared by the present invention, and there is outstanding inoxidizability.
(4) Chinese torreya nut extract solution Mineral Elements prepared by the present invention, potassium, magnesium, calcium, zinc, manganese equal size enrich, and sodium Content is relatively low, meets rational hyperkalemia hyponatremia fitness mode.
(5) of the invention to extract oil grouts as raw material using Chinese torreya nut, making full use of accessory substance, economy is imitated as processing raw material It is beneficial high.
(6) dissolubility of water extract prepared by the present invention in acid and neutral solution is high and stability is strong, solution tool Standby vivid color and luster, can be good at being applied to beverage systems.
Embodiment
In order to facilitate the understanding of the purposes, features and advantages of the present invention, with reference to specific embodiment pair The embodiment of the present invention is described in detail.
Many details are elaborated in the following description to facilitate a thorough understanding of the present invention, still the present invention can be with It is different from other manner described here using other to implement, those skilled in the art can be without prejudice to intension of the present invention In the case of do similar popularization, therefore the present invention is not limited by following public specific embodiment.
Secondly, " one embodiment " or " embodiment " referred to herein refers to may be included at least one realization side of the present invention Special characteristic, structure or characteristic in formula." in one embodiment " that different places occur in this manual not refers both to Same embodiment, nor the single or selective embodiment mutually exclusive with other embodiment.
Embodiment 1
After Chinese torreya nut shells, kernel is cleaned, is dried at 35 DEG C, without the technique such as high temperature frying is broken, directly by fruit Benevolence is added in twin-screw oil mill, and for control temperature at 55 DEG C, collection obtains Chinese torreya nut grouts, grouts through omnipotent crusher in crushing, And cross 40 mesh sieves and obtain Chinese torreya nut grouts powder.A certain amount of Chinese torreya nut grouts powder is weighed, uses deionized water as Extraction solvent, is expected Liquor ratio is m Chinese torreya nut powder:V water=1:8 (g/mL), at 25 DEG C, 600r/min is stirred 2 hours and is centrifuged 10000g, 20min, most Afterwards with 8 layers of filtered through gauze 2 times, Chinese torreya nut extract solution is obtained.According to mass fraction, Chinese torreya nut drink formula is as follows:Chinese torreya nut carries Take liquid 100%, sugar 2.0%, strawberry essence 0.12%, sodium citrate 0.05%, xanthans 0.02%.
The measure of total phenol content is determined using the method for forint phenol-sodium carbonate, after testing 0.56mg/mL containing phenols.
With the inoxidizability ABTS+ working solutions in ABTS+ method determination samples by 7.0mmol/L ABTS and 2.45mmol/L potassium peroxydisulfate is made into, and is placed 16h in dark and obtained.In use, ABTS+ working solutions tune absorbance is 0.70 ± 0.01 (734nm) is designated as Abscontrol.Sample concentration is suitably diluted to 0.5~3.5mg/mL, take 20 μ L samples with 1mL ABTS+ liquid is mixed, and ultraviolet-spectrophotometer determination sample extinction under 734nm wavelength is used after dark treatment 10min Degree, is designated as Abssample.Standard curve, antioxygen are done with the Trolox (watermiscible vitamin E) that concentration is 50~2500 μm of ol/L The Trolox equivalents (mmol/100g) for changing sexuality in 100g samples to contain calculate.
The ABTS+ inhibiting rate computational methods of the sample of various concentrations are as described below:
After measured to the inhibiting rates of ABTS+ free radicals up to 78.50%.
Ash content test is carried out to Chinese torreya nut extract solution, measures and accounts for the 22.51% of total content, illustrate to contain in water extract A large amount of mineral elements, extracting method are advantageous to the leaching of soluble mineral element, and potassium in extract solution, magnesium, calcium, zinc, and manganese etc. contains Amount is abundant, and the content of sodium is relatively low, meets rational hyperkalemia hyponatremia fitness mode.
Also contain polysaccharide, Soluble Fiber and other soluble components in the present embodiment in Chinese torreya nut water extract, account for The 60.06% of total content, the presence of these materials, invent preferable sugared addition with us and form cooperative effect, can be water extraction Thing is taken to provide Chinese torreya nut beverage made from preferable taste and flavor, mouthfeel is soft, and in terms of subjective appreciation mouthfeel, ten point system obtains 9.6 points, and beverage flavor is strong and shelf life in flavor quality it is constant.
Dissolubility of the Chinese torreya seed extract made from the present embodiment in acid and neutral solution is high and stability is strong, solution Possess vivid color and luster, can be good at being applied to beverage systems.
Embodiment 2
After Chinese torreya nut shells, kernel is cleaned, is dried at 30 DEG C, without the technique such as high temperature frying is broken, directly by fruit Benevolence is added in twin-screw oil mill, and for control temperature at 60 DEG C, collection obtains Chinese torreya nut grouts, grouts through omnipotent crusher in crushing, And cross 35 mesh sieves and obtain Chinese torreya nut grouts powder.A certain amount of Chinese torreya nut grouts powder is weighed, uses deionized water as Extraction solvent, is expected Liquor ratio is m Chinese torreya nut powder:V water=1:7 (g/mL), at 30 DEG C, 700r/min is stirred 3 hours and is centrifuged 12000g, 15min, most Afterwards with 8 layers of filtered through gauze 2 times, Chinese torreya nut extract solution is obtained.According to mass fraction, Chinese torreya nut drink formula is as follows:Chinese torreya nut carries Take liquid 100%, sugar 2.2%, milk flavour 0.12%, sodium citrate 0.04%, xanthans 0.03%.
The measure of total phenol content is determined using the method for forint phenol-sodium carbonate, after testing 0.54mg/mL containing phenols.
With the inoxidizability ABTS+ working solutions in ABTS+ method determination samples by 7.0mmol/L ABTS and 2.45mmol/L potassium peroxydisulfate is made into, and is placed 16h in dark and obtained.In use, ABTS+ working solutions tune absorbance is 0.70 ± 0.01 (734nm) is designated as Abscontrol.Sample concentration is suitably diluted to 0.5~3.5mg/mL, take 20 μ L samples with 1mL ABTS+ liquid is mixed, and ultraviolet-spectrophotometer determination sample extinction under 734nm wavelength is used after dark treatment 10min Degree, is designated as Abssample.Standard curve, antioxygen are done with the Trolox (watermiscible vitamin E) that concentration is 50~2500 μm of ol/L The Trolox equivalents (mmol/100g) for changing sexuality in 100g samples to contain calculate.
The ABTS+ inhibiting rate computational methods of the sample of various concentrations are as described below:
To the inhibiting rates of ABTS+ free radicals up to 77.32%.
Ash content test is carried out to Chinese torreya nut extract solution, measures and accounts for the 18.50% of total content, illustrate to contain in water extract A large amount of mineral elements, extracting method are advantageous to the leaching of soluble mineral element, and potassium in extract solution, magnesium, calcium, zinc, and manganese etc. contains Amount is abundant, and the content of sodium is relatively low, meets rational hyperkalemia hyponatremia fitness mode.
Also contain polysaccharide, Soluble Fiber and other soluble components in the present embodiment in Chinese torreya nut water extract, account for The 58.14% of total content, the presence of these materials, invent preferable sugared addition with us and form cooperative effect, can be water extraction Thing is taken to provide Chinese torreya nut beverage made from preferable taste and flavor, mouthfeel is soft, and in terms of subjective appreciation mouthfeel, ten point system obtains 9.0 points, and beverage flavor is strong and shelf life in flavor quality it is constant.
Dissolubility of the Chinese torreya seed extract made from the present embodiment in acid and neutral solution is high and stability is strong, solution Possess vivid color and luster, can be good at being applied to beverage systems.
Embodiment 3
After Chinese torreya nut shells, kernel is cleaned, is dried at 30 DEG C, without the technique such as high temperature frying is broken, directly by fruit Benevolence is added in twin-screw oil mill, and for control temperature at 55 DEG C, collection obtains Chinese torreya nut grouts, grouts through omnipotent crusher in crushing, And cross 40 mesh sieves and obtain Chinese torreya nut grouts powder.A certain amount of Chinese torreya nut grouts powder is weighed, uses deionized water as Extraction solvent, is expected Liquor ratio is m Chinese torreya nut powder:V water=1:8 (g/mL), at 30 DEG C, 700r/min is stirred 2 hours and is centrifuged 8000g, 15min, finally With 8 layers of filtered through gauze 2 times, Chinese torreya nut extract solution is obtained.According to mass fraction, Chinese torreya nut drink formula is as follows:Chinese torreya nut extracts Liquid 100%, sugar 2.2%, small wheat essence 0.10%, sodium citrate 0.04%, xanthans 0.03%.
The measure of total phenol content is determined using the method for forint phenol-sodium carbonate, after testing 0.54mg/mL containing phenols.
With the inoxidizability ABTS+ working solutions in ABTS+ method determination samples by 7.0mmol/L ABTS and 2.45mmol/L potassium peroxydisulfate is made into, and is placed 16h in dark and obtained.In use, ABTS+ working solutions tune absorbance is 0.70 ± 0.01 (734nm) is designated as Abscontrol.Sample concentration is suitably diluted to 0.5~3.5mg/mL, take 20 μ L samples with 1mL ABTS+ liquid is mixed, and ultraviolet-spectrophotometer determination sample extinction under 734nm wavelength is used after dark treatment 10min Degree, is designated as Abssample.Standard curve, antioxygen are done with the Trolox (watermiscible vitamin E) that concentration is 50~2500 μm of ol/L The Trolox equivalents (mmol/100g) for changing sexuality in 100g samples to contain calculate.
The ABTS+ inhibiting rate computational methods of the sample of various concentrations are as described below:
To the inhibiting rates of ABTS+ free radicals up to 77.89%.
Ash content test is carried out to Chinese torreya nut extract solution, measures and accounts for the 15.42% of total content, illustrate to contain in water extract A large amount of mineral elements, extracting method are advantageous to the leaching of soluble mineral element, and potassium in extract solution, magnesium, calcium, zinc, and manganese etc. contains Amount is abundant, and the content of sodium is relatively low, meets rational hyperkalemia hyponatremia fitness mode.
Also contain polysaccharide, Soluble Fiber and other soluble components in the present embodiment in Chinese torreya nut water extract, account for The 57.62 of total content, the presence of these materials, invent preferable sugared addition with us and form cooperative effect, can be that water extracts Thing provides Chinese torreya nut beverage made from preferable taste and flavor, and mouthfeel is soft, and in terms of subjective appreciation mouthfeel, ten point system obtains 8.9 points, and beverage flavor is strong and shelf life in flavor quality it is constant.
Dissolubility of the Chinese torreya seed extract made from the present embodiment in acid and neutral solution is high and stability is strong, solution Possess vivid color and luster, can be good at being applied to beverage systems.
Embodiment 4
After Chinese torreya nut shells, kernel is cleaned, is dried at 30 DEG C, without the technique such as high temperature frying is broken, directly by fruit Benevolence is added in twin-screw oil mill, and for control temperature at 60 DEG C, collection obtains Chinese torreya nut grouts, grouts through omnipotent crusher in crushing, And cross 35 mesh sieves and obtain Chinese torreya nut grouts powder.A certain amount of Chinese torreya nut grouts powder is weighed, uses deionized water as Extraction solvent, is expected Liquor ratio is m Chinese torreya nut powder:V water=1:8 (g/mL), at 25 DEG C, 600r/min is stirred 3 hours and is centrifuged 10000g, 25min, most Afterwards with 8 layers of filtered through gauze 2 times, Chinese torreya nut extract solution is obtained.According to mass fraction, Chinese torreya nut drink formula is as follows:Chinese torreya nut carries Liquid 100% is taken, sugar 1.8%, smears tea perfume essence 0.10%, sodium citrate 0.05%, xanthans 0.02%.
The measure of total phenol content is determined using the method for forint phenol-sodium carbonate, after testing 0.55mg/mL containing phenols.
With the inoxidizability ABTS+ working solutions in ABTS+ method determination samples by 7.0mmol/L ABTS and 2.45mmol/L potassium peroxydisulfate is made into, and is placed 16h in dark and obtained.In use, ABTS+ working solutions tune absorbance is 0.70 ± 0.01 (734nm) is designated as Abscontrol.Sample concentration is suitably diluted to 0.5~3.5mg/mL, take 20 μ L samples with 1mL ABTS+ liquid is mixed, and ultraviolet-spectrophotometer determination sample extinction under 734nm wavelength is used after dark treatment 10min Degree, is designated as Abssample.Standard curve, antioxygen are done with the Trolox (watermiscible vitamin E) that concentration is 50~2500 μm of ol/L The Trolox equivalents (mmol/100g) for changing sexuality in 100g samples to contain calculate.
The ABTS+ inhibiting rate computational methods of the sample of various concentrations are as described below:
To the inhibiting rates of ABTS+ free radicals up to 77.67%.
Ash content test is carried out to Chinese torreya nut extract solution, measures and accounts for the 16.83% of total content, illustrate to contain in water extract A large amount of mineral elements, extracting method are advantageous to the leaching of soluble mineral element, and potassium in extract solution, magnesium, calcium, zinc, and manganese etc. contains Amount is abundant, and the content of sodium is relatively low, meets rational hyperkalemia hyponatremia fitness mode.
Also contain polysaccharide, Soluble Fiber and other soluble components in the present embodiment in Chinese torreya nut water extract, account for The 57.02% of total content, the presence of these materials, invent preferable sugared addition with us and form cooperative effect, can be water extraction Thing is taken to provide Chinese torreya nut beverage made from preferable taste and flavor, mouthfeel is soft, and in terms of subjective appreciation mouthfeel, ten point system obtains 8.5 points, and beverage flavor is strong and shelf life in flavor quality it is constant.
Dissolubility of the Chinese torreya seed extract made from the present embodiment in acid and neutral solution is high and stability is strong, solution Possess vivid color and luster, can be good at being applied to beverage systems.
Embodiment 5
After Chinese torreya nut shells, kernel is cleaned, is dried at 40 DEG C, without the technique such as high temperature frying is broken, directly by fruit Benevolence is added in twin-screw oil mill, and for control temperature at 55 DEG C, collection obtains Chinese torreya nut grouts, grouts through omnipotent crusher in crushing, And cross 40 mesh sieves and obtain Chinese torreya nut grouts powder.A certain amount of Chinese torreya nut grouts powder is weighed, uses deionized water as Extraction solvent, is expected Liquor ratio is m Chinese torreya nut powder:V water=1:8 (g/mL), at 30 DEG C, 700r/min is stirred 3 hours and is centrifuged 10000g, 25min, most Afterwards with 8 layers of filtered through gauze 2 times, Chinese torreya nut extract solution is obtained.According to mass fraction, Chinese torreya nut drink formula is as follows:Chinese torreya nut carries Take liquid 100%, sugar 2.0%, jasmine flower essence 0.12%, sodium citrate 0.05%, xanthans 0.01%.
The measure of total phenol content is determined using the method for forint phenol-sodium carbonate, after testing 0.55mg/mL containing phenols.
With the inoxidizability ABTS+ working solutions in ABTS+ method determination samples by 7.0mmol/L ABTS and 2.45mmol/L potassium peroxydisulfate is made into, and is placed 16h in dark and obtained.In use, ABTS+ working solutions tune absorbance is 0.70 ± 0.01 (734nm) is designated as Abscontrol.Sample concentration is suitably diluted to 0.5~3.5mg/mL, take 20 μ L samples with 1mL ABTS+ liquid is mixed, and ultraviolet-spectrophotometer determination sample extinction under 734nm wavelength is used after dark treatment 10min Degree, is designated as Abssample.Standard curve, antioxygen are done with the Trolox (watermiscible vitamin E) that concentration is 50~2500 μm of ol/L The Trolox equivalents (mmol/100g) for changing sexuality in 100g samples to contain calculate.
The ABTS+ inhibiting rate computational methods of the sample of various concentrations are as described below:
To the inhibiting rates of ABTS+ free radicals up to 78.12%.
Ash content test is carried out to Chinese torreya nut extract solution, measures and accounts for the 17.11% of total content, illustrate to contain in water extract A large amount of mineral elements, extracting method are advantageous to the leaching of soluble mineral element, and potassium in extract solution, magnesium, calcium, zinc, and manganese etc. contains Amount is abundant, and the content of sodium is relatively low, meets rational hyperkalemia hyponatremia fitness mode.
Also contain polysaccharide, Soluble Fiber and other soluble components in the present embodiment in Chinese torreya nut water extract, account for The 55.02% of total content, the presence of these materials, invent preferable sugared addition with us and form cooperative effect, can be water extraction Thing is taken to provide Chinese torreya nut beverage made from preferable taste and flavor, mouthfeel is soft, and in terms of subjective appreciation mouthfeel, ten point system obtains 8.5 points, and beverage flavor is strong and shelf life in flavor quality it is constant.
Dissolubility of the Chinese torreya seed extract made from the present embodiment in acid and neutral solution is high and stability is strong, solution Possess vivid color and luster, can be good at being applied to beverage systems.
It is noted that our invention finds that we invents the Chinese torreya nut extract solution of extraction, contained in research process Abundant polysaccharide and polyphenols can influence each other, and produce cooperative effect, can improve flavor, the nutritive value of food Energetically acted on preventing that its oxidation, brown stain etc. have.Polyphenol being esterified, it is acylated and by way of methylating with Carbohydrate is combined, and polysaccharide can also be combined as large biological molecule material by active forces such as hydrophobic, electrostatic and hydrogen bonds with polyphenol, So as to give play to more functional characteristics.Further, we, which invents, passes through selection process, from 50~60 DEG C of oil expression temperature Degree so that polysaccharide, polyphenol substance can keep stable in Chinese torreya nut, also, in extraction process, use mixing speed as 500 ~700r/min, temperature remain 20~30 DEG C, specific during the two conditions can promote present invention extraction Chinese torreya nut Mixing speed cause electric charge rearrangement in the extract solution in extraction process, the larger polysaccharide of active force during arrangement And polyphenol can more be combined during recovering after electric charge order is upset, stirred simultaneously by the combination of electrostatic interaction Specific mixing speed and bulk temperature is preferred during mixing, and the energy brought in whipping process is enabled to, in part The temperature difference is produced, the presence of this temperature difference promotes polyphenol and combined with carbohydrate by methylating, the presence of both effect so that rich Rich polysaccharide and polyphenols produce bigger synergy, improve flavor, the inoxidizability of product comprehensively.
Simultaneously it is to be noted that in extraction process, the auxochrome groups such as hydroxyl, carboxyl easily occur and are oxidized to carbonyl, ester The phenomenon of the chromophoric groups such as base so that the color is too dark for the Chinese torreya nut extract solution extracted, and Foods or drinkses can not be met in sense organ The requirement of aspect.It is 500~700r/min that to this, we, which invents mixing speed when being extracted by preferred optimization, and temperature remains 20~30 DEG C of extraction scheme, prevent from that hydroxyl, carboxylic-oxidized occur in extraction process, and by promoting polysaccharide and Polyphenols Combination, maintain the vivid color and luster of extract solution.Secondly, the ratio of suitable grouts and extraction water, also substantially increases extraction Efficiency.
It is a little that we invents in addition to find by studying, the albumen that Chinese torreya extract solution contains in itself, is added in specific sugar In the case of amount, synergy can be formed, protects the stability of addition essence later so that essence is with rich flavor and very steady It is fixed lasting.Other are a little that we has found under study for action in invention, and the extraction process of offer is invented using us, enables to water Content of ashes in extract increases, and promotes the leaching of soluble mineral element, and rareer promoted in extraction process Enter potassium, magnesium, calcium, zinc, the leaching of manganese, and the content of sodium is very low, has met rational hyperkalemia hyponatremia fitness mode.
As can be seen here, the present invention prepare Chinese torreya seed extract technological equipment investment it is few, it is with short production cycle, prepare it is efficient, Simple to operate, safety, cost is low, is easy to industrialized production;The preferred specified quantitative white granulated sugar of Chinese torreya nut beverage prepared by the present invention is made For sweetener, its addition is low, will not only cover Chinese torreya nut and the intrinsic flavor of flavoring essence, may also provide energy, and So that Chinese torreya nut beverage vessel is for good mouthfeel, and cooperateed with the albumen of Chinese torreya seed extract and can make the strong stabilization of beverage flavor; Contain more aldehydes matter in Chinese torreya nut beverage prepared by the present invention, and there is outstanding inoxidizability;Prepared by the present invention Chinese torreya nut extract solution Mineral Elements, potassium, magnesium, calcium, zinc, manganese equal size enriches, and the content of sodium is relatively low, meets rational high potassium Low sodium fitness mode;The present invention is used as raw material using Chinese torreya nut oil expression grouts, makes full use of accessory substance as processing raw material, economy High efficiency;The dissolubility of water extract prepared by the present invention in acid and neutral solution is high and stability is strong, and solution possesses fresh Bright color and luster, it can be good at being applied to beverage systems.
It should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to preferable The present invention is described in detail embodiment, it will be understood by those within the art that, can be to the technology of the present invention Scheme is modified or equivalent substitution, and without departing from the spirit and scope of technical solution of the present invention, it all should cover in this hair Among bright right.

Claims (10)

  1. A kind of 1. preparation method of feature Chinese torreya nut flavor beverage, it is characterised in that:Including,
    Pretreatment:Chinese torreya nut shells, and by kernel cleaning, drying, oil expression, obtains Chinese torreya nut grouts, after crushing, obtains Chinese torreya nut cake Dregs of rice powder;
    Prepare extract solution:The Chinese torreya nut grouts powder is taken, adds water, is centrifuged after stirring, filters, obtains Chinese torreya nut extract solution;
    Prepare feature Chinese torreya nut flavor beverage:Chinese torreya nut extract solution is mixed with other auxiliary materials, obtains feature Chinese torreya nut wind Flavor beverage.
  2. 2. the preparation method of feature Chinese torreya nut flavor beverage according to claim 1, it is characterised in that:Other described auxiliary materials Including the one or more in sugar, flavoring essence, sodium citrate or xanthans.
  3. 3. the preparation method of feature Chinese torreya nut flavor beverage according to claim 1 or claim 2, it is characterised in that:It is described by perfume (or spice) Chinese torreyanut extract solution mixes with other auxiliary materials, wherein, counted using the Chinese torreya nut extract solution quality as 100%, other described accessory packages Include sugar 1.8~2.2%, flavoring essence 0.10~0.12%, sodium citrate 0.04~0.06%, xanthans 0.01~0.03%.
  4. 4. the preparation method of feature Chinese torreya nut flavor beverage according to claim 1, it is characterised in that:The stirring, its Mixing speed is 500~700r/min, and mixing time is 1~3h, during temperature remain 20~30 DEG C.
  5. 5. according to the preparation method of feature Chinese torreya nut flavor beverage any one of claim 1,2 or 4, its feature exists In:Described plus water, the addition of its reclaimed water add 7~9mL water for every gram of Chinese torreya nut grouts powder.
  6. 6. the preparation method of feature Chinese torreya nut flavor beverage according to claim 5, it is characterised in that:The centrifugation, its Centrifugal force is 8000~12000g, and the time is 15~25min.
  7. 7. according to the preparation method of feature Chinese torreya nut flavor beverage any one of claim 1,2,4 or 6, its feature exists In:The drying, its drying temperature are 30~40 DEG C.
  8. 8. the preparation method of feature Chinese torreya nut flavor beverage according to claim 7, it is characterised in that:The oil expression, bag Temperature remains 50~60 DEG C during including oil expression.
  9. 9. according to the preparation method of feature Chinese torreya nut flavor beverage any one of claim 1,2,4,6 or 8, its feature It is:The crushing, it is to cross 35~45 mesh sieves after crushing.
  10. A kind of 10. feature Chinese torreya nut flavor beverage, it is characterised in that:Including,
    Counted using Chinese torreya nut extract solution quality as claimed in claim 1 as 100%, the feature Chinese torreya nut flavor beverage includes Sugar 1.8~2.2%, flavoring essence 0.10~0.12%, sodium citrate 0.04~0.06%, xanthans 0.01~0.03%.
CN201710697255.1A 2017-08-15 2017-08-15 A kind of preparation method of feature Chinese torreya nut flavor beverage and products thereof Pending CN107397099A (en)

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