CN101098851B - β-烷氧基丙酰胺类、溶剂、洗涤剂和液态药物组合物以及β-烷氧基丙酰胺类的制备方法 - Google Patents
β-烷氧基丙酰胺类、溶剂、洗涤剂和液态药物组合物以及β-烷氧基丙酰胺类的制备方法 Download PDFInfo
- Publication number
- CN101098851B CN101098851B CN2005800465154A CN200580046515A CN101098851B CN 101098851 B CN101098851 B CN 101098851B CN 2005800465154 A CN2005800465154 A CN 2005800465154A CN 200580046515 A CN200580046515 A CN 200580046515A CN 101098851 B CN101098851 B CN 101098851B
- Authority
- CN
- China
- Prior art keywords
- beta
- solvent
- alkoxypropionamide
- alkoxypropionamides
- general formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000002904 solvent Substances 0.000 title claims abstract description 38
- 239000007788 liquid Substances 0.000 title abstract description 14
- 239000003599 detergent Substances 0.000 title abstract 4
- 239000008194 pharmaceutical composition Substances 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title description 2
- 239000000203 mixture Substances 0.000 claims description 24
- 125000004432 carbon atom Chemical group C* 0.000 claims description 16
- 238000005406 washing Methods 0.000 claims description 14
- 125000000217 alkyl group Chemical group 0.000 claims description 13
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 5
- 229940125904 compound 1 Drugs 0.000 claims description 2
- 150000001408 amides Chemical class 0.000 abstract description 18
- 239000003814 drug Substances 0.000 abstract description 16
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 abstract description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 13
- 125000001931 aliphatic group Chemical group 0.000 abstract description 13
- 238000000034 method Methods 0.000 abstract description 8
- 239000003054 catalyst Substances 0.000 abstract description 7
- 239000012188 paraffin wax Substances 0.000 abstract description 7
- 229940079593 drug Drugs 0.000 abstract description 3
- 230000007774 longterm Effects 0.000 abstract description 2
- 229940080818 propionamide Drugs 0.000 abstract 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 16
- 150000001875 compounds Chemical class 0.000 description 13
- 238000002360 preparation method Methods 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 12
- MFRIHAYPQRLWNB-UHFFFAOYSA-N sodium tert-butoxide Chemical compound [Na+].CC(C)(C)[O-] MFRIHAYPQRLWNB-UHFFFAOYSA-N 0.000 description 10
- 229910052757 nitrogen Inorganic materials 0.000 description 9
- -1 methane amide Chemical class 0.000 description 7
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- 239000003905 agrochemical Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000000376 reactant Substances 0.000 description 5
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 4
- 238000005160 1H NMR spectroscopy Methods 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 4
- 239000002244 precipitate Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 239000006200 vaporizer Substances 0.000 description 4
- YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 description 3
- 102000004160 Phosphoric Monoester Hydrolases Human genes 0.000 description 3
- 108090000608 Phosphoric Monoester Hydrolases Proteins 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 125000000623 heterocyclic group Chemical group 0.000 description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 3
- LPNYRYFBWFDTMA-UHFFFAOYSA-N potassium tert-butoxide Chemical group [K+].CC(C)(C)[O-] LPNYRYFBWFDTMA-UHFFFAOYSA-N 0.000 description 3
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 3
- XLPJNCYCZORXHG-UHFFFAOYSA-N 1-morpholin-4-ylprop-2-en-1-one Chemical compound C=CC(=O)N1CCOCC1 XLPJNCYCZORXHG-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 description 2
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 229910052736 halogen Inorganic materials 0.000 description 2
- 150000002367 halogens Chemical class 0.000 description 2
- FQPSGWSUVKBHSU-UHFFFAOYSA-N methacrylamide Chemical compound CC(=C)C(N)=O FQPSGWSUVKBHSU-UHFFFAOYSA-N 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Natural products C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- SWPMNMYLORDLJE-UHFFFAOYSA-N n-ethylprop-2-enamide Chemical compound CCNC(=O)C=C SWPMNMYLORDLJE-UHFFFAOYSA-N 0.000 description 2
- 125000004433 nitrogen atom Chemical group N* 0.000 description 2
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 235000015320 potassium carbonate Nutrition 0.000 description 2
- QLNJFJADRCOGBJ-UHFFFAOYSA-N propionamide Chemical compound CCC(N)=O QLNJFJADRCOGBJ-UHFFFAOYSA-N 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- GHYOCDFICYLMRF-UTIIJYGPSA-N (2S,3R)-N-[(2S)-3-(cyclopenten-1-yl)-1-[(2R)-2-methyloxiran-2-yl]-1-oxopropan-2-yl]-3-hydroxy-3-(4-methoxyphenyl)-2-[[(2S)-2-[(2-morpholin-4-ylacetyl)amino]propanoyl]amino]propanamide Chemical compound C1(=CCCC1)C[C@@H](C(=O)[C@@]1(OC1)C)NC([C@H]([C@@H](C1=CC=C(C=C1)OC)O)NC([C@H](C)NC(CN1CCOCC1)=O)=O)=O GHYOCDFICYLMRF-UTIIJYGPSA-N 0.000 description 1
- QFLWZFQWSBQYPS-AWRAUJHKSA-N (3S)-3-[[(2S)-2-[[(2S)-2-[5-[(3aS,6aR)-2-oxo-1,3,3a,4,6,6a-hexahydrothieno[3,4-d]imidazol-4-yl]pentanoylamino]-3-methylbutanoyl]amino]-3-(4-hydroxyphenyl)propanoyl]amino]-4-[1-bis(4-chlorophenoxy)phosphorylbutylamino]-4-oxobutanoic acid Chemical compound CCCC(NC(=O)[C@H](CC(O)=O)NC(=O)[C@H](Cc1ccc(O)cc1)NC(=O)[C@@H](NC(=O)CCCCC1SC[C@@H]2NC(=O)N[C@H]12)C(C)C)P(=O)(Oc1ccc(Cl)cc1)Oc1ccc(Cl)cc1 QFLWZFQWSBQYPS-AWRAUJHKSA-N 0.000 description 1
- RESPXSHDJQUNTN-UHFFFAOYSA-N 1-piperidin-1-ylprop-2-en-1-one Chemical class C=CC(=O)N1CCCCC1 RESPXSHDJQUNTN-UHFFFAOYSA-N 0.000 description 1
- DLFVBJFMPXGRIB-UHFFFAOYSA-N Acetamide Chemical compound CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 1
- SUAKHGWARZSWIH-UHFFFAOYSA-N N,N‐diethylformamide Chemical compound CCN(CC)C=O SUAKHGWARZSWIH-UHFFFAOYSA-N 0.000 description 1
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical class CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 1
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- RWRDLPDLKQPQOW-UHFFFAOYSA-N Pyrrolidine Chemical compound C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 125000003545 alkoxy group Chemical group 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- 230000009435 amidation Effects 0.000 description 1
- 238000007112 amidation reaction Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229940125773 compound 10 Drugs 0.000 description 1
- 229940125797 compound 12 Drugs 0.000 description 1
- 229940125782 compound 2 Drugs 0.000 description 1
- 229940126214 compound 3 Drugs 0.000 description 1
- 229940125898 compound 5 Drugs 0.000 description 1
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000005265 dialkylamine group Chemical group 0.000 description 1
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 125000005448 ethoxyethyl group Chemical group [H]C([H])([H])C([H])([H])OC([H])([H])C([H])([H])* 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000001183 hydrocarbyl group Chemical group 0.000 description 1
- ZLVXBBHTMQJRSX-VMGNSXQWSA-N jdtic Chemical compound C1([C@]2(C)CCN(C[C@@H]2C)C[C@H](C(C)C)NC(=O)[C@@H]2NCC3=CC(O)=CC=C3C2)=CC=CC(O)=C1 ZLVXBBHTMQJRSX-VMGNSXQWSA-N 0.000 description 1
- 125000004184 methoxymethyl group Chemical group [H]C([H])([H])OC([H])([H])* 0.000 description 1
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 125000004573 morpholin-4-yl group Chemical group N1(CCOCC1)* 0.000 description 1
- OVHHHVAVHBHXAK-UHFFFAOYSA-N n,n-diethylprop-2-enamide Chemical compound CCN(CC)C(=O)C=C OVHHHVAVHBHXAK-UHFFFAOYSA-N 0.000 description 1
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N n-Octanol Natural products CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- YRVUCYWJQFRCOB-UHFFFAOYSA-N n-butylprop-2-enamide Chemical compound CCCCNC(=O)C=C YRVUCYWJQFRCOB-UHFFFAOYSA-N 0.000 description 1
- KERBAAIBDHEFDD-UHFFFAOYSA-N n-ethylformamide Chemical compound CCNC=O KERBAAIBDHEFDD-UHFFFAOYSA-N 0.000 description 1
- 125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 125000005936 piperidyl group Chemical group 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- BDAWXSQJJCIFIK-UHFFFAOYSA-N potassium methoxide Chemical compound [K+].[O-]C BDAWXSQJJCIFIK-UHFFFAOYSA-N 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000017550 sodium carbonate Nutrition 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001052 transient effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C233/04—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
- C07C233/05—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C235/00—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms
- C07C235/02—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton
- C07C235/04—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C235/06—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton the carbon skeleton being acyclic and saturated having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
- C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
Abstract
Description
Claims (3)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/JP2005/000290 WO2006075373A1 (ja) | 2005-01-13 | 2005-01-13 | β−アルコキシプロピオンアミド類、溶剤、洗浄剤および液状薬剤組成物、並びにβ−アルコキシプロピオンアミド類の製造方法 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201010601400XA Division CN102134203B (zh) | 2005-01-13 | 2005-01-13 | β-烷氧基丙酰胺类、溶剂、洗涤剂和液态药物组合物以及β-烷氧基丙酰胺类的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101098851A CN101098851A (zh) | 2008-01-02 |
CN101098851B true CN101098851B (zh) | 2011-02-23 |
Family
ID=36677409
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2005800465154A Active CN101098851B (zh) | 2005-01-13 | 2005-01-13 | β-烷氧基丙酰胺类、溶剂、洗涤剂和液态药物组合物以及β-烷氧基丙酰胺类的制备方法 |
Country Status (4)
Country | Link |
---|---|
JP (1) | JPWO2006075373A1 (zh) |
KR (1) | KR101114711B1 (zh) |
CN (1) | CN101098851B (zh) |
WO (1) | WO2006075373A1 (zh) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101304723B1 (ko) * | 2006-08-22 | 2013-09-05 | 동우 화인켐 주식회사 | 아미드계 화합물을 포함하는 포토레지스트 박리액 및 이를이용한 박리 방법 |
JP5233028B2 (ja) * | 2006-12-19 | 2013-07-10 | ライオン株式会社 | 液体洗浄剤組成物用洗浄溶剤 |
FR2930774B1 (fr) | 2008-04-30 | 2010-09-17 | Rhodia Operations | Composes de type ether-amide, procede de preparation et utilisation |
JP5568863B2 (ja) * | 2009-01-21 | 2014-08-13 | 東洋インキScホールディングス株式会社 | β−アルコキシプロピオンアミド類を使用した水性インキ組成物 |
JP5716260B2 (ja) * | 2009-02-06 | 2015-05-13 | 東洋インキScホールディングス株式会社 | 非水性インキ組成物 |
EP2664610A1 (en) * | 2009-05-01 | 2013-11-20 | Idemitsu Kosan Co., Ltd | Method for producing alpha,beta-unsaturated carboxylic acid-N,N-disubstituted amide and method for producing 3-alkoxycarboxylic acid-N,N-disubstituted amide |
ES2700778T3 (es) | 2009-07-31 | 2019-02-19 | Basf Se | Composición líquida que contienen un pesticida, un tensioactivo no iónico y una propionamida |
JP5499344B2 (ja) * | 2009-09-28 | 2014-05-21 | 大日本塗料株式会社 | 水性インク組成物 |
JP5574099B2 (ja) | 2010-05-26 | 2014-08-20 | セイコーエプソン株式会社 | インクジェット捺染用インク組成物およびインクジェット捺染方法 |
JP2011246571A (ja) | 2010-05-26 | 2011-12-08 | Seiko Epson Corp | インクジェット記録用非水系インク組成物およびインクジェット記録方法 |
JP5513994B2 (ja) * | 2010-06-01 | 2014-06-04 | 出光興産株式会社 | 洗浄剤組成物及びそれを用いたエアゾール組成物 |
FR2961205B1 (fr) * | 2010-06-09 | 2012-06-29 | Rhodia Operations | Procede de preparation de composes esteramides |
JP5700195B2 (ja) | 2010-09-03 | 2015-04-15 | セイコーエプソン株式会社 | インクジェット記録用非水系インク組成物、インクセット、およびインクジェット記録方法 |
JP5793909B2 (ja) * | 2011-03-29 | 2015-10-14 | セイコーエプソン株式会社 | インクジェット用非水系インク組成物およびインクジェット記録方法 |
EP2703464A4 (en) * | 2011-04-25 | 2014-11-19 | Asahi Glass Co Ltd | HYDROFUGE AGENT AND OLEO-REPELLENT COMPOSITION, PROCESS FOR PRODUCING THE SAME, AND ARTICLE CONTAINING THE SAME |
KR20140022391A (ko) * | 2011-04-27 | 2014-02-24 | 아사히 가라스 가부시키가이샤 | 발수발유제 조성물, 그 제조 방법 및 물품 |
KR101892775B1 (ko) | 2011-04-27 | 2018-08-28 | 에이지씨 가부시키가이샤 | 발수발유제 조성물, 그 제조 방법 및 물품 |
JP5804532B2 (ja) * | 2013-12-27 | 2015-11-04 | 大日本塗料株式会社 | 水性インク組成物 |
CN104478749A (zh) * | 2014-11-10 | 2015-04-01 | 平湖优康药物研发有限公司 | 一种新型液晶材料3-丁氧基-n,n-二甲基丙酰胺的合成工艺 |
CN112218531B (zh) * | 2018-05-28 | 2021-10-01 | 日产化学株式会社 | 农药乳化性组合物 |
JP7133838B2 (ja) * | 2018-06-27 | 2022-09-09 | フマキラー株式会社 | 害虫防除組成物、エアゾール剤及びエアゾール製品 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2704280A (en) * | 1951-05-29 | 1955-03-15 | Colgate Palmolive Co | Long-chain aliphatic ether-amides in detergent compositions |
GB1218168A (en) * | 1968-05-10 | 1971-01-06 | Basf Ag | Finishing agent for textile material |
US3712926A (en) * | 1969-04-25 | 1973-01-23 | Basf Ag | Production of n-polyalkoxymethylamides |
US5599947A (en) * | 1993-01-14 | 1997-02-04 | G. D. Searle & Co. | Fatty acid analogs and prodrugs |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5094058A (zh) * | 1973-09-25 | 1975-07-26 | ||
JPH0784427B2 (ja) * | 1987-06-04 | 1995-09-13 | 株式会社トクヤマ | 医・農薬中間原料の製造方法 |
JPH01172367A (ja) * | 1987-12-25 | 1989-07-07 | Tokuyama Soda Co Ltd | オキシアルキルカーバメート化合物の製造方法 |
JP4279088B2 (ja) * | 2003-07-17 | 2009-06-17 | 出光興産株式会社 | β−アルコキシプロピオンアミド類、溶剤、洗浄剤および液状薬剤組成物、並びにβ−アルコキシプロピオンアミド類の製造方法 |
-
2005
- 2005-01-13 KR KR1020077015950A patent/KR101114711B1/ko not_active IP Right Cessation
- 2005-01-13 WO PCT/JP2005/000290 patent/WO2006075373A1/ja not_active Application Discontinuation
- 2005-01-13 JP JP2006552798A patent/JPWO2006075373A1/ja not_active Withdrawn
- 2005-01-13 CN CN2005800465154A patent/CN101098851B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2704280A (en) * | 1951-05-29 | 1955-03-15 | Colgate Palmolive Co | Long-chain aliphatic ether-amides in detergent compositions |
GB1218168A (en) * | 1968-05-10 | 1971-01-06 | Basf Ag | Finishing agent for textile material |
US3712926A (en) * | 1969-04-25 | 1973-01-23 | Basf Ag | Production of n-polyalkoxymethylamides |
US5599947A (en) * | 1993-01-14 | 1997-02-04 | G. D. Searle & Co. | Fatty acid analogs and prodrugs |
Non-Patent Citations (1)
Title |
---|
GB 1218168 A,说明书第1页右栏50-61行. |
Also Published As
Publication number | Publication date |
---|---|
CN101098851A (zh) | 2008-01-02 |
WO2006075373A1 (ja) | 2006-07-20 |
JPWO2006075373A1 (ja) | 2008-06-12 |
KR101114711B1 (ko) | 2012-02-29 |
KR20070100734A (ko) | 2007-10-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101098851B (zh) | β-烷氧基丙酰胺类、溶剂、洗涤剂和液态药物组合物以及β-烷氧基丙酰胺类的制备方法 | |
JP4279088B2 (ja) | β−アルコキシプロピオンアミド類、溶剤、洗浄剤および液状薬剤組成物、並びにβ−アルコキシプロピオンアミド類の製造方法 | |
JPS6181498A (ja) | 過酸および漂白剤活性剤化合物およびクリーニング組成物におけるそれらの用途 | |
US2761874A (en) | Amino derivatives of n-alkyl substituted aspartic acids and their functional derivatives | |
WO2014060852A2 (en) | Compounds useful in the synthesis of benzamide compounds | |
EP3444244B1 (en) | Preparation process for high-purity dabigatran etexilate | |
JP5565677B2 (ja) | 新規ジカルボン酸型化合物 | |
US2381071A (en) | N-phosphono-phosphatoalkyl cyclic amines | |
CN102134203B (zh) | β-烷氧基丙酰胺类、溶剂、洗涤剂和液态药物组合物以及β-烷氧基丙酰胺类的制备方法 | |
CN101939289A (zh) | 用于制备伏立诺他的新方法 | |
CN100376316C (zh) | 一种Gemini表面活性剂 | |
JP5582930B2 (ja) | 抗菌性カチオン界面活性剤 | |
US2856427A (en) | Substituted glycinamides | |
CN103113408A (zh) | 一种制备磷霉素左磷右胺盐的新方法 | |
US2789976A (en) | Nu-carboxyalkyl hexityl amines | |
RU2809166C2 (ru) | Способ получения органосульфатных солей сложных эфиров аминокислот | |
US3059029A (en) | Process for alkyl and aralkyl biguanides | |
JP2009102653A (ja) | β−アルコキシプロピオンアミド類を含む溶剤および洗浄剤 | |
CN108623577B (zh) | 阿莫奈韦及其中间体的制备方法 | |
PL207345B1 (pl) | Nowe N-[2-(alkoksykarbonylo)etylo]-N-alkilo-1-amino-1-dezoksy-D-glucitole i sposób ich wytwarzania | |
US862675A (en) | Orthodioxyphenylethanolamin. | |
US921944A (en) | Alkyl esters of methylene citric acid. | |
EP0060712A1 (en) | Alpha-oxyalkylene amine oxide compounds and their use in detergent compositions | |
US2719862A (en) | Substituted glycinamides | |
PL237059B1 (pl) | Sposób otrzymywania 2-hydroksypropanosulfonianów [(3-alkanoilo metyloamino)propylo] dimetyloamoniowych |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20170125 Address after: Dezhou City, Qingyun Province East Ring Road, No. 1689, No. Patentee after: Yamato Nobutoshimegumi Chemical Group Co.,Ltd. Address before: Tokyo, Japan Patentee before: IDEMITSU KOSAN Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20190829 Address after: 253700 Donghuan Road 1689, Qingyun County, Dezhou City, Shandong Province Patentee after: SHANDONG QINGYUN CHANGXIN CHEMICAL SCIENCE-TECH Co.,Ltd. Address before: 253700 Donghuan Road 1689, Qingyun County, Dezhou City, Shandong Province Patentee before: Yamato Nobutoshimegumi Chemical Group Co.,Ltd. |
|
CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: 253700 No. 1689 East Ring Road, Qingyun County, Shandong, Dezhou Patentee after: Shandong Changxin Chemical Technology Co.,Ltd. Address before: 253700 No. 1689 East Ring Road, Qingyun County, Shandong, Dezhou Patentee before: SHANDONG QINGYUN CHANGXIN CHEMICAL SCIENCE-TECH Co.,Ltd. |