CN100580491C - Capillary pipe optical fibre light forceps and its manufacture method - Google Patents

Capillary pipe optical fibre light forceps and its manufacture method Download PDF

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CN100580491C
CN100580491C CN200810136912A CN200810136912A CN100580491C CN 100580491 C CN100580491 C CN 100580491C CN 200810136912 A CN200810136912 A CN 200810136912A CN 200810136912 A CN200810136912 A CN 200810136912A CN 100580491 C CN100580491 C CN 100580491C
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capillary
optical fiber
sandwich layer
cone
fiber
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CN101339274A (en
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苑立波
杨军
张涛
耿涛
戴强
田凤军
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Harbin Engineering University
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Harbin Engineering University
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Abstract

The invention provides a capillary fiber optical tweezers and a manufacturing method thereof. One end of the hollow capillary fiber with an annular core layer is processed with a cone which causes the emergent light to form an annular pyramidal decussation light field; a small hole is opened on one side of the middle of the hollow capillary optical fiber with the annular core layer; the small hole is connected with a barometric pressure adjusting device and the other end of the hollow capillary optical fiber with the annular core layer is welded with a standard solid optical fiber; the standard solid optical fiber and the hollow capillary optical fiber with the annular core layer are integrated into a whole by drawing the welding position into a conical transition region. In the capillary fiber optical tweezers of the invention, the capillary provides a storage location for micro particles; on one hand, the captured micro particles can be stored in the capillary through the micro negative pressure absorption function in the capillary; on the other hand, the micro particles can be supplied to a fiber-end tweezers through micro positive pressure, thus realizing the operation of continuous assembly of a large amount of micro particles.

Description

Capillary pipe optical fibre light forceps and preparation method thereof
(1) technical field
What the present invention relates to is a kind of smooth tweezer, particularly a kind of light tweezer based on the toroidal cores capillary fiber.The present invention also relates to a kind of preparation method of smooth tweezer.
(2) background technology
The light tweezer is meant the instrument that fine particle was captured and handled to the gradient force that utilizes light intensity distributions and light scattering power.Since Askin[A.Ashkin in 1986, J.M.Dziedzic, J.E.Bjorkholm, and S.Chu, Observation of a single-beam gradient force optical trap for dielectric particles, Opt.Lett.11,288-290,1986] single beam laser is introduced high-NA objective and formed the three-dimensional optical potential well, after having realized three dimensions control to particle, optical tweezer technology develops by leaps and bounds becomes important investigative technique means, and has promoted the fast development of some crossing domains.For example: fine particle catch and the fields such as assembling of carrying, skin ox level force measurement, micromechanics and micro element are widely used.At life science, optical tweezer technology is contactless with it, the intrinsic propesties of lossless detection has shown its impayable advantage especially, has brought into play enormous function for the manipulation that promotes development of life science and little life entity.The particle size that the light tweezer is captured can be rigid particles from several nanometers to tens micron, also can be soft material grains; Can be abiotic particle, also can be active somatic cell or virus.
Tradition light tweezer normally makes up based on optical microscope system, and it focuses on laser beam by microcobjective, utilizes near the gradient field of force of focusing center to form ligh trap, and fine particle is caught and handled.Tradition optical tweezer technology maturation, but its complex structure and shortage are flexible, bulky, cost an arm and a leg, and ligh trap mobile system complexity, operative skill requires high.For this reason, optical waveguide optical tweezer technology scheme has been proposed, realize [Lu Si, Yang Changxi, the Zhou Zhaoying of catching of fine particle by means of a plurality of waveguide channels on same block of material matrix, optical waveguide optical spanner system, Chinese invention patent, publication number CN1740831A], to have a volume bigger in view of this optical waveguide optical tweezer end, the big deficiency of preparation difficulty, people have further developed optical fiber optical tweezers technology [A.Constable, J.Kim, J.Mervis, F.Zarinetchi, and M.Prentiss, Demonstration of a fiber-opticallight-force trap, Opt.Lett.18,1867-1869,1993; Zhihai Liu, Chengkai Guo, JunYang, and Libo Yuan, Tapered fiber optical tweezers for microscopic particletrapping:fabrication and application, Optics Express, 14 (25), 12510-12516,2006].Optical fiber optical tweezers is simple in structure, can make the miniature probe form, and ligh trap and manipulation thereof separate with optical microscope system, so the ligh trap manoeuvrable, and degree of freedom in system is big.There is the comparatively advanced optical fiber optical tweezers technology of several technology in the existing technology formerly, as: the end surface grinding of two single-mode fibers is become cone, at hemisphere face of the most advanced and sophisticated formation of cone, make outgoing beam have the weak focusing characteristic, become certain optical axis included angle to place these two optical fiber, the ligh trap that the overlapping light field forms can be realized capture particles and suspension [E.R.Lyons and G.J.Sonek, Confinement and bistability in a tapered hemispherically lensed optical fiber trap, Appl.Phys.Lett.66,1584-1586,1995]; Publication number is the patent of invention of CN 1963583A becomes to have parabolic microstructure with an end melting and pulling of one section optical fiber an optical fiber pin.With laser coupled in the other end of optical fiber, the light field that converges that laser forms at optical fiber pin front end after the outgoing of optical fiber pin less than 1 micron waist spot diameter, can form stable three-dimensional light potential well, thereby realize single fiber optical tweezers [Liu Zhihai, the garden vertical wave, Yang Jun, the melting and pulling of parabolic microstructure single fiber optical tweezers is made method, Chinese patent, publication number CN 1963583A]; The Chinese invention patent of publication number CN101118300 has provided a kind of small core diameter ultra-high numerical aperture cone optical fiber optical tweezers and preparation method thereof.It adopts small core diameter ultra-high numerical aperture optical fiber to process, and its optical fiber end is ground into cone shape.Disperse light field and can form bigger light field gradient force potential well owing to what the large-numerical aperture of this fiber optic tip formed, thereby can overcome the deadweight of particle, realize single fiber three-dimensionally capturing [garden vertical wave, Yang Jun to fine particle, Liu Zhihai, the ultra-high numerical aperture cone optical fiber optical tweezers technology].For the further attitude to the fine particle of being caught is controlled, publication number is to have provided a kind of twin-core fiber light tweezer [garden vertical wave again in the Chinese invention patent file of CN101149449; Liu Zhihai; Yang Jun is used for twin-core single fiber optical tweezers of capturing minute particle and preparation method thereof].
Although the above-mentioned technology formerly that constitutes the light tweezer by optical fiber has certain advantage, but still comes with some shortcomings.For example, for the particle of catching, deposit nowhere.For quantity bigger a plurality of particle carryings and assembling task, it handles with efficiency of assembling low.
(3) summary of the invention
The object of the present invention is to provide a kind of particle that not only can catch, but also can deposit particle, be more suitable in the capillary pipe optical fibre light forceps of the bigger a plurality of particles carryings of quantity performed with the assembling task.The present invention also aims to provide a kind of method for making of capillary pipe optical fibre light forceps.
The object of the present invention is achieved like this:
Capillary pipe optical fibre light forceps of the present invention comprises one section capillary hollow optical fiber with annular sandwich layer, be processed with at an end of capillary hollow optical fiber and make emergent light form annular cone to intersect the cone of light field with annular sandwich layer, one side has an aperture at the middle part of the capillary hollow optical fiber with annular sandwich layer, and this aperture is connected with a maintenance unit, the other end at the capillary hollow optical fiber with annular sandwich layer is welded with a segment standard solid core fibres, and the standard solid core fibres fuses by weld is drawn the cone zone of transition that forms with the capillary hollow optical fiber with annular sandwich layer.
Capillary pipe optical fibre light forceps of the present invention can also comprise:
1, the quartz of the refractive index ratio capillary wall of the leaded light of described capillary hollow optical fiber with annular sandwich layer annular sandwich layer or glass material are slightly high, and the leaded light sandwich layer is positioned at capillary tube inner wall or is positioned at the kapillary outer wall or is in the centre of capillary wall.
2, the semi-cone angle of described capillary hollow optical fiber one end with the annular sandwich layer cone of processing is between 10 °~80 ° degree.
3, described standard solid core fibres is multimode optical fiber or single-mode fiber.
The method for making of capillary pipe optical fibre light forceps of the present invention is:
1, one section end with capillary hollow optical fiber of annular sandwich layer is processed into cone, makes emergent light form annular cone intersection light field; 2, open an aperture in the middle part of capillary hollow optical fiber one side, and install a maintenance unit additional with annular sandwich layer; 3, at the other end of capillary hollow optical fiber, weld, and weld is drawn into the cone zone of transition by the method that adds the hot-drawn awl with a segment standard solid core fibres with annular sandwich layer.
The method for making of capillary pipe optical fibre light forceps of the present invention can also comprise:
1, describedly one section end with capillary hollow optical fiber of annular sandwich layer is processed into cone processes by precise finiss or chemical corrosion method or deep ultraviolet laser micro-processing technology.
2, describedly open an aperture in the middle part of capillary hollow optical fiber one side and process by precise finiss method or deep ultraviolet laser micro-processing technology with annular sandwich layer.
3, described weld is drawn into cone by the method that adds hot-drawn awl, used heating means are hydrogen-oxygen combustion or CO 2Any of laser instrument or electric arc or high temperature resistance.
The present invention is directed to the deficiencies in the prior art and defective, proposed a kind of light tweezer based on the toroidal cores capillary fiber.This optical fiber optical tweezers is on the basis of toroidal cores capillary fiber, by attrition process to optical fiber end, utilize outside refraction or internal reflection and the symphyogenetic mode of outside refraction, make the light field of toroidal cores capillary fiber outgoing can converge the intersection light cone combined light field that forms annular.The taper of this light field crosses to distinguish and has constituted a photo potential trap, utilizes this potential well can realize the operations such as catching, move of fine particle in three dimensions.It is last with combining of capillary function that the major advantage of this optical fiber optical tweezers is embodied in optical fiber optical tweezers, kapillary provides a storage for fine particle, this makes that the fine particle that the light tweezer is captured can be stored in the kapillary by the little negative-pressure adsorption effect in the kapillary on the one hand; On the other hand, the fine particle that is stored in the kapillary also can offer fine end light tweezer by pressure-fired, finishes a large amount of fine particles are implemented the manipulation of assembling continuously.For example, in the process of cell operation and sorting and cleaning, other light tweezer can't be realized active somatic cell is transported under the disengaging liquid environment, and capillary pipe optical fibre light forceps proposed by the invention is because compound kapillary memory storage, thereby can realize the carrying of active somatic cell under the different liquids environment.Another advantage of this optical fiber optical tweezers is: its 3 D captured power is big, thereby, for the fine particle of same size, do not need very powerful light source can realize Three dimensional steerable.Not only reduced greatly by light source and cause light tweezer tip temperature to rise, and weakened the disturbance of localized heat convection current the fine particle that captures to the influence of the little life of live body.Reduce the cost of system, improved the stability of system.
Major technique of the present invention is characterised in that: (1) this optical fiber optical tweezers is on the basis of one section capillary hollow optical fiber with annular sandwich layer, and an end of optical fiber is processed into cone, makes emergent light form annular cone and intersects light field; (2) have an aperture in the middle part of capillary hollow optical fiber one side, and be connected, be used for the fine particle in the capillary fiber is applied a small malleation or negative pressure with a maintenance unit with annular sandwich layer; (3) at the other end of the capillary hollow optical fiber with annular sandwich layer, weld with a segment standard solid core fibres, and weld is drawn into the cone zone of transition, feasible light source from standard fiber can be injected in the annular sandwich layer of capillary hollow optical fiber.
(4) description of drawings
Fig. 1-a is a kind of capillary fiber cross-sectional view with toroidal cores structure, and its annular leaded light sandwich layer is positioned at capillary tube inner wall.Wherein 1 is the capillary fiber matrix, is lower quartz of refractive index or glass; 2 are the disc waveguide fiber cores; The 3rd, cavity capillaceous.
Fig. 1-b is the capillary fiber cross-sectional view that another kind has the toroidal cores structure, and its annular leaded light sandwich layer is positioned in the middle of the capillary wall.Wherein 1 is the capillary fiber matrix, is lower quartz of refractive index or glass; 2 are the disc waveguide fiber cores; The 3rd, cavity capillaceous.
Fig. 2 is that toroidal cores capillary fiber end is ground into the formed refractive capillary pipe optical fibre light forceps of cone synoptic diagram.Wherein 1 is the capillary fiber matrix, is lower quartz of refractive index or glass; 2 are the disc waveguide fiber cores; The 3rd, cavity capillaceous; 4 for grinding to form the optical fiber end of cone; The 5th, expose the fiber cores that is in the annular spread state on the cone surface; The 6th, the outgoing light cone summit that crosses; The 7th, the far field light cone of outgoing.
Fig. 3 is that toroidal cores capillary fiber end is ground into the formed total internal reflection of taper Rotary-table---refractive optical fiber optical tweezers synoptic diagram.Wherein 1 is the capillary fiber matrix, is lower quartz of refractive index or glass; 2 are the disc waveguide fiber cores; The 3rd, cavity capillaceous; 4 for grinding to form the capillary fiber end of cone; The 5th, expose the fiber cores that is in the annular spread state on the cone surface; The 6th, the outgoing light cone summit that crosses; The 7th, the far field light cone of outgoing; The 8th, via the annular light field distributive province that arrives conical hollow Rotary-table upper surface after the conical walls total reflection.
Fig. 4-a is the welding synoptic diagram of toroidal cores capillary fiber and standard single mode or multimode optical fiber.Wherein 1 is the capillary fiber with toroidal cores structure; 2 for being in the fiber cores of annular spread state; 9 is the solder joint place of single-core fiber and toroidal cores optical fiber; 11 is common single-core fiber; 12 light sources for injection.
Fig. 4-b is toroidal cores capillary fiber and standard single mode or the optically-coupled connection diagram of multimode optical fiber after solder joint place process is drawn awl.Wherein 1 is the capillary fiber with toroidal cores structure; 2 for being in the fiber cores of annular spread state; 10 for being drawn into the two optical fiber connection zone of transition of bicone; 11 is common single-core fiber; 12 light sources for injection.
Fig. 5 is the overall scheme of toroidal cores capillary pipe optical fibre light forceps.Wherein 1 is the capillary fiber with toroidal cores structure; 4 for grinding to form the capillary fiber end of cone; 10 for being drawn into the two optical fiber connection zone of transition of bicone; 11 is common single-core fiber; 12 light sources for injection; 13 for passing through the aperture that little processing forms at the capillary fiber sidewall, is connected with a minute-pressure force adjusting device in the external world, is used to control the pressure in the kapillary.
(5) embodiment
For example the present invention is done description in more detail below in conjunction with accompanying drawing:
Embodiment (one):
Fig. 2 has provided the implementation method of a kind of cone optical fiber optical tweezers of the present invention.Its implementation process is as follows:
Step 1, cone is ground: get one section toroidal cores capillary fiber shown in Fig. 1-a, the ducting layer of this optical fiber is positioned at capillary tube inner wall.By means of the bare fiber ends grinding system, the one end is ground to form as shown in Figure 2 cone shape, in order to guarantee can to form cross one another cone-shaped beam after emergent light is through the circular conical surface refraction, semi-cone angle α is controlled at pi/2-arcsin (n Liquid/ n CoreIn the scope of)<α<pi/2.For fiber core refractive index n Core=1.4868, cladding index n Cladding=1.4571 and the residing liquid refractivity n of optical fiber optical tweezers WaterUnder=1.333 the situation, the scope of this semi-cone angle should be controlled between 26.3 °~80 °.
Step 2, cone polishing: place the bare fibre polishing system to polish above-mentioned ground optical fiber cone, after microscopically is qualified through detection, be placed on cleaning, dry for standby in the ultrasonic cleaning tank;
Step 3 is of coupled connections: the other end of the tapered optical fiber for preparing is carried out overlay dispel, cut, weld with single-mode fiber that has the light source tail optical fiber or multimode optical fiber then.Be heated to soft state at solder joint 9 places shown in Fig. 4 (a), draw awl then, and carry out optical power monitoring, when being coupled to luminous power and reaching maximum with toroidal cores optical fiber till;
Step 4, packaging protection: the quartz socket tube of internal diameter overgauge optical fiber or capillary fiber is transferred to 10 places, cone coupled zone shown in Fig. 4 (b), then at quartz socket tube two ends CO 2Laser instrument heating welded seal is perhaps used the epoxide resin package curing, carries out the secondary coating then and finishes Global Macros.
Step 5, capillary fiber and standard fiber is of coupled connections a little and the capillary fiber cone segments between, the employing wavelength is that deep ultraviolet lasers or the femto-second laser of 157nm processed the aperture that diameter is about 20~30 microns at the kapillary sidewall, and this aperture is connected with a minute-pressure force adjusting device.Just finished as shown in Figure 5 have a toroidal cores capillary fiber cone refractive optical fiber optical tweezers.
Embodiment (two):
Fig. 3 has provided the another kind that the present invention provides and has had an implementation method of toroidal cores capillary pipe optical fibre light forceps.Its implementation process is as follows:
Step 1, cone is ground: get one section toroidal cores capillary fiber shown in Fig. 1-b, by means of the bare fiber ends grinding system, the one end is ground to form as shown in Figure 3 cone truncated conical shape, in order to guarantee to form total internal reflection light after emergent light is through the round platform conical surface 4, refraction through cone round platform top end face forms cross one another cone-shaped beam, and semi-cone angle α should be controlled at 0<α<pi/2-arcsin (n Liquid/ n Core) scope in.For fiber core refractive index n Core=1.4868, cladding index n Cladding=1.4571 and the residing liquid refractivity n of optical fiber optical tweezers WaterUnder=1.333 the situation, the scope of this semi-cone angle α should be controlled between 10~26.3 °.
Step 2, cone polishing: place the bare fibre polishing system to polish on above-mentioned ground optical fiber taper round platform, after microscopically is qualified through detection, be placed on cleaning, dry for standby in the ultrasonic cleaning tank;
Step 3 is of coupled connections: the other end of the tapered optical fiber for preparing is carried out overlay dispel, cut, weld with single-mode fiber that has the light source tail optical fiber or multimode optical fiber then.9 places are heated to soft state at the solder joint shown in Fig. 4-a, draw awl then, and carry out optical power monitoring, when being coupled to luminous power and reaching maximum with toroidal cores optical fiber till;
Step 4, packaging protection: the quartz socket tube of internal diameter overgauge optical fiber or capillary fiber is transferred to 10 places, cone coupled zone shown in Fig. 4-b, then at quartz socket tube two ends CO 2Laser instrument heating welded seal is perhaps used the epoxide resin package curing, carries out the secondary coating then and finishes Global Macros.
Step 5, capillary fiber and standard fiber is of coupled connections a little and the capillary fiber cone segments between, the employing wavelength is that deep ultraviolet lasers or the femto-second laser of 157nm processed the aperture that diameter is about 20~30 microns at the kapillary sidewall, and this aperture is connected with a minute-pressure force adjusting device.Just finished as shown in Figure 5 have a toroidal cores capillary fiber cone refractive optical fiber optical tweezers.

Claims (6)

1, a kind of capillary pipe optical fibre light forceps, it is characterized in that: comprise one section capillary hollow optical fiber with annular sandwich layer, be processed with at an end of capillary hollow optical fiber and make emergent light form annular cone to intersect the cone of light field with annular sandwich layer, one side has an aperture at the middle part of the capillary hollow optical fiber with annular sandwich layer, and this aperture is connected with a maintenance unit, the other end at the capillary hollow optical fiber with annular sandwich layer is welded with a segment standard solid core fibres, the standard solid core fibres fuses by weld is drawn the cone zone of transition that forms with the capillary hollow optical fiber with annular sandwich layer, the quartz or the glass material of the refractive index ratio capillary wall of the leaded light annular sandwich layer of described capillary hollow optical fiber with annular sandwich layer are slightly high, and leaded light annular sandwich layer is positioned at capillary tube inner wall or is positioned at the kapillary outer wall or is in the centre of capillary wall.
2, capillary pipe optical fibre light forceps according to claim 1 is characterized in that: the semi-cone angle of the cone that described capillary hollow optical fiber one end with annular sandwich layer is processed is between 10 °~80 ° degree.
3, capillary pipe optical fibre light forceps according to claim 2 is characterized in that: described standard solid core fibres is multimode optical fiber or single-mode fiber.
4, a kind of method for making of capillary pipe optical fibre light forceps is characterized in that:
(1) one section end with capillary hollow optical fiber of annular sandwich layer is processed into cone, make emergent light form annular cone intersection light field, the quartz of the refractive index ratio capillary wall of the leaded light annular sandwich layer of described capillary hollow optical fiber with annular sandwich layer or glass material is slightly high, the annular sandwich layer of leaded light is positioned at capillary tube inner wall or be positioned at the kapillary outer wall or be in the centre of capillary wall, the described cone that is processed into is by precise finiss or chemical corrosion method or the processing of deep ultraviolet laser micro-processing technology; (2) open an aperture in the middle part of capillary hollow optical fiber one side, and install a maintenance unit additional with annular sandwich layer; (3) at the other end of capillary hollow optical fiber, weld, and weld is drawn into the cone zone of transition by the method that adds the hot-drawn awl with a segment standard solid core fibres with annular sandwich layer.
5, the method for making of capillary pipe optical fibre light forceps according to claim 4 is characterized in that: describedly open an aperture in the middle part of the capillary hollow optical fiber with annular sandwich layer one side and process by precise finiss method or deep ultraviolet laser micro-processing technology.
6, the method for making of capillary pipe optical fibre light forceps according to claim 4 is characterized in that: described weld is drawn into cone by the method that adds hot-drawn awl, used heating means are any of hydrogen-oxygen combustion or CO2 laser instrument or electric arc or high temperature resistance.
CN200810136912A 2008-08-13 2008-08-13 Capillary pipe optical fibre light forceps and its manufacture method Expired - Fee Related CN100580491C (en)

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