CN100560272C - 一种焊锡膏及其制备方法 - Google Patents
一种焊锡膏及其制备方法 Download PDFInfo
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- CN100560272C CN100560272C CNB2007100311250A CN200710031125A CN100560272C CN 100560272 C CN100560272 C CN 100560272C CN B2007100311250 A CNB2007100311250 A CN B2007100311250A CN 200710031125 A CN200710031125 A CN 200710031125A CN 100560272 C CN100560272 C CN 100560272C
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- solder
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- 229910000679 solder Inorganic materials 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 238000003466 welding Methods 0.000 claims abstract description 36
- 239000000843 powder Substances 0.000 claims abstract description 34
- 239000004094 surface-active agent Substances 0.000 claims abstract description 23
- 150000007524 organic acids Chemical class 0.000 claims abstract description 22
- 229910045601 alloy Inorganic materials 0.000 claims abstract description 21
- 239000000956 alloy Substances 0.000 claims abstract description 21
- 239000011347 resin Substances 0.000 claims abstract description 21
- 229920005989 resin Polymers 0.000 claims abstract description 21
- 239000003960 organic solvent Substances 0.000 claims abstract description 19
- 238000006243 chemical reaction Methods 0.000 claims description 40
- 239000000463 material Substances 0.000 claims description 21
- 239000010949 copper Substances 0.000 claims description 18
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 12
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 10
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- LVHBHZANLOWSRM-UHFFFAOYSA-N itaconic acid Chemical compound OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 claims description 9
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 8
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 8
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims description 8
- 239000004359 castor oil Substances 0.000 claims description 8
- 235000019438 castor oil Nutrition 0.000 claims description 8
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 8
- 239000002202 Polyethylene glycol Substances 0.000 claims description 6
- 229920001223 polyethylene glycol Polymers 0.000 claims description 6
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 5
- 235000021314 Palmitic acid Nutrition 0.000 claims description 5
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 4
- RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 claims description 4
- CUDYYMUUJHLCGZ-UHFFFAOYSA-N 2-(2-methoxypropoxy)propan-1-ol Chemical compound COC(C)COC(C)CO CUDYYMUUJHLCGZ-UHFFFAOYSA-N 0.000 claims description 4
- FALRKNHUBBKYCC-UHFFFAOYSA-N 2-(chloromethyl)pyridine-3-carbonitrile Chemical compound ClCC1=NC=CC=C1C#N FALRKNHUBBKYCC-UHFFFAOYSA-N 0.000 claims description 4
- SVTBMSDMJJWYQN-UHFFFAOYSA-N 2-methylpentane-2,4-diol Chemical compound CC(O)CC(C)(C)O SVTBMSDMJJWYQN-UHFFFAOYSA-N 0.000 claims description 4
- KBIWNQVZKHSHTI-UHFFFAOYSA-N 4-n,4-n-dimethylbenzene-1,4-diamine;oxalic acid Chemical compound OC(=O)C(O)=O.CN(C)C1=CC=C(N)C=C1 KBIWNQVZKHSHTI-UHFFFAOYSA-N 0.000 claims description 4
- KDVYCTOWXSLNNI-UHFFFAOYSA-N 4-t-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 4
- 239000005711 Benzoic acid Substances 0.000 claims description 4
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 4
- 239000001293 FEMA 3089 Substances 0.000 claims description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- 241001272567 Hominoidea Species 0.000 claims description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Natural products OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 4
- 229910019142 PO4 Inorganic materials 0.000 claims description 4
- 239000001089 [(2R)-oxolan-2-yl]methanol Substances 0.000 claims description 4
- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 claims description 4
- 235000010233 benzoic acid Nutrition 0.000 claims description 4
- 229910052802 copper Inorganic materials 0.000 claims description 4
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims description 4
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims description 4
- 150000004702 methyl esters Chemical class 0.000 claims description 4
- LYGJENNIWJXYER-UHFFFAOYSA-N nitromethane Chemical compound C[N+]([O-])=O LYGJENNIWJXYER-UHFFFAOYSA-N 0.000 claims description 4
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 claims description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 4
- 239000010452 phosphate Substances 0.000 claims description 4
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 4
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 4
- 229940014800 succinic anhydride Drugs 0.000 claims description 4
- BSYVTEYKTMYBMK-UHFFFAOYSA-N tetrahydrofurfuryl alcohol Chemical compound OCC1CCCO1 BSYVTEYKTMYBMK-UHFFFAOYSA-N 0.000 claims description 4
- 235000011187 glycerol Nutrition 0.000 claims description 2
- 229940051250 hexylene glycol Drugs 0.000 claims description 2
- -1 phenmethylol Chemical compound 0.000 claims description 2
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 2
- 229910052709 silver Inorganic materials 0.000 claims description 2
- 239000004332 silver Substances 0.000 claims description 2
- 238000005476 soldering Methods 0.000 abstract description 8
- 238000000034 method Methods 0.000 abstract description 4
- 230000000694 effects Effects 0.000 description 6
- 239000006071 cream Substances 0.000 description 4
- 238000010923 batch production Methods 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 239000002932 luster Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000013008 thixotropic agent Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
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Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CNB2007100311250A CN100560272C (zh) | 2007-10-24 | 2007-10-24 | 一种焊锡膏及其制备方法 |
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CNB2007100311250A CN100560272C (zh) | 2007-10-24 | 2007-10-24 | 一种焊锡膏及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN101143407A CN101143407A (zh) | 2008-03-19 |
CN100560272C true CN100560272C (zh) | 2009-11-18 |
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CNB2007100311250A Expired - Fee Related CN100560272C (zh) | 2007-10-24 | 2007-10-24 | 一种焊锡膏及其制备方法 |
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CN (1) | CN100560272C (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103521948A (zh) * | 2013-10-08 | 2014-01-22 | 无锡华燕新电源有限公司 | 一种胶体动力电池铸焊助焊剂及其制备方法 |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101508061B (zh) * | 2009-03-30 | 2012-10-03 | 汕头市骏码凯撒有限公司 | 用于SnAgCu合金焊锡粉的助焊剂及其制备方法 |
CN101642855B (zh) * | 2009-08-19 | 2012-02-22 | 浙江一远电子材料研究院 | 一种含稀土无卤素Sn-Ag-Cu系焊锡膏 |
CN102166689B (zh) * | 2011-03-30 | 2013-05-22 | 浙江强力焊锡材料有限公司 | 一种无卤素无铅焊锡膏及其所用助焊剂 |
CN102179644B (zh) * | 2011-04-29 | 2012-12-26 | 东莞永安科技有限公司 | 一种助焊剂 |
CN102728817A (zh) * | 2012-05-22 | 2012-10-17 | 山东圣阳电源科技有限公司 | 一种蓄电池铅钙合金极板板栅铸焊用助焊剂配制方法 |
CN102689113B (zh) * | 2012-06-15 | 2014-06-18 | 东莞市剑鑫电子材料有限公司 | 免清洗无残留助焊剂及其制备方法 |
CN103659053B (zh) * | 2012-09-13 | 2016-05-04 | 苏州铜宝锐新材料有限公司 | 一种钎焊用铜焊膏及其制备方法与应用 |
CN103350291A (zh) * | 2013-06-27 | 2013-10-16 | 东莞市和阳电子科技有限公司 | 一种助焊剂 |
CN104084711B (zh) * | 2014-06-20 | 2016-12-28 | 青岛申达众创技术服务有限公司 | 一种无铅焊锡助焊膏 |
CN104275561A (zh) * | 2014-09-17 | 2015-01-14 | 明光市锐创电气有限公司 | 一种环保型无铅助焊膏 |
CN104384753A (zh) * | 2014-09-23 | 2015-03-04 | 明光旭升科技有限公司 | 一种环保型电路板焊接剂 |
CN108098182A (zh) * | 2017-12-18 | 2018-06-01 | 苏州铜宝锐新材料有限公司 | 一种环保抗腐蚀的焊锡膏 |
CN108788521B (zh) * | 2018-06-28 | 2021-08-10 | 广东剑鑫科技股份有限公司 | 一种变压器助焊剂及其制备方法 |
CN111347189A (zh) * | 2020-04-21 | 2020-06-30 | 深圳市唯特偶新材料股份有限公司 | 用于低温烧结工艺的高散热的焊锡膏及其制备方法 |
CN114101972A (zh) * | 2021-10-29 | 2022-03-01 | 江苏正能电子科技有限公司 | 一种高润湿分散性和耐候性的smt焊锡膏及其制备方法 |
CN115781106A (zh) * | 2022-12-27 | 2023-03-14 | 深圳市晨日科技股份有限公司 | 一种低温无卤无铅锡膏及其制备方法 |
-
2007
- 2007-10-24 CN CNB2007100311250A patent/CN100560272C/zh not_active Expired - Fee Related
Non-Patent Citations (2)
Title |
---|
免洗低残留助焊剂的选择与使用. 夏建亭.电子工艺技术,第20卷第1期. 1999 |
免洗低残留助焊剂的选择与使用. 夏建亭.电子工艺技术,第20卷第1期. 1999 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103521948A (zh) * | 2013-10-08 | 2014-01-22 | 无锡华燕新电源有限公司 | 一种胶体动力电池铸焊助焊剂及其制备方法 |
CN103521948B (zh) * | 2013-10-08 | 2015-10-21 | 无锡华燕新电源有限公司 | 一种胶体动力电池铸焊助焊剂及其制备方法 |
Also Published As
Publication number | Publication date |
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CN101143407A (zh) | 2008-03-19 |
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