CN100510063C - Complex enzyme preparation and process for producing offal using the complex enzyme - Google Patents
Complex enzyme preparation and process for producing offal using the complex enzyme Download PDFInfo
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- CN100510063C CN100510063C CNB2005101044436A CN200510104443A CN100510063C CN 100510063 C CN100510063 C CN 100510063C CN B2005101044436 A CNB2005101044436 A CN B2005101044436A CN 200510104443 A CN200510104443 A CN 200510104443A CN 100510063 C CN100510063 C CN 100510063C
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- offal
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- lignoenzyme
- polygalacturonase
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Abstract
This invention relates to the preparation a compound enzyme. Its components and their weight percentages are that lignin enzyme 0.001%-0.5%, pectolase 0.001%-0.5%, cellulose 0.001%-0.5%, amylolytic enzyme 0.001%-0.5%, protease 0.001%-0.5%, esterase 0.001%-0.5% and the else is water. The preparation of producing tobacco stem using this compound enzyme is as follows: Compound enzyme liquid is formed by blending and stirring its components homogeneously according to the proportion, and the tobacco stem is dipped into this compound enzyme liquid. Stem steaming is conducted to destroy enzyme and to promote the reaction of coloration, aroma and taste producing. Smoking result shows that nearly each index of cut stem treated with compound enzyme is significantly higher that control products, such as aroma quality, aroma amount and remaining taste, while odors and irritation property decrease by great extend, with a proportion of 25%-60% and 20%-50%.
Description
Technical field
The present invention relates to production of cigarettes auxiliary and cigarette producing process, specifically be meant a kind of compound enzymic preparation and this prozyme is used for the technology that offal is produced.
Background technology
There are 1,100,000,000 people's smokings in the whole world, account for 22% of whole world population, and China has 3.3 hundred million smokers approximately, accounts for 25% of China's population, accounts for 30% of world's smoking population, and its tobacco volume of production and marketing occupies the hat in the whole world.Therefore, 40 in China industrial trade in, the level of profitability of the tobacco industry is ranked first, Return on Net Assets reaches 27.69%.
Offal or stem are one of important composition compositions in the cigarette composition pipe tobacco; processing good stem can not only increase the filling value of pipe tobacco; reduce the cigarette unit consumption; improve the incendivity of cigarette and the saturating property sent out of flue gas; but also can reduce the tarry matters in smoke amount; improve the color, smell and taste of cigarette, simultaneously, offal also is the important source material of tobacco sheet.Therefore, cigarette enterprise is all paid much attention to the offal Study on Processing Technology.
Show that from existing result of study the stem insufficient fragrance is very low because influence aroma component content such as some important component of cigarette local flavor such as β phenylethyl alcohol, dorinone, the green ketone of leaf, and furfural, phenylacetic aldehyde equal size are very high, xylon gas's weight.In order to overcome these problems, present domestic offal throwing technology just changes the physical behavior of offal, and utilizes interpolation spices that its pungency, assorted gas are covered, and the Chemical Composition of offal does not change.Therefore, utilize prior art to reduce wooden assorted gas and irritating degree very limited.With regard to offal itself, there are the difference of essence in its physical property and chemical composition and tobacco leaf, and the major ingredient of offal is Mierocrystalline cellulose, hemicellulose, xylogen, pectin substance, contains a spot of ester class, starch and protein simultaneously.Its ester class burning easily increases tar content; Mierocrystalline cellulose, xylogen burn to produce when insufficient and easily cause the irritating smell that the smoker chokes and coughs; Xylogen and pectin burning can produce materials such as deleterious methyl alcohol, and have bigger wooden assorted gas; The nitrogenous compound burning easily produces free radical and unique nitrosamine; The xylogen burning easily produces 3,4 benzopyrenes etc.
Summary of the invention
The invention provides a kind of compound enzymic preparation and this prozyme is used for the technology that offal is produced, its main purpose is to reduce tar, irritating smell and other poisonous, deleterious material that existing offal produces by changing the chemical ingredients of offal in combustion processes.
The present invention adopts following technical scheme: a kind of compound enzymic preparation, form by two or more and water in lignoenzyme, polygalacturonase, cellulase, amylase, proteolytic enzyme and the esterase, wherein, the weight percent content of each component in the compound enzymic preparation that becomes by above-mentioned arbitrary formulated in combination is: lignoenzyme 0.001%-0.5%, polygalacturonase 0.001%-0.5%, cellulase 0.001%-0.5%, amylase 0.001%-0.5%, proteinase-10 .001%-0.5%, esterase 0.001%-0.5%, surplus is a water.
Above-mentioned compound enzymic preparation preferably get moiety and weight percent content is: lignoenzyme 0.02%, polygalacturonase 0.02%, cellulase 0.02%, amylase 0.02%, proteinase-10 .02%, esterase 0.02%, surplus are water.
Above-mentioned compound enzymic preparation preferably get moiety and weight percent content is: polygalacturonase 0.03%, cellulase 0.05%, lignoenzyme 0.02%, surplus are water.
The technology that above-mentioned compound enzymic preparation is applied to offal production comprises the steps: 1) described various enzymes and water to be mixed, water temperature is controlled at 45 ℃ ± 9 ℃, and pH value is controlled at 4.4 ± 1.0, stirs to form prozyme liquid; 2) offal is immersed 7-60 second in the above-mentioned prozyme liquid, under 30-40 ℃ of condition, stored 3-20 hour then; 3) offal is steamed the stalk enzyme that goes out under greater than 90 ℃ temperature, promote colour generation, be fragrant, be the flavor reaction.
The present invention can make stalk wax, grease, pectin substance, starch, protein, Mierocrystalline cellulose and the xylogen in the offal partly degrade, and when steaming stalk, the enzyme that not only can effectively go out can promote Maillard reaction between degradation product and esterification etc. simultaneously.So can make that the stem color and luster is more lucid and more lively, sponginess, high resilience, meet the requirement that rolls more.Moreover because variation has taken place for the structure and the composition of offal, physico-chemical property also changes thereupon, and then reaches the purpose that the xylon gas and irritating smell, the improvement that reduce cigarette are inhaled flavor, improved inner quality and exterior quality.The present invention has important and far-reaching meaning to the Sustainable development of making stem technologic improvement, the processing of low-grade tobacco leaf, tobacco sheet processing, sleep and reducing tar and reducing harm, promotion tobacco industry, the health level of improving the smoker.
Specific embodiment
Specific embodiments of the invention one, according to following weight percent each component is mixed: lignoenzyme 0.001%, polygalacturonase 0.001%, cellulase 0.001%, amylase 0.001%, proteinase-10 .001%, esterase 0.001%, water 99.994%, water temperature is controlled at 45 ℃ ± 5 ℃, pH value is controlled at 4.4 ± 0.3, stirs to form prozyme liquid; Offal is immersed 7-30 second in the above-mentioned prozyme liquid, under 30-40 ℃ of condition, stored 3-5 hour then; At last offal is steamed the stalk enzyme that goes out under greater than 90 ℃ temperature, promote colour generation, be fragrant, be the flavor reaction.
After in offal, adding prozyme, prove through repetition test repeatedly, by enzymatic reaction, increased aminocompound, as amino acid, and carbonyl compound, as soluble sugar, senior saturated monohydroxy alcohol and higher fatty acid etc., the reaction substrate of increase Maillard reaction and various esterifications etc. with being effective.
In the present embodiment, in conjunction with and utilized the technical qualification such as processing unit of cigarette enterprise system stem, the research sieve is joined the multi-functional prozyme of biologically active targetedly, handle by the stalk liquid of washing after enzyme-added, an amount of degraded of the unwanted component that produces when offal is burnt or modification, and steam go out enzyme and promote chemical reaction between degradation product or the modifier of stalk by high temperature, reach and regulate the flue gas potential of hydrogen, reduce the flue gas pungency, reduce wooden assorted gas, improve the purpose of stem inner quality and exterior quality.
Because variation has taken place for the chemical structure and the composition of offal, the color, smell and taste of stem also change thereupon.Smoking result shows, in the index of smokeing panel test, and the every index of smokeing panel test of stem after prozyme is handled, all be significantly higher than reference product as fragrance matter, perfume quantity, pleasant impression etc., especially assorted gas and pungency all descend significantly, and assorted gas descends and reaches 25%-60%, and pungency descends and reaches 20%-50%.
Embodiments of the invention two, the weight percent content that is each component in its prozyme liquid with the difference of embodiment one is different, its each component is respectively: lignoenzyme 0.02%, polygalacturonase 0.02%, cellulase 0.02%, amylase 0.02%, proteinase-10 .02%, esterase 0.02%,, water 99.88%.Its technological process is identical with embodiment one.
Embodiments of the invention three, the weight percent content that is each component in its prozyme liquid with the difference of embodiment one is different, its each component is respectively: lignoenzyme 0.5%, polygalacturonase 0.5%, cellulase 0.5%, amylase 0.5%, proteinase-10 .5%, esterase 0.5%,, water 97%.Its technological process is identical with embodiment one.
Embodiments of the invention four are in its prozyme liquid that with the difference of embodiment one each component and weight percent content thereof are different, and its each component is respectively: polygalacturonase 0.03%, cellulase 0.05%, lignoenzyme 0.02%, water 99.9%.Its technological process is identical with embodiment one.
Determining of the selection of above-mentioned various enzymes and content thereof can be determined according to the particular case of selected offal.
Above-mentioned only is several specific embodiment of the present invention, but design concept of the present invention is not limited thereto, and allly utilizes this design that the present invention is carried out the change of unsubstantiality, all should belong to the behavior of invading protection domain of the present invention.
Claims (4)
1, a kind of compound enzymic preparation, form by two or more and water in lignoenzyme, polygalacturonase, cellulase, amylase, proteolytic enzyme and the esterase, wherein, the weight percent content of each component in the compound enzymic preparation that becomes by above-mentioned arbitrary formulated in combination is: lignoenzyme 0.001%-0.5%, polygalacturonase 0.001%-0.5%, cellulase 0.001%-0.5%, amylase 0.001%-0.5%, proteinase-10 .001%-0.5%, esterase 0.001%-0.5%, surplus is a water.
2, a kind of compound enzymic preparation as claimed in claim 1, its preferred moiety and weight percent content are: lignoenzyme 0.02%, polygalacturonase 0.02%, cellulase 0.02%, amylase 0.02%, proteinase-10 .02%, esterase 0.02%, surplus are water.
3, a kind of compound enzymic preparation as claimed in claim 1, its preferred moiety and weight percent content are: polygalacturonase 0.03%, cellulase 0.05%, lignoenzyme 0.02%, surplus are water.
4, the described compound enzymic preparation of claim 1 is applied to the technology that offal is produced, comprises the steps:
1) described various enzymes and water are mixed, water temperature is controlled at 45 ℃ ± 9 ℃, and pH value is controlled at 4.4 ± 1.0, stirs to form prozyme liquid;
2) offal is immersed 7-60 second in the above-mentioned prozyme liquid, under 30-40 ℃ of condition, stored 3-20 hour then;
3) offal is steamed the stalk enzyme that goes out under greater than 90 ℃ temperature, promote colour generation, be fragrant, be the flavor reaction.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005101044436A CN100510063C (en) | 2005-10-28 | 2005-10-28 | Complex enzyme preparation and process for producing offal using the complex enzyme |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005101044436A CN100510063C (en) | 2005-10-28 | 2005-10-28 | Complex enzyme preparation and process for producing offal using the complex enzyme |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1955281A CN1955281A (en) | 2007-05-02 |
| CN100510063C true CN100510063C (en) | 2009-07-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005101044436A Expired - Fee Related CN100510063C (en) | 2005-10-28 | 2005-10-28 | Complex enzyme preparation and process for producing offal using the complex enzyme |
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| CN (1) | CN100510063C (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101711600B (en) * | 2008-10-08 | 2012-04-25 | 武汉达汇创新科技有限公司 | Process for biochemically treating cut stems |
| CN102326857B (en) * | 2011-06-19 | 2013-05-01 | 红云红河烟草(集团)有限责任公司 | Method for improving quality of low-grade tobacco leaf raw material |
| CN102631021B (en) * | 2012-04-08 | 2013-11-27 | 红云红河烟草(集团)有限责任公司 | Two-stage enzyme treatment method for improving smoking quality of cut stems |
| CN102613690A (en) * | 2012-04-08 | 2012-08-01 | 红云红河烟草(集团)有限责任公司 | Method for improving quality of cut stems |
| CN102894472B (en) * | 2012-09-29 | 2014-12-24 | 福建中烟工业有限责任公司 | Method for improving sensory quality of tobacco leaves by using compound enzymic preparation |
| CN102972859A (en) * | 2012-12-27 | 2013-03-20 | 云南瑞升烟草技术（集团）有限公司 | Method for preparing burley tobacco stems into stem particles or strip-shaped stem threads |
| CN103704867B (en) * | 2014-01-02 | 2016-03-23 | 福建中烟工业有限责任公司 | A kind of method improving cut stem quality |
| CN108354217A (en) * | 2018-03-14 | 2018-08-03 | 红云红河烟草(集团)有限责任公司 | Tobacco stem saccharification treatment method |
| CN115161123B (en) * | 2022-07-21 | 2024-05-10 | 陕西中烟工业有限责任公司 | Cleaning agent for cleaning tobacco stems and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3513857A (en) * | 1967-12-26 | 1970-05-26 | Philip Morris Inc | Process for the treatment of tobacco stems |
-
2005
- 2005-10-28 CN CNB2005101044436A patent/CN100510063C/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3513857A (en) * | 1967-12-26 | 1970-05-26 | Philip Morris Inc | Process for the treatment of tobacco stems |
Non-Patent Citations (4)
| Title |
|---|
| 微生物和酶在烟叶发酵中的应用. 杨虹琦等.湖南农业科学，第6卷. 2003 |
| 微生物和酶在烟叶发酵中的应用. 杨虹琦等.湖南农业科学，第6卷. 2003 * |
| 烟草工业中微生物和酶作用的控制与利用. 程彪.烟草科技/烟草工艺，第3期. 1999 |
| 烟草工业中微生物和酶作用的控制与利用. 程彪.烟草科技/烟草工艺，第3期. 1999 * |
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| CN1955281A (en) | 2007-05-02 |
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Granted publication date: 20090708 Termination date: 20211028 |