CN100436398C - 氧化反应的装置及方法 - Google Patents

氧化反应的装置及方法 Download PDF

Info

Publication number
CN100436398C
CN100436398C CNB011210176A CN01121017A CN100436398C CN 100436398 C CN100436398 C CN 100436398C CN B011210176 A CNB011210176 A CN B011210176A CN 01121017 A CN01121017 A CN 01121017A CN 100436398 C CN100436398 C CN 100436398C
Authority
CN
China
Prior art keywords
reactor
inlet tube
gas
parts
inert fluid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB011210176A
Other languages
English (en)
Chinese (zh)
Other versions
CN1328989A (zh
Inventor
S·J·贝克尔
T·C·布里斯托
R·W·克拉克
D·A·科尔曼
D·纽顿
I·A·B·雷德
B·L·威廉斯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BP Chemicals Ltd
Original Assignee
BP Chemicals Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BP Chemicals Ltd filed Critical BP Chemicals Ltd
Publication of CN1328989A publication Critical patent/CN1328989A/zh
Application granted granted Critical
Publication of CN100436398C publication Critical patent/CN100436398C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/24—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons
    • C07C253/26—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons containing carbon-to-carbon multiple bonds, e.g. unsaturated aldehydes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
    • B01J12/007—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor in the presence of catalytically active bodies, e.g. porous plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1818—Feeding of the fluidising gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/24—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00477—Controlling the temperature by thermal insulation means
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00884—Means for supporting the bed of particles, e.g. grids, bars, perforated plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00245—Avoiding undesirable reactions or side-effects
    • B01J2219/00259—Preventing runaway of the chemical reaction
    • B01J2219/00263—Preventing explosion of the chemical mixture
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
CNB011210176A 2000-06-14 2001-06-14 氧化反应的装置及方法 Expired - Fee Related CN100436398C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB0014580.5 2000-06-14
GBGB0014580.5A GB0014580D0 (en) 2000-06-14 2000-06-14 Appatarus and process

Publications (2)

Publication Number Publication Date
CN1328989A CN1328989A (zh) 2002-01-02
CN100436398C true CN100436398C (zh) 2008-11-26

Family

ID=9893674

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB011210176A Expired - Fee Related CN100436398C (zh) 2000-06-14 2001-06-14 氧化反应的装置及方法

Country Status (11)

Country Link
US (1) US20020006368A1 (enExample)
EP (1) EP1163953A3 (enExample)
JP (1) JP2002058989A (enExample)
KR (1) KR100836544B1 (enExample)
CN (1) CN100436398C (enExample)
BR (1) BR0102384A (enExample)
CA (1) CA2349807A1 (enExample)
GB (1) GB0014580D0 (enExample)
GC (1) GC0000288A (enExample)
SG (1) SG100717A1 (enExample)
TW (1) TW541206B (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7547418B2 (en) * 2004-01-23 2009-06-16 Gm Global Technology Operations, Inc. Fluidized-bed reactor system
KR101432549B1 (ko) * 2006-10-18 2014-08-21 미쯔비시 가스 케미칼 컴파니, 인코포레이티드 모노과황산의 제조방법 및 모노과황산 연속 제조장치
JP2009276829A (ja) * 2008-05-12 2009-11-26 Nintendo Co Ltd 情報処理プログラムおよび情報処理装置
JP2014504952A (ja) * 2010-12-29 2014-02-27 アイヴァンホー エナジー インコーポレイテッド 改良された反応器供給ノズル
CN103121953B (zh) * 2011-11-18 2015-07-08 中国石油化工股份有限公司 乙烯气相氧化法醋酸乙烯制备方法
US9587993B2 (en) * 2012-11-06 2017-03-07 Rec Silicon Inc Probe assembly for a fluid bed reactor
US10379637B2 (en) * 2015-01-30 2019-08-13 Logitech Europe S.A. Rotational element enabling touch-like gestures

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0085961A1 (en) * 1982-02-08 1983-08-17 Sterling Drug Inc. An oxygen injection nozzle
CN1121063A (zh) * 1994-06-02 1996-04-24 标准石油公司 乙酸乙烯基酯生产中用于乙烯乙酰氧基化的流化床方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USRE24485E (en) * 1958-06-10 Method of carrying out homogeneous vapor phase reactions
US2654658A (en) * 1948-04-02 1953-10-06 Kellogg M W Co Apparatus for nitration of organic compounds
US2794681A (en) * 1950-01-31 1957-06-04 Voest Ag Nozzle and control assembly for the introduction of fluid material into a heated chamber
US3059913A (en) * 1958-09-29 1962-10-23 Henry J Kaiser Company Cooling systems for devices used in metal refining processes
US3351634A (en) * 1963-07-15 1967-11-07 Chevron Res Method of carrying out exothermic vapor phase chemical reactions
US3411716A (en) * 1966-05-11 1968-11-19 United States Steel Corp Oxygen lance for steelmaking furnaces
US4084958A (en) * 1974-05-20 1978-04-18 Stora Kopparbergs Bergslags Aktiebolag Method of reducing finely grained material containing iron oxides in a fluid bed
US4191539A (en) * 1976-06-07 1980-03-04 Institute Of Gas Technology Method for feeding caking coal particles to a gasifier
SE429898B (sv) * 1980-01-16 1983-10-03 Stora Kopparbergs Bergslags Ab Sett att forhindra pakladdning vid reduktion i flytbedd av finfordelat metalloxidhaltigt material
US4469487A (en) * 1982-09-20 1984-09-04 Bergwerksverband Gmbh Arrangement for and method of dosing fuel in fluidized bed reactor
US4582120A (en) * 1985-01-03 1986-04-15 Ashland Oil, Inc. Apparatus for cooling fluid solid particles in a regeneration system
US5256810A (en) * 1992-10-14 1993-10-26 The Standard Oil Company Method for eliminating nitriding during acrylonitrile production
US5550281A (en) * 1994-06-02 1996-08-27 Cirjak; Larry M. Fluid bed process for the acetoxylation of ethylene in the production of vinyl acetate
KR0169027B1 (ko) * 1995-04-07 1999-03-20 유미꾸라 레이이찌 알파,베타-불포화 니트릴의 제조 방법
FR2734345B1 (fr) * 1995-05-18 1997-06-20 Soudure Autogene Francaise Installation d'alimentation en gaz, equipement de mise en oeuvre d'une flamme la comportant, et detenteur correspondant
DE19847647A1 (de) * 1998-10-15 2000-04-20 Elenac Gmbh Wirbelschichtverfahren und Reaktor zur Behandlung von Katalysatoren und Katalysatorträgern

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0085961A1 (en) * 1982-02-08 1983-08-17 Sterling Drug Inc. An oxygen injection nozzle
CN1121063A (zh) * 1994-06-02 1996-04-24 标准石油公司 乙酸乙烯基酯生产中用于乙烯乙酰氧基化的流化床方法

Also Published As

Publication number Publication date
CN1328989A (zh) 2002-01-02
KR20010112112A (ko) 2001-12-20
GB0014580D0 (en) 2000-08-09
EP1163953A3 (en) 2004-01-14
JP2002058989A (ja) 2002-02-26
EP1163953A2 (en) 2001-12-19
US20020006368A1 (en) 2002-01-17
KR100836544B1 (ko) 2008-06-10
BR0102384A (pt) 2002-04-23
GC0000288A (en) 2006-11-01
CA2349807A1 (en) 2001-12-14
TW541206B (en) 2003-07-11
SG100717A1 (en) 2003-12-26

Similar Documents

Publication Publication Date Title
KR100368517B1 (ko) 액체풀안으로가스를도입하는방법
KR101361889B1 (ko) 산소 주입 방법
US5044932A (en) Nitrogen oxide control using internally recirculated flue gas
US5135387A (en) Nitrogen oxide control using internally recirculated flue gas
KR930004731B1 (ko) 용융욕 속에서 발생한 반응가스의 후연소방법 및 장치
CN100436398C (zh) 氧化反应的装置及方法
KR100810449B1 (ko) 고온 산업 공정에서의 향상된 안전 특성을 가진 장치
EP1194224B1 (en) Sparger for oxygen injection into a fluid bed reactor
CA2184020C (en) Method and apparatus for direct oxygen injection with a reactant stream into a fluidized bed reactor
US5588974A (en) Process, and apparatus, for the injection of preheated oxygen into a high temperature reactor
US4775314A (en) Coal gasification burner
EP1497472B1 (en) Injection of solids into liquids by means of a shrouded supersonic gas jet
KR100390053B1 (ko) 유동층반응기내로반응물스트림과함께산소를직접분사하는방법및장치
JP2005147656A (ja) 燃料希釈方法及び燃料希釈装置
JP2002058989A5 (enExample)
KR100818948B1 (ko) 유동층 반응 방법 및 장치
EP4003582A1 (en) Inherently safe oxygen/hydrocarbon gas mixer
JPS6232185A (ja) 石炭ガス化炉
JPH03204849A (ja) α・β―不飽和ニトリルの製造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20081126