CN100377772C - 具有用于固体床催化剂的过滤器的反应器 - Google Patents

具有用于固体床催化剂的过滤器的反应器 Download PDF

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Publication number
CN100377772C
CN100377772C CNB2003801101391A CN200380110139A CN100377772C CN 100377772 C CN100377772 C CN 100377772C CN B2003801101391 A CNB2003801101391 A CN B2003801101391A CN 200380110139 A CN200380110139 A CN 200380110139A CN 100377772 C CN100377772 C CN 100377772C
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reactor
catalyst
tube
annular space
annulus
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Expired - Fee Related
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Chinese (zh)
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CN1758954A (zh
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P·G·巴兰
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Lyondell Chemical Technology LP
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Lyondell Chemical Technology LP
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
    • B01D29/018—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements ring shaped
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/50—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
    • B01D29/56—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection
    • B01D29/58—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection arranged concentrically or coaxially
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B01J8/009—Membranes, e.g. feeding or removing reactants or products to or from the catalyst bed through a membrane
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0242—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical
    • B01J8/0257—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical in a cylindrical annular shaped bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00805—Details of the particulate material
    • B01J2208/00814—Details of the particulate material the particulate material being provides in prefilled containers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00823—Mixing elements
    • B01J2208/00831—Stationary elements
    • B01J2208/00849—Stationary elements outside the bed, e.g. baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00823—Mixing elements
    • B01J2208/00858—Moving elements
    • B01J2208/00876—Moving elements outside the bed, e.g. rotary mixer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00884—Means for supporting the bed of particles, e.g. grids, bars, perforated plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
CNB2003801101391A 2003-03-10 2003-12-19 具有用于固体床催化剂的过滤器的反应器 Expired - Fee Related CN100377772C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/385,180 2003-03-10
US10/385,180 US7279145B2 (en) 2003-03-10 2003-03-10 Multiphase reactor design incorporating filtration system for fixed--bed catalyst

Publications (2)

Publication Number Publication Date
CN1758954A CN1758954A (zh) 2006-04-12
CN100377772C true CN100377772C (zh) 2008-04-02

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CNB2003801101391A Expired - Fee Related CN100377772C (zh) 2003-03-10 2003-12-19 具有用于固体床催化剂的过滤器的反应器

Country Status (11)

Country Link
US (2) US7279145B2 (enExample)
EP (1) EP1601453B1 (enExample)
JP (1) JP2006513850A (enExample)
KR (1) KR20050106068A (enExample)
CN (1) CN100377772C (enExample)
AT (1) ATE445456T1 (enExample)
AU (1) AU2003300361A1 (enExample)
BR (1) BR0318173A (enExample)
CA (1) CA2514456A1 (enExample)
DE (1) DE60329716D1 (enExample)
WO (1) WO2004080584A1 (enExample)

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KR100798024B1 (ko) * 2006-03-30 2008-01-28 한국생산기술연구원 다층 필름으로부터 알루미늄을 분리하기 위한 반응기
EP1849804A1 (en) * 2006-04-27 2007-10-31 Arkema France Process of free-radical polymerization or crosslinking in the presence of an organic peroxide by an ex situ process
EP1852418A1 (en) 2006-04-27 2007-11-07 Arkema France Process for synthesizing selected organic peroxides
US7748891B2 (en) * 2007-02-27 2010-07-06 Chicago Bridge & Iron Company Liquid storage tank with draft tube mixing system
US7649102B2 (en) * 2008-03-28 2010-01-19 Lyondell Chemical Technology, L.P. Propylene oxide process
US7550610B1 (en) 2008-03-28 2009-06-23 Lyondell Chemical Technology, L.P. Direct epoxidation process
US7541479B1 (en) 2008-05-27 2009-06-02 Lyondell Chemical Technology, L.P. Direct epoxidation process
BRPI0805341B1 (pt) * 2008-12-05 2017-02-07 Petroleo Brasileiro S A - Petrobras reator multifásico multifuncional
US20100174099A1 (en) * 2009-01-05 2010-07-08 Lyondell Chemical Technology, L.P. Propylene oxide reactor gas distribution system
US8167981B2 (en) * 2009-04-21 2012-05-01 Spx Corporation Vacuum filter assembly
US8207360B2 (en) * 2010-01-29 2012-06-26 Lyondell Chemical Technology, L.P. Propylene oxide process
FR2959677B1 (fr) * 2010-05-06 2012-05-18 Inst Francais Du Petrole Paniers amovibles contenant des particules de filtration pour reacteur a lit fixe.
FR2966752B1 (fr) * 2010-11-03 2013-11-01 IFP Energies Nouvelles Dispositif de test de solides mis en forme fonctionnant en phase heterogene
US9222924B1 (en) * 2013-07-30 2015-12-29 E3Tec Service, Llc Differential kinetic test unit
MY184843A (en) * 2015-11-26 2021-04-26 Evonik Operations Gmbh Process for the epoxidation of an olefin
DE102016204717A1 (de) * 2016-03-22 2017-09-28 Siemens Aktiengesellschaft Reaktor zur Durchführung von gleichgewichtslimitierten Reaktionen
DE102016204718A1 (de) 2016-03-22 2017-09-28 Siemens Aktiengesellschaft Reaktor
DE102016210224A1 (de) * 2016-06-09 2017-12-14 Friedrich-Alexander-Universität Erlangen-Nürnberg Reaktor und Verfahren zur Umsetzung von gleichgewichtslimitierten Reaktionen
WO2018039155A1 (en) * 2016-08-24 2018-03-01 The Regents Of The University Of California Selective solid catalyst for tail end of olefin-epoxidation flow reactor
US10308568B2 (en) * 2017-05-01 2019-06-04 Chevron Phillips Chemical Company Lp Selective poisoning of aromatization catalysts to increase catalyst activity and selectivity
US10241014B2 (en) * 2017-07-10 2019-03-26 Cem Corporation Instrument for analytical sample preparation
EP3784644B1 (en) 2018-04-25 2022-03-02 Lyondell Chemical Technology, L.P. Methods and apparatuses for purifying crude propane
CN108940130B (zh) * 2018-07-23 2020-04-24 新奥科技发展有限公司 一种固定床催化反应器
US20200108366A1 (en) * 2018-10-05 2020-04-09 Uop Llc Apparatus for retaining solid material in a radial flow reactor and method of converting hydrocarbons
CN111375353B (zh) * 2018-12-30 2021-06-04 中国石油化工股份有限公司 固定床上流式反应器及其应用
CN109833832B (zh) * 2019-04-08 2024-01-26 江苏扬农化工集团有限公司 一种轴径向hppo固定床反应器
CN110681319B (zh) * 2019-10-10 2020-10-16 潍坊弘润新材料有限公司 引射循环甲醇芳烃甲基化反应生产均四甲苯的系统及工艺
CN110841349B (zh) * 2019-11-26 2024-06-18 中国成达工程有限公司 一种新型byd废催化剂处理系统
CN111676058B (zh) * 2020-06-19 2022-01-07 中耐工程科技有限公司 一种物料流向交替变化的渣油加氢反应器、含有该反应器的渣油加氢系统及其渣油加氢工艺
CN112958013A (zh) * 2021-02-20 2021-06-15 国家能源集团宁夏煤业有限责任公司 固定床反应管和中试装置
CN112973581A (zh) * 2021-02-24 2021-06-18 中国石油化工股份有限公司 一种积垢过滤器、积垢过滤设备和大型固定床反应器
EP4541456A1 (en) * 2023-10-16 2025-04-23 Basf Se Differential recycle reactor
CN118949859B (zh) * 2024-10-09 2024-12-20 浙江长城搅拌设备股份有限公司 具有催化剂的扰流调温结构的反应器
CN118987731B (zh) * 2024-10-18 2025-01-28 天富(江苏)科技有限公司 一种生产磷酸氢二钾用料浆的离心脱水装置

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US4971771A (en) * 1987-05-20 1990-11-20 Haldor Topsoe A/S Modular manifold means for distributing a flow of a gas in a preferably catalytic reactor
US5500199A (en) * 1986-10-22 1996-03-19 Eniricerche S.P.A. Bonded zeolites and process for preparing them
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US6106803A (en) * 1997-07-23 2000-08-22 Degussa-Huls Ag Granulates which contain titanium silicalite-1
EP1117821A1 (en) * 1998-09-28 2001-07-25 The Penn State Research Foundation Mixer systems
US20010022954A1 (en) * 2000-03-15 2001-09-20 Motoaki Sakashita Chemical decontamination liquid decomposing system having catalyst tower and catalyst tower therefor
US6376686B1 (en) * 2001-09-05 2002-04-23 Arco Chemical Technology, L.P. Direct epoxidation process

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Publication number Priority date Publication date Assignee Title
US3998932A (en) * 1972-05-15 1974-12-21 Montedison Fibre S.P.A. Process for the catalytic synthesis of ammonia
US5500199A (en) * 1986-10-22 1996-03-19 Eniricerche S.P.A. Bonded zeolites and process for preparing them
US4971771A (en) * 1987-05-20 1990-11-20 Haldor Topsoe A/S Modular manifold means for distributing a flow of a gas in a preferably catalytic reactor
US5859265A (en) * 1994-07-20 1999-01-12 Basf Aktiengesellschaft Oxidation catalyst, its preparation and oxidation using the oxidation catalyst
WO1998000413A1 (en) * 1996-07-01 1998-01-08 The Dow Chemical Company Process for the direct oxidation of olefins to olefin oxides
US6106803A (en) * 1997-07-23 2000-08-22 Degussa-Huls Ag Granulates which contain titanium silicalite-1
EP1117821A1 (en) * 1998-09-28 2001-07-25 The Penn State Research Foundation Mixer systems
US20010022954A1 (en) * 2000-03-15 2001-09-20 Motoaki Sakashita Chemical decontamination liquid decomposing system having catalyst tower and catalyst tower therefor
US6376686B1 (en) * 2001-09-05 2002-04-23 Arco Chemical Technology, L.P. Direct epoxidation process

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Publication number Publication date
US20040179983A1 (en) 2004-09-16
BR0318173A (pt) 2006-02-21
KR20050106068A (ko) 2005-11-08
US7279145B2 (en) 2007-10-09
DE60329716D1 (de) 2009-11-26
CA2514456A1 (en) 2004-09-23
US7642365B2 (en) 2010-01-05
AU2003300361A1 (en) 2004-09-30
WO2004080584A1 (en) 2004-09-23
EP1601453A1 (en) 2005-12-07
ATE445456T1 (de) 2009-10-15
US20080009657A1 (en) 2008-01-10
JP2006513850A (ja) 2006-04-27
EP1601453B1 (en) 2009-10-14
CN1758954A (zh) 2006-04-12

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