CL2012003376A1 - Proceso para remover lignina de licor negro acidificando el licor negro, en donde el licor negro es oxidado antes de dicha acidificacion para minimizar elazufre reducido total (trs) en el licor negro, de manera que las hemicelulosas sean oxidadas para formar un agente de acidificacion, el cual complementa a dicho acidificante en la acidificacion; proceso para separar lignina de licor negro. - Google Patents
Proceso para remover lignina de licor negro acidificando el licor negro, en donde el licor negro es oxidado antes de dicha acidificacion para minimizar elazufre reducido total (trs) en el licor negro, de manera que las hemicelulosas sean oxidadas para formar un agente de acidificacion, el cual complementa a dicho acidificante en la acidificacion; proceso para separar lignina de licor negro.Info
- Publication number
- CL2012003376A1 CL2012003376A1 CL2012003376A CL2012003376A CL2012003376A1 CL 2012003376 A1 CL2012003376 A1 CL 2012003376A1 CL 2012003376 A CL2012003376 A CL 2012003376A CL 2012003376 A CL2012003376 A CL 2012003376A CL 2012003376 A1 CL2012003376 A1 CL 2012003376A1
- Authority
- CL
- Chile
- Prior art keywords
- black liquor
- acidification
- oxidized
- lignin
- acidifier
- Prior art date
Links
- 230000020477 pH reduction Effects 0.000 title abstract 6
- 229920005610 lignin Polymers 0.000 title abstract 4
- 229920002488 Hemicellulose Polymers 0.000 title abstract 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title abstract 2
- 239000002535 acidifier Substances 0.000 title abstract 2
- 239000003795 chemical substances by application Substances 0.000 title abstract 2
- 229910052717 sulfur Inorganic materials 0.000 title abstract 2
- 239000011593 sulfur Substances 0.000 title abstract 2
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0057—Oxidation of liquors, e.g. in order to reduce the losses of sulfur compounds, followed by evaporation or combustion if the liquor in question is a black liquor
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
- C07G1/00—Lignin; Lignin derivatives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H8/00—Macromolecular compounds derived from lignocellulosic materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Paper (AREA)
- Compounds Of Unknown Constitution (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US35096910P | 2010-06-03 | 2010-06-03 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CL2012003376A1 true CL2012003376A1 (es) | 2013-01-25 |
Family
ID=45063558
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CL2012003376A CL2012003376A1 (es) | 2010-06-03 | 2012-11-30 | Proceso para remover lignina de licor negro acidificando el licor negro, en donde el licor negro es oxidado antes de dicha acidificacion para minimizar elazufre reducido total (trs) en el licor negro, de manera que las hemicelulosas sean oxidadas para formar un agente de acidificacion, el cual complementa a dicho acidificante en la acidificacion; proceso para separar lignina de licor negro. |
Country Status (11)
| Country | Link |
|---|---|
| US (3) | US8771464B2 (enExample) |
| EP (1) | EP2576662B1 (enExample) |
| JP (1) | JP5898677B2 (enExample) |
| CN (1) | CN103154097B (enExample) |
| BR (1) | BR112012030594A2 (enExample) |
| CA (1) | CA2799798C (enExample) |
| CL (1) | CL2012003376A1 (enExample) |
| ES (1) | ES2854725T3 (enExample) |
| PL (1) | PL2576662T3 (enExample) |
| PT (1) | PT2576662T (enExample) |
| WO (1) | WO2011150508A1 (enExample) |
Families Citing this family (71)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2440703B1 (en) * | 2009-06-10 | 2016-02-17 | Valmet Aktiebolag | Method for precipitating lignin from black liquor by utilizing waste gases |
| US9879119B2 (en) | 2009-09-25 | 2018-01-30 | Michael A. Lake | Lignin product and process for making same |
| US9260464B2 (en) * | 2009-09-25 | 2016-02-16 | Michael A. Lake | Process for recovering lignin |
| AT510812A1 (de) * | 2010-10-29 | 2012-06-15 | Annikki Gmbh | Verfahren zur gewinnung von lignin |
| US9790641B2 (en) * | 2011-05-24 | 2017-10-17 | Liquid Lignin Company, Llc | Process for treating lignin |
| CA2839864C (en) * | 2011-06-22 | 2018-06-12 | Metso Power Ab | Method for lignin separation from black liquor comprising multiple acidification steps |
| RS63442B1 (sr) | 2011-12-09 | 2022-08-31 | Upm Kymmene Corp | Postupak za pripremu komponente lignina, komponenta lignina i njena primena i proizvod |
| US9163169B2 (en) | 2012-03-13 | 2015-10-20 | Georgia-Pacific Chemicals Llc | Adhesive compositions having a reduced cure time and methods for making and using same |
| EP2825698B1 (en) * | 2012-03-16 | 2016-10-05 | Valmet Aktiebolag | Method for lignin separation from black liquor |
| BR112014027474B1 (pt) | 2012-05-03 | 2020-03-17 | Virdia, Inc. | Métodos de processamento de materiais lingnocelulósicos |
| US8809426B2 (en) | 2012-05-11 | 2014-08-19 | Cyclewood Solutions, Inc. | Chemical modification of lignin and lignin derivatives |
| FI127010B (en) * | 2012-08-24 | 2017-09-29 | Upm Kymmene Corp | A method for recovering low molecular weight lignin from a filtrate |
| US9586338B2 (en) | 2012-10-01 | 2017-03-07 | Georgia-Pacific Chemicals Llc | Methods for making lignocellulose containing composite products |
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| US9777032B2 (en) * | 2012-10-30 | 2017-10-03 | Cyclewood Solutions, Inc. | Injection of a chemical reagent into a process stream that contains lignin |
| US20140121359A1 (en) * | 2012-10-30 | 2014-05-01 | Blackburn John C | Ph-induced fractionation processes for recovery of lignin |
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| FI20135105A7 (fi) * | 2013-02-04 | 2014-08-05 | Andritz Oy | Menetelmä kemikaalien ja sivutuotteiden talteenottamiseksi korkean sulfiditeetin keittolipeistä |
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| AU2013388054B2 (en) | 2013-05-03 | 2017-09-21 | Virdia, Inc. | Methods for treating lignocellulosic materials |
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| SE1551720A1 (sv) * | 2013-05-29 | 2015-12-29 | Kiram Ab | A method for the treatment of spent pulping liquor for the removal and production of a ligning containing product |
| PL3080138T3 (pl) * | 2013-12-12 | 2021-06-14 | Solenis Technologies, L.P. | Dyspersje nanocząstek ligniny i sposoby ich wytwarzania i stosowania |
| MX375461B (es) | 2013-12-20 | 2025-03-06 | Ecolab Usa Inc | Coadyuvantes que se pueden liberar con puntos de turbidez para procesos de crepeado. |
| WO2015153519A1 (en) | 2014-04-02 | 2015-10-08 | Georgia-Pacific Chemicals Llc | Methods for making lignocellulose composite products with oxidative binders and complexed metal catalyst |
| WO2015153520A1 (en) | 2014-04-02 | 2015-10-08 | Georgia-Pacific Chemicals Llc | Methods for making lignocellulose composite products with oxidative binders and encapsulated catalyst |
| WO2015153517A1 (en) | 2014-04-02 | 2015-10-08 | Georgia-Pacific Chemicals Llc | Methods for making lignocellulose composite products |
| FI127601B (en) * | 2014-04-03 | 2018-10-15 | Andritz Oy | Method for handling spent wash solution of a lignin-recovery process |
| FI126369B (en) * | 2014-06-06 | 2016-10-31 | Andritz Oy | A method for using lignin extracted from black liquor as fuel for a lime kiln |
| JP6687594B2 (ja) * | 2014-07-09 | 2020-04-22 | ヴァーディア, インコーポレイテッド | 黒液からリグニンを分離および精製する方法ならびにその組成物 |
| SE539887C2 (en) * | 2014-10-03 | 2018-01-02 | Stora Enso Oyj | A method to purify lignin from Sulfur by using an electric field |
| KR101521238B1 (ko) * | 2014-11-04 | 2015-05-18 | (재)울산테크노파크 | 흑액으로부터 고순도 리그닌을 추출하는 방법 |
| US20160186067A1 (en) * | 2014-12-30 | 2016-06-30 | Shell Oil Company | Methods and systems for processing cellulosic biomass |
| BR112017022080B1 (pt) | 2015-04-15 | 2022-04-12 | Fpinnovations | Adesivo, método de produção de um adesivo de madeira, e, produto de madeira |
| FI129778B (en) | 2015-06-26 | 2022-08-31 | Teknologian Tutkimuskeskus Vtt Oy | Procedure for activation and precipitation of lignin |
| US10253214B2 (en) | 2015-07-07 | 2019-04-09 | Solenis Technologies, L.P. | Methods for inhibiting the deposition of organic contaminates in pulp and papermaking systems |
| FI128962B (en) * | 2015-11-06 | 2021-04-15 | Teknologian Tutkimuskeskus Vtt Oy | Alkali-O2 oxidized lignin as a dispersant |
| CN109196056A (zh) * | 2016-03-31 | 2019-01-11 | 威斯福林产有限公司 | 包含木浆的纤维素复合材料 |
| RU2741610C2 (ru) | 2016-05-03 | 2021-01-27 | Соленис Текнолоджиз, Л.П. | Биополимерные проклеивающие агенты |
| EP3462908A4 (en) * | 2016-06-07 | 2019-10-30 | FPInnovations Inc. | ANTIMICROBIAL LIGNIN COMPOSITION FROM WOODEN BIO |
| CN106750362B (zh) * | 2016-11-30 | 2019-06-11 | 海南金海浆纸业有限公司 | 一种木质素的分级方法 |
| US11591472B2 (en) | 2016-12-02 | 2023-02-28 | The Williamette Valley Company Llc | Wax-organic extender emulsion and method for manufacture thereof |
| PT3592802T (pt) | 2017-03-09 | 2024-02-05 | Fpinnovations | Processo para produzir um copolímero de lenhina aniónico sob condições aquosas ácidas |
| BR112019018573A2 (pt) | 2017-03-09 | 2020-04-14 | Fpinnovations | métodos para preparar um copolímero de lignina catiônico e de floculação de águas residuais, e, copolímero de lignina catiônico |
| FI129362B (fi) * | 2017-05-16 | 2021-12-31 | Andritz Oy | Menetelmä kemiallisen massan tuottamiseksi |
| CN109485871B (zh) * | 2017-09-09 | 2021-03-05 | 中国石油化工股份有限公司 | 一种高活性酶解木质素及其制备方法 |
| CN108455754B (zh) * | 2018-02-24 | 2022-01-07 | 北京林业大学 | 一种水热酸解用于处理植物原料预水解液的方法 |
| WO2019165443A1 (en) * | 2018-02-26 | 2019-08-29 | The Texas A&M University System | Lignin fractionation and fabrication for quality carbon fiber |
| WO2019241408A1 (en) * | 2018-06-12 | 2019-12-19 | Domtar Paper Company, Llc | Methods and processes for lignin isolation/extraction |
| WO2019241413A1 (en) * | 2018-06-12 | 2019-12-19 | Domtar Paper Company, Llc | Methods and processes for lignin isolation/extraction |
| AT521179B1 (de) | 2018-06-15 | 2019-11-15 | Papierholz Austria Gmbh | Verfahren zur Isolierung von Lignin aus einem alkalischen Prozessstrom |
| CN109054045B (zh) * | 2018-08-13 | 2021-05-07 | 南京工业大学 | 一种亚微米木质素的制备方法 |
| JP6662423B1 (ja) * | 2018-09-06 | 2020-03-11 | 日本製紙株式会社 | リグニンを分離する方法 |
| FI129347B (en) | 2018-10-23 | 2021-12-15 | Teknologian Tutkimuskeskus Vtt Oy | Extraction of valuable components from bark |
| EP3693508A1 (en) | 2019-02-08 | 2020-08-12 | Scitech-service OY | Method for lignin production |
| CN110372883B (zh) * | 2019-08-14 | 2021-01-01 | 南京工业大学 | 一种从黑液中提取木质素和硅酸的方法 |
| US11752660B2 (en) | 2019-08-26 | 2023-09-12 | Walker Industries Holdings Limited | Aqueous wax emulsions and dispersions and uses thereof |
| SE2050074A1 (en) * | 2020-01-28 | 2021-01-29 | Soedra Skogsaegarna Ekonomisk Foerening | Process for producing one, or more, compounds |
| US12234603B2 (en) * | 2020-03-03 | 2025-02-25 | Robert C. Casad, Jr. | High solids alkaline oxidation and biomethane conversion of residual lignin |
| JP2021155661A (ja) * | 2020-03-30 | 2021-10-07 | 日本製紙株式会社 | ソーダリグニンの分離方法 |
| US11866456B2 (en) * | 2020-07-14 | 2024-01-09 | Liquid Lignin Company | Process for treating lignin |
| CN111771454B (zh) * | 2020-08-24 | 2023-09-12 | 山东农业大学 | 一种基于造纸黑液制备的水稻耐盐种子包衣组分及其应用方法 |
| US20240052530A1 (en) * | 2020-08-25 | 2024-02-15 | The Texas A&M University System | Lignin Fractionation and Fabrication for Quality Carbon Fiber |
| RU2756631C1 (ru) * | 2020-10-12 | 2021-10-04 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Санкт-Петербургский государственный университет промышленных технологий и дизайна" | Способ удаления лигноуглеводного комплекса из черного щелока производства сульфатной целлюлозы (3 варианта) |
| SE545888C2 (en) * | 2021-07-15 | 2024-03-05 | Suncarbon Ab | Treating black liquor with bio-oil acids for lignin recovery |
| WO2023015325A1 (en) | 2021-08-06 | 2023-02-09 | Lignorganic (Pty) Ltd | System and method for obtaining lignin and carboxylic acid from byproducts of pulping processes |
| WO2024187276A1 (en) * | 2023-03-14 | 2024-09-19 | Fpinnovations | Improved process for the extraction of kraft lignin from hardwood and eucalyptus black liquors |
| CN116425998A (zh) * | 2023-04-21 | 2023-07-14 | 天津科技大学 | 一种高效分离麦草生物化学机械浆废液中木素的方法 |
| CN116715865A (zh) * | 2023-04-21 | 2023-09-08 | 天津科技大学 | 一种提高麦草生物化学机械浆废液木素产品质量的方法 |
| WO2025043331A1 (en) * | 2023-08-25 | 2025-03-06 | Red Leaf Sustainable Ip Corp. | Apparatus and methods for extracting lignin from non-wood black liquor |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2406867A (en) * | 1943-12-31 | 1946-09-03 | Smith Paper Mills Ltd Howard | Method of treating lignocellulosic material |
| GB664811A (en) * | 1944-08-21 | 1952-01-16 | Smith Paper Mills Ltd Howard | Improvements in the recovery of lignin from black liquor |
| SE8204365L (sv) * | 1981-07-23 | 1983-01-24 | Domtar Inc | Sett for behandling av restlut fran en alkalisk massakokningsprocess av lignocellulosamaterial |
| US4521336A (en) * | 1984-04-16 | 1985-06-04 | Westvaco Corporation | Process for preparing lignosulfonates |
| US4764597A (en) * | 1987-06-15 | 1988-08-16 | Westvaco Corporation | Method for methylolation of lignin materials |
| CA1335976C (en) | 1989-05-31 | 1995-06-20 | Mahmoud Kamran Azarniouch | Recovery of naoh and other values from spent liquors and bleach plant effluents |
| US20030041982A1 (en) * | 2001-08-31 | 2003-03-06 | Prior Eric S. | Organic biomass fractionation process |
| CN1989292A (zh) * | 2004-09-07 | 2007-06-27 | 株式会社K·I系统 | 黑液的处理方法 |
| SE0402201D0 (sv) * | 2004-09-14 | 2004-09-14 | Stfi Packforsk Ab | Method for separating lignin from black liquor |
| SE0402437D0 (sv) * | 2004-10-07 | 2004-10-07 | Stfi Packforsk Ab | Method for separating lignin from a lignin containing liquid/slurry |
| US7699958B2 (en) * | 2006-11-27 | 2010-04-20 | Ut-Battelle, Llc | Method for improving separation of carbohydrates from wood pulping and wood or biomass hydrolysis liquors |
| US9382389B2 (en) * | 2008-02-21 | 2016-07-05 | Valmet Aktiebolag | Method for separating lignin from black liquor, a lignin product, and use of a lignin product for the production of fuels or materials |
| US9260464B2 (en) * | 2009-09-25 | 2016-02-16 | Michael A. Lake | Process for recovering lignin |
-
2011
- 2011-05-31 JP JP2013512709A patent/JP5898677B2/ja active Active
- 2011-05-31 PT PT117890178T patent/PT2576662T/pt unknown
- 2011-05-31 PL PL11789017T patent/PL2576662T3/pl unknown
- 2011-05-31 CA CA2799798A patent/CA2799798C/en active Active
- 2011-05-31 WO PCT/CA2011/000654 patent/WO2011150508A1/en not_active Ceased
- 2011-05-31 EP EP11789017.8A patent/EP2576662B1/en active Active
- 2011-05-31 US US13/118,666 patent/US8771464B2/en active Active
- 2011-05-31 BR BR112012030594A patent/BR112012030594A2/pt not_active Application Discontinuation
- 2011-05-31 CN CN201180027562.XA patent/CN103154097B/zh active Active
- 2011-05-31 ES ES11789017T patent/ES2854725T3/es active Active
-
2012
- 2012-11-30 CL CL2012003376A patent/CL2012003376A1/es unknown
-
2014
- 2014-05-22 US US14/284,558 patent/US8940130B2/en active Active
- 2014-12-16 US US14/571,907 patent/US9091023B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| US20140256920A1 (en) | 2014-09-11 |
| EP2576662A1 (en) | 2013-04-10 |
| JP2013527339A (ja) | 2013-06-27 |
| CN103154097B (zh) | 2017-01-18 |
| US8940130B2 (en) | 2015-01-27 |
| PT2576662T (pt) | 2021-02-16 |
| WO2011150508A1 (en) | 2011-12-08 |
| JP5898677B2 (ja) | 2016-04-06 |
| BR112012030594A2 (pt) | 2016-08-16 |
| EP2576662B1 (en) | 2020-11-18 |
| EP2576662A4 (en) | 2014-09-03 |
| ES2854725T3 (es) | 2021-09-22 |
| PL2576662T3 (pl) | 2021-09-27 |
| US8771464B2 (en) | 2014-07-08 |
| CA2799798A1 (en) | 2011-12-08 |
| CN103154097A (zh) | 2013-06-12 |
| US9091023B2 (en) | 2015-07-28 |
| CA2799798C (en) | 2015-01-20 |
| US20150096697A1 (en) | 2015-04-09 |
| US20110297340A1 (en) | 2011-12-08 |
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