CH303514A - Process for the preparation of a quaternary ammonium compound. - Google Patents

Process for the preparation of a quaternary ammonium compound.

Info

Publication number
CH303514A
CH303514A CH303514DA CH303514A CH 303514 A CH303514 A CH 303514A CH 303514D A CH303514D A CH 303514DA CH 303514 A CH303514 A CH 303514A
Authority
CH
Switzerland
Prior art keywords
quaternary ammonium
ammonium compound
preparation
new
benzyl chloride
Prior art date
Application number
Other languages
German (de)
Inventor
Zuerich Friedrich Seifenfabrik
Original Assignee
Friedrich Steinfels Ag Seifenf
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Friedrich Steinfels Ag Seifenf filed Critical Friedrich Steinfels Ag Seifenf
Publication of CH303514A publication Critical patent/CH303514A/en

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/655—Compounds containing ammonium groups
    • D06P1/66—Compounds containing ammonium groups containing quaternary ammonium groups
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
    • A01N31/12—Bis-chlorophenols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines

Description

       

  <B>Zusatzpatent</B> zum     Hauptpatent    Nr.     301409.       Gegenstand des vorliegenden Patentes ist  ein Verfahren zur Herstellung einer neuen       quaternären        Ammonnumverbindung,    das da  cl'urch gekennzeichnet ist,     da.ss    man     Di        (oxy-          äthyl)        -hexadeeyloxyäthyl-#amin    mit     Benzyl-          ehlorid    zur Reaktion bringt..  



  Das neue kristalline Reaktionsprodukt. löst  sieh in destilliertem und, hartem Wasser voll  ständig     klar        mit,    neutraler Reaktion und un  ter starker     'Schaumbildung.    Es hat, wertvolle       higenschaften        als    Färbe-,     Egalisier-    und       Avivagemittel.    Mit     äubstant.iven    Farbstoffen.

         bildet    es     Komplexverbindungen    und erhöht       to    die     Wasserechtheit        substantiver        Färbun-          ;'en.    Da es     gleichzeitig    ein     Aufziehvermögen     auf die Faser besitzt, kann man es als     sub-          stantives        Avivagemittel    bezeichnen.  



  Ausserdem besitzt. dieser Stoff eine starke  bakterizide und     bakteriostatische    Wirkung  und kann deshalb vorzüglich als     Desinfektions-          mittel        verwendet    werden.         Beispiel:       1     Hol    reines     Di(oxyäthyl)-h        exaeeyloxy-          ithyl-amin    (Kp. 192 bis 198      C/0,02'    mm     1-I-)     wird mit. 1 Moll reinem     Benzylchlorid    ver  mischt und etwa 4 bis 6     ;Stunden.    auf etwa 80  bis     100     C erwärmt.

   Diese Reaktion kann ohne       Zusätze        oder    unter     Verwendung    eines geeig-    nieten     Lösunittels        erfolgen.    Das Reaktions  produkt     kristallisiert    und     wird    vorteilhaft aus       eineue        passenden    Lösungsmittel wie zum     Bei-          spiel        Essigsäi-treäthylester    oder einem     Gemisch          von        Essiggäureäthylester        unid        

  Äthyläther     Es     kristallisiert    in     glänzenden          Blättchen    vom     SchmelzDunkt    85     bis        87     C.



  <B> Additional patent </B> to the main patent No. 301409. The subject of the present patent is a process for the production of a new quaternary ammonium compound, which is characterized by the fact that di (oxy-ethyl) -hexadeeyloxyethyl- # amine reacts with benzyl chloride ..



  The new crystalline reaction product. Dissolves completely clear in distilled and hard water with a neutral reaction and strong foaming. It has valuable properties as a coloring, leveling and softening agent. With constant colorants.

         it forms complex compounds and increases the water fastness of substantive dyes. Since it also has the ability to be absorbed by the fiber, it can be referred to as a substantial softener.



  Also owns. this substance has a strong bactericidal and bacteriostatic effect and can therefore be used as a disinfectant. Example: 1 Hol of pure di (oxyethyl) -h exaeeyloxy-ithyl-amine (bp. 192 to 198 C / 0.02 'mm 1-I-) is mixed with 1 Moll pure benzyl chloride mixed together and about 4 to 6; hours heated to about 80 to 100 C.

   This reaction can take place without additives or with the use of a suitable solvent. The reaction product crystallizes and is advantageously obtained from a suitable solvent such as, for example, ethyl acetate or a mixture of ethyl acetate

  Ethyl ether It crystallizes in shiny flakes with a melting point of 85 to 87 C.

Claims (1)

PATENTANSPRUCH Verfahren zur Herstellung einer neuen quaternären Ammoniumverbindung, d@a@durch gekennzeichnet, idass man Dl (oxyäthyl)-hexa- deeyl.oxyäthyl-amän' mit Benzylchlorid zur Umsetzung bringt. Die neue Verbindhang bildet. glänzende Blättchen vom : PATENT CLAIM Process for the production of a new quaternary ammonium compound, d @ a @ characterized by the fact that Dl (oxyethyl) hexadeeyl.oxyäthylamine is reacted with benzyl chloride. The new connection slope forms. shiny leaves from: Schmelzpunkt 85 bis 87 C. UNTERANSPRZTGHE 1. Verfahren nach Patentanspruch, da durch ,gekennzeichnet, dass man mit äquimo- laren Mengen der Ausgangsstoffe arbeitet. Verfahren nach Patentanspruch und Unteranspruch 1, dadurch gekennzeichnet, Melting point 85 to 87 C. UNTERANSPRZTGHE 1. Process according to claim, characterized in that equimolar amounts of the starting materials are used. Method according to claim and dependent claim 1, characterized in that dass man d'ie quaternäre Ammonäumverbin- clung zur Reinigung umkristallisiert. Verfahren nach Pat.entansprueh und I?nt:eranspruch 1, dadurch gekennzeichnet, dass man in Gegenwart. eines Lösungsmittels arbeitet. that the quaternary ammonium compound is recrystallized for purification. Method according to patent claim 1, characterized in that in the presence of. of a solvent works.
CH303514D 1951-07-30 1951-07-30 Process for the preparation of a quaternary ammonium compound. CH303514A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH301409T 1951-07-30
CH303514T 1951-07-30

Publications (1)

Publication Number Publication Date
CH303514A true CH303514A (en) 1954-11-30

Family

ID=25734325

Family Applications (1)

Application Number Title Priority Date Filing Date
CH303514D CH303514A (en) 1951-07-30 1951-07-30 Process for the preparation of a quaternary ammonium compound.

Country Status (1)

Country Link
CH (1) CH303514A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1274281B (en) * 1965-12-02 1968-08-01 Unilever Nv Germicide

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1274281B (en) * 1965-12-02 1968-08-01 Unilever Nv Germicide

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