CH303510A - Process for the preparation of a quaternary ammonium compound. - Google Patents

Process for the preparation of a quaternary ammonium compound.

Info

Publication number
CH303510A
CH303510A CH303510DA CH303510A CH 303510 A CH303510 A CH 303510A CH 303510D A CH303510D A CH 303510DA CH 303510 A CH303510 A CH 303510A
Authority
CH
Switzerland
Prior art keywords
quaternary ammonium
ammonium compound
preparation
oxyethyl
dependent
Prior art date
Application number
Other languages
German (de)
Inventor
Zuerich Friedrich Seifenfabrik
Original Assignee
Friedrich Steinfels Ag Seifenf
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Friedrich Steinfels Ag Seifenf filed Critical Friedrich Steinfels Ag Seifenf
Publication of CH303510A publication Critical patent/CH303510A/en

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/655—Compounds containing ammonium groups
    • D06P1/66—Compounds containing ammonium groups containing quaternary ammonium groups
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
    • A01N31/12—Bis-chlorophenols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines

Landscapes

  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Pest Control & Pesticides (AREA)
  • Organic Chemistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Description

       

  <B>Zusatzpatent</B> zum Hauptpatent Nr. 301409.    Verfahren zur Herstellung     einer        quaternären        Ammoniumverbindung.            Gegenstand    des vorliegenden Patentes ist  ein Verfahren zur Herstellung einer neuen       quaternären        Ammoniumverbindung,    das da  durch gekennzeichnet ist, dass man     Di(oxy-          äthyl)-octyloxyäthylamin    mit     Benzylbromid     zur Reaktion bringt.  



  Das neue kristalline     Reaktionsprodukt    löst  sich in destilliertem und hartem Wasser voll  ständig klar mit neutraler Reaktion und unter  starker Schaumbildung. Es hat wertvolle  Eigenschaften als Färbe-, Egalisier- und     Avi-          vagemittel.    Mit     substantiven    Farbstoffen bildet  es Komplexverbindungen und erhöht so die  Wasserechtheit     substantiver    Färbungen. Da es  gleichzeitig ein     Aufziehvermögen    auf die Faser  besitzt, kann man es als     substantives        Avivage-          mittel    bezeichnen.  



  Ausserdem besitzt dieser Stoff eine starke  bakterizide und     bakteriostatische    Wirkung und  kann deshalb vorzüglich als Desinfektions  mittel verwendet werden. ,         Beispiel:     1.     Mol    reines     Di(oxyäthyl)-octyloxyäthyl-          amin        (Kp.    138 bis 141'C/0,02 mm     Hg)    wird  mit 1     Mol.    reinem     Benzylbromid    vermischt und  bis zur Beendigung der Reaktion stehenge  lassen.     Diese    Reaktion kann ohne Zusätze oder  unter Verwendung eines geeigneten Lösungs-    mittels wie z. B.     Äthyläther    erfolgen.

   Das  Reaktionsprodukt kristallisiert und wird vor  teilhaft aus einem passenden Lösungsmittel  wie z. B.     Essigsäureäthylester    oder einem Ge  misch von     Essigsäureäthylester    und     Äthyläther     umkristallisiert. Es kristallisiert in glänzenden  Blättchen vom Schmelzpunkt 75 bis 75,5  C.



  <B> Additional patent </B> to main patent no. 301409. Process for the production of a quaternary ammonium compound. The subject matter of the present patent is a process for the preparation of a new quaternary ammonium compound which is characterized in that di (oxyethyl) octyloxyethylamine is reacted with benzyl bromide.



  The new crystalline reaction product dissolves in distilled and hard water completely clear with a neutral reaction and with strong foaming. It has valuable properties as a coloring, leveling and avivating agent. It forms complex compounds with substantive dyes and thus increases the waterfastness of substantive dyes. Since it can also be absorbed by the fiber, it can be called a substantive finishing agent.



  In addition, this substance has a strong bactericidal and bacteriostatic effect and can therefore be used as a disinfectant. , Example: 1. Mol of pure di (oxyethyl) octyloxyethylamine (bp. 138 to 141 ° C / 0.02 mm Hg) is mixed with 1 mole of pure benzyl bromide and left to stand until the reaction is complete. This reaction can be carried out without additives or using a suitable solvent such as. B. Ethyl ether.

   The reaction product crystallizes and is taken from a suitable solvent such as. B. ethyl acetate or a Ge mixture of ethyl acetate and ethyl ether recrystallized. It crystallizes in shiny flakes with a melting point of 75 to 75.5 C.

Claims (1)

PATEN TANS'PRUCH Verfahren zur Herstellung einer neuen quaternären Ammoniumverbindung, dadurch gekennzeichnet, dass man Di(oxyäthyl)-octyl- oxyäthyl-amin mit Benzylbromid zur Umset zung bringt. Die neue Verbindung bildet glänzende Blättchen vom Schmelzpunkt 75 bis 75,5 C. UNTERANSPRÜCHE 1. Verfahren nach Patentanspruch, dadurch gekennzeichnet, dass man mit äquimolaren Mengen der Ausgangsstoffe arbeitet. 2. PATENT TANS'PRUCH Process for the production of a new quaternary ammonium compound, characterized in that di (oxyethyl) octyl oxyethyl amine is reacted with benzyl bromide. The new compound forms shiny flakes with a melting point of 75 to 75.5 C. SUBSTANTIAL CLAIMS 1. Process according to patent claim, characterized in that equimolar amounts of the starting materials are used. 2. Verfahren nach Patentanspruch und Unteranspruch 1, dadurch gekennzeichnet, dass man die quaternäre Ammoniumverbindung zur Reinigung umkristallisiert. 3. Verfahren nach Patentanspruch und Unteranspruch 1, dadurch gekennzeichnet, dass man in Gegenwart eines Lösungsmittels ar beitet. Process according to claim and dependent claim 1, characterized in that the quaternary ammonium compound is recrystallized for purification. 3. The method according to claim and dependent claim 1, characterized in that ar processed in the presence of a solvent.
CH303510D 1951-07-30 1951-07-30 Process for the preparation of a quaternary ammonium compound. CH303510A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH303510T 1951-07-30
CH301409T 1951-07-30

Publications (1)

Publication Number Publication Date
CH303510A true CH303510A (en) 1954-11-30

Family

ID=25734321

Family Applications (1)

Application Number Title Priority Date Filing Date
CH303510D CH303510A (en) 1951-07-30 1951-07-30 Process for the preparation of a quaternary ammonium compound.

Country Status (1)

Country Link
CH (1) CH303510A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1274281B (en) * 1965-12-02 1968-08-01 Unilever Nv Germicide

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1274281B (en) * 1965-12-02 1968-08-01 Unilever Nv Germicide

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