CH227743A - Process for the preparation of a solid molecular compound containing mercury. - Google Patents
Process for the preparation of a solid molecular compound containing mercury.Info
- Publication number
- CH227743A CH227743A CH227743DA CH227743A CH 227743 A CH227743 A CH 227743A CH 227743D A CH227743D A CH 227743DA CH 227743 A CH227743 A CH 227743A
- Authority
- CH
- Switzerland
- Prior art keywords
- molecular compound
- solution
- compound
- preparation
- compound containing
- Prior art date
Links
- 150000001875 compounds Chemical class 0.000 title claims description 11
- 239000007787 solid Substances 0.000 title claims description 7
- 238000000034 method Methods 0.000 title claims description 6
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 title claims description 4
- 229910052753 mercury Inorganic materials 0.000 title claims description 4
- 239000000243 solution Substances 0.000 claims description 6
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- YAPQBXQYLJRXSA-UHFFFAOYSA-N theobromine Chemical compound CN1C(=O)NC(=O)C2=C1N=CN2C YAPQBXQYLJRXSA-UHFFFAOYSA-N 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 229940100892 mercury compound Drugs 0.000 claims description 3
- 150000002731 mercury compounds Chemical class 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 238000001704 evaporation Methods 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 230000001376 precipitating effect Effects 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 229960004559 theobromine Drugs 0.000 claims description 2
- 238000001556 precipitation Methods 0.000 claims 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/10—Mercury compounds
- C07F3/12—Aromatic substances containing mercury
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicinal Preparation (AREA)
Description
Verfahren zur Herstellung einer festen quecksilberhaltigen Holekularverbindung. . Gegenstand des vorliegenden Zusatz patentes ist ein Verfahren zur Herstellung einer festen quecksilberhaltigen Molekular verbindung, das dadurch gekennzeichnet ist, dass man die komplexe Quecksilberverbin dung des salicylallylamid - 0 -essigsauren hTatriums der Formel:
EMI0001.0008
und Theobramin in wäBriger Lösung aufein ander einwirken, lässt und aus der Lösung die entstandene Molekularverbindung in fester Form ausscheidet, vorzugsweise durch Zusatz geeigneter fällender Lösungsmittel oder durch Eindampfen der Lösung zur Trockne.
Beispiel: 10.g der komplexen Quecksilberverbin dung des Salicylallylamid-0-essigsauren Na triums der Formel;
EMI0001.0017
und 4 g Theobromin werden in 100 cm' Wasser unter Schütteln gelöst, und im Va kuum wird dann diese Lösung zur Trockne eingedampft. Dabei wird ein fester, leicht pulverisierbarer Körper erhalten, der die Molekularverbindung darstellt.
Die erhaltene neue Verbindung, die in der Therapie verwendet werden soll, ist ein farbloses, lichtbeständiges Pulver, :das .sich leicht und klar in Wasser mit curcuma- alkalischer Reaktion löst und in Äther und Aceton unlöslich ist.
Process for the production of a solid mercury-containing molecular compound. . The subject of the present additional patent is a process for the production of a solid mercury-containing molecular compound, which is characterized in that the complex mercury compound of salicylallylamide-0-acetic acid sodium of the formula:
EMI0001.0008
and theobramine in aqueous solution can act on one another, and the resulting molecular compound is precipitated in solid form from the solution, preferably by adding suitable precipitating solvents or by evaporating the solution to dryness.
Example: 10.g of the complex mercury compound of salicylallylamide-0-acetic acid sodium of the formula;
EMI0001.0017
and 4 g of theobromine are dissolved in 100 cm 'of water with shaking, and this solution is then evaporated to dryness in a vacuum. A solid, easily pulverizable body is obtained, which represents the molecular compound.
The new compound obtained, which is to be used in therapy, is a colorless, light-resistant powder: that dissolves easily and clearly in water with a curcuma-alkaline reaction and is insoluble in ether and acetone.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH227743T | 1938-11-29 | ||
| CH219010T | 1938-11-29 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH227743A true CH227743A (en) | 1943-06-30 |
Family
ID=25726235
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH227743D CH227743A (en) | 1938-11-29 | 1938-11-29 | Process for the preparation of a solid molecular compound containing mercury. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH227743A (en) |
-
1938
- 1938-11-29 CH CH227743D patent/CH227743A/en unknown
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