CH204443A - Process for the production of a new azo dye. - Google Patents

Process for the production of a new azo dye.

Info

Publication number
CH204443A
CH204443A CH204443DA CH204443A CH 204443 A CH204443 A CH 204443A CH 204443D A CH204443D A CH 204443DA CH 204443 A CH204443 A CH 204443A
Authority
CH
Switzerland
Prior art keywords
azo dye
benzoylamino
new azo
production
amino
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH204443A publication Critical patent/CH204443A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00—Monoazo dyes prepared by diazotising and coupling
    • C09B29/24—Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
    • C09B29/28—Amino naphthols
    • C09B29/30—Amino naphtholsulfonic acid
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00—Monoazo dyes prepared by diazotising and coupling
    • C09B29/34—Monoazo dyes prepared by diazotising and coupling from other coupling components
    • C09B29/36—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds
    • C09B29/3604—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom
    • C09B29/3647—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms
    • C09B29/3652—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles
    • C09B29/366—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles containing hydroxy-1,2-diazoles, e.g. pyrazolone

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

  Verfahren zur Herstellung eines neuen     Azofarbstoffes.       Es wurde gefunden, dass man einen neuen       Azofarbstoff    erhält, wenn man 1     Mol        1-(3'-          [3"-    (4"'-     Amino)        -benzoylamino    - 5" -     aminol        -          benzoylamino)-phenyl-    5     -pyrazolon-3-carbon-          säure        mit    1     Mol        diazotierter        Sulfanilsäure     vereinigt.

   Der so erhaltene Farbstoff bildet  ein     hellviolettbraunes    Pulver, das sich in  Wasser mit gelber Farbe löst und Baum  wolle in gelben Tönen färbt, die durch     ZV        ei-          terdiazotieren    auf der Faser und     Entwickeln     mit     ss-Naphthol    intensiv orangerot werden.

      <I>Beispiel:</I>    173 Teile     Sulfanilsäure    werden in üb  licher Weise     diazotiert.    Die     Diazolösung     wird in eine kalte; mit 10     J        iger    Essigsäure  schwach angesäuerte Lösung aus 496 Teilen  1-     (3'-    [3" - (4"' -     Amino)    -     benzoylamino    - 5"  amino]     -benzoylamino)        -phenyl-5-pyrazolon-3-          carbonsäure,    140 Teilen Natronlauge ä     30%,       200 Teilen kristallisiertem     Natriumacetat     und 20 000 Teilen Wasser eingerührt.

   Nach  beendeter     Kupplung    wird der Farbstoff aus  gesalzen,     abfiltriert    und getrocknet.



  Process for the production of a new azo dye. It has been found that a new azo dye is obtained if 1 mole of 1- (3'- [3 "- (4" '- amino) -benzoylamino - 5 "- aminol - benzoylamino) -phenyl-5-pyrazolone-3 carbonic acid combined with 1 mol of diazotized sulfanilic acid.

   The dye obtained in this way forms a light purple-brown powder which dissolves in water with a yellow color and dyes cotton in yellow tones which become intensely orange-red when the fibers are diazotized with pus and developed with s-naphthol.

      <I> Example: </I> 173 parts of sulfanilic acid are diazotized in the usual way. The diazo solution is in a cold; solution of 496 parts of 1- (3'- [3 "- (4" '- amino) - benzoylamino - 5 "amino] -benzoylamino) -phenyl-5-pyrazolone-3-carboxylic acid, weakly acidified with 10 J acetic acid, 140 Parts of 30% sodium hydroxide solution, 200 parts of crystallized sodium acetate and 20,000 parts of water are stirred in.

   After coupling has ended, the dyestuff is salted out, filtered off and dried.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Azofarbstoffes, dadurch gekennzeichnet, dass 1 Mol 1-(3'- [3"-(4"'-Amino)-benzoylamino-5" amino]-benzoylamino)-phenyl-5-pyrazolon- 3-carbonsäure mit 1 Mol diazotierter Sulfanil- säure vereinigt. Claim: Process for the preparation of a new azo dye, characterized in that 1 mol of 1- (3'- [3 "- (4" '- amino) -benzoylamino-5 "amino] -benzoylamino) -phenyl-5-pyrazolone- 3 -carboxylic acid combined with 1 mol of diazotized sulfanilic acid. Der so erhaltene Farbstoff bildet ein hellviolett-braunes Pulver, das sich in Wasser mit gelber Farbe löst und Baum wolle in gelben Tönen färbt, die durch Wei- terdiazotieren auf der Faser und Entwickeln mit ss-Naphthol intensiv orangerot werden. The dye obtained in this way forms a light purple-brown powder which dissolves in water with a yellow color and dyes cotton in yellow tones, which become intensely orange-red when the fibers are further diazotized and developed with ss-naphthol.
CH204443D 1937-02-10 1937-02-10 Process for the production of a new azo dye. CH204443A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH204443T 1937-02-10
CH200672T 1938-10-31

Publications (1)

Publication Number Publication Date
CH204443A true CH204443A (en) 1939-04-30

Family

ID=25723547

Family Applications (1)

Application Number Title Priority Date Filing Date
CH204443D CH204443A (en) 1937-02-10 1937-02-10 Process for the production of a new azo dye.

Country Status (1)

Country Link
CH (1) CH204443A (en)

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