CH171588A - Process for producing a water-soluble diazoamido compound. - Google Patents

Process for producing a water-soluble diazoamido compound.

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Publication number
CH171588A
CH171588A CH171588DA CH171588A CH 171588 A CH171588 A CH 171588A CH 171588D A CH171588D A CH 171588DA CH 171588 A CH171588 A CH 171588A
Authority
CH
Switzerland
Prior art keywords
water
soluble
compound
diazoamido
producing
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH171588A publication Critical patent/CH171588A/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung einer     wasserlösliehen        Diazoamidoverbindung.       Gegenstand des vorliegenden Patentes ist  ein Verfahren zur Herstellung einer wasser  löslichen     Diazoamidoverbindnng.    Es ist da  durch gekennzeichnet, dass man     Piperidin-          3-sialfonsäure    auf     diazotiertes        1-Amino-4-(4'-          metliyl        -phenoxyacetylamino)    - 2,5-     dimethoxy-          benzol    in Gegenwart eines säurebindenden  Mittels einwirken lässt.  



  <I>Beispiel:</I>  In eine wässerige Lösung von     1"7        gr        pipe-          ridin-3-sulfonsaurem        Natrium    und 20     gi-    Soda  lässt man bei<B>150</B> eine     Diazolösung    aus 23     gr     1-     Amino-    4 - (4' -     methylphenoxyacetylamino)-          2,5-dimethogybenzol    langsam zufliessen. Die       Reaktion    ist schnell beendet. Aus der Lösung  wird die gelblich gefärbte Diazoamidoverbin-    Jung bei 40   durch Zusatz von Kochsalz  ausgefällt.

   Sie ist in Wasser löslich und ist  ein wertvolles Produkt für     Färbereizwecke.  



  Process for producing a water-soluble diazoamido compound. The subject of the present patent is a process for the preparation of a water-soluble diazoamido compound. It is characterized in that piperidine-3-sialfonic acid is allowed to act on diazotized 1-amino-4- (4'-methylphenoxyacetylamino) -2,5-dimethoxybenzene in the presence of an acid-binding agent.



  <I> Example: </I> A diazo solution of 23 g 1-amino is added at <B> 150 </B> to an aqueous solution of 1 "7 gr. Of piperidine-3-sulfonic acid sodium and 20 g - 4 - (4 '- methylphenoxyacetylamino) - 2,5-dimethogybenzene slowly pour in. The reaction is quickly over. The yellowish colored diazoamido compound is precipitated from the solution by adding sodium chloride.

   It is soluble in water and is a valuable product for dyeing purposes.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung einer wasser löslichen Diazoamidoverbindung, dadurch ge kennzeichnet, dass man Piperidin.3-sulfonsäui-e auf diazotiertes 1-Amino-4-(4'-methylphen- oxyacetylamino) - 2,5 - dimethoxybenzol in Gegenwart eines säurebindenden Mittels ein wirken lässt. Die neue, wasserlösliche Verbindung be sitzt eine gelbliche Farbe. Claim: Process for the preparation of a water-soluble diazoamido compound, characterized in that one piperidine.3-sulfonic acid on diazotized 1-amino-4- (4'-methylphenoxyacetylamino) -2,5-dimethoxybenzene in the presence of an acid-binding agent one lets work. The new, water-soluble compound has a yellowish color.
CH171588D 1932-05-23 1933-05-11 Process for producing a water-soluble diazoamido compound. CH171588A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE171588X 1932-05-23
CH169351T 1933-05-11

Publications (1)

Publication Number Publication Date
CH171588A true CH171588A (en) 1934-08-31

Family

ID=25718713

Family Applications (1)

Application Number Title Priority Date Filing Date
CH171588D CH171588A (en) 1932-05-23 1933-05-11 Process for producing a water-soluble diazoamido compound.

Country Status (1)

Country Link
CH (1) CH171588A (en)

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