CH155014A - Process for the production of a new azo dye. - Google Patents

Process for the production of a new azo dye.

Info

Publication number
CH155014A
CH155014A CH155014DA CH155014A CH 155014 A CH155014 A CH 155014A CH 155014D A CH155014D A CH 155014DA CH 155014 A CH155014 A CH 155014A
Authority
CH
Switzerland
Prior art keywords
production
azo dye
new azo
new
new dye
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH155014A publication Critical patent/CH155014A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/10Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
    • C09B29/18Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides
    • C09B29/20Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides of the naphthalene series

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

      Verfahren    zur     Herstellung    eines neuen     Azofarbstoffes.       Es wurde gefunden, dass man einen neuen  Farbstoff erhält, welcher der Formel:  
EMI0001.0004     
    entspricht, wenn man dianotiertes 4-(1'       Methyl)-phenoxyacetylamino-2,5-dimethoxy-l-          aminobenzol    mit dem     p-Phenetidid    der 2 .     3-          Oxynaphthoesäure    kuppelt.  



  Der neue Farbstoff bildet ein dunkel  violettes Pulver. Auf geeigneten Substraten,  wie zum Beispiel pflanzlichen Fasern, her  gestellt, färbt er diese in echten violetten  Tönen.  



  <I>Beispiel:</I>  31,6 Teile     4-(1'-Methyl)-phenoxyacetyl-          amino-2,5-dimethoxy-l-aminobenzol    werden  wie üblich dianotiert und in eine Lösung von  30,7 Teilen des     p-Phenetidids    der 2.     3-Oxy-          naphthoesäure,    50 Teilen 30      /oiger    Natron  lauge, 30 Teilen Soda und 2000 Teilen    Wasser eingetragen. Der gebildete Farbstoff  fällt sofort aus. Der dunkelviolette Nieder  schlag wird filtriert und getrocknet.



      Process for the production of a new azo dye. It has been found that a new dye is obtained which has the formula:
EMI0001.0004
    corresponds if one dianotated 4- (1 'methyl) -phenoxyacetylamino-2,5-dimethoxy-l-aminobenzene with the p-phenetidide of the 2. 3- oxynaphthoic acid couples.



  The new dye forms a dark purple powder. Produced on suitable substrates, such as vegetable fibers, he dyes them in real purple tones.



  <I> Example: </I> 31.6 parts of 4- (1'-methyl) -phenoxyacetyl-amino-2,5-dimethoxy-1-aminobenzene are dianotized as usual and poured into a solution of 30.7 parts of the p -Phenetidids of the 2. 3-oxynaphthoic acid, 50 parts of 30% sodium hydroxide solution, 30 parts of soda and 2000 parts of water entered. The dye formed precipitates immediately. The dark purple precipitate is filtered and dried.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Farbstoffes, welcher der Formel: OCHS I N=N- < __,>-NHCOCH2-0- < ::>-CHs I 0g OCH3 C CONH--C>-0C2H5 entspricht, dadurch gekennzeichnet, dass man dianotiertes 4-(1'-DIethyl)-phenoxyacetylamino- 2.5-dimethoxy-l-aminobenzol mit dem p-Phe- netidid der 2.3-Oxynaphthoesäure kuppelt. Der neue Farbstoff bildet ein dunkel violettes Pulver. PATENT CLAIM: Process for the production of a new dye which corresponds to the formula: OCHS IN = N- <__,> - NHCOCH2-0- <::> - CHs I 0g OCH3 C CONH - C> -0C2H5, characterized in that dianotated 4- (1'-DIethyl) -phenoxyacetylamino-2.5-dimethoxy-1-aminobenzene is coupled with the p-phenetidide of 2.3-oxynaphthoic acid. The new dye forms a dark purple powder. Auf geeigneten Substraten, wie zum Beispiel pflanzlichen Fasern, herge stellt, färbt er diese in echten violetten Tönen. On suitable substrates, such as vegetable fibers, he dyes them in real purple tones.
CH155014D 1930-10-25 1930-10-25 Process for the production of a new azo dye. CH155014A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH155014T 1930-10-25
CH152881T 1930-10-25

Publications (1)

Publication Number Publication Date
CH155014A true CH155014A (en) 1932-05-31

Family

ID=25716066

Family Applications (1)

Application Number Title Priority Date Filing Date
CH155014D CH155014A (en) 1930-10-25 1930-10-25 Process for the production of a new azo dye.

Country Status (1)

Country Link
CH (1) CH155014A (en)

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